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Presented By
Rahul Kshirsagar (11505619)
Under the guidance of
Mr.Sumit Shoor
OUTLINE
 Introduction.
 Scope of the study.
 Objectives of the study.
 Review of Literature.
 Materials, Equipments and Manufacturing Process.
 Research Methodology.
 Experimentation.
 Numerical Modeling.
 Results and Discussions .
 Conclusions.
 References
INTRODUCTION
1. Composite Materials : A composite material that is “Composition
of Materials” consists of reinforcing phase like fibers, particles or
sheets ingrained in the matrix phase.
2. Reinforcing material is the main load carrying member.
3. Matrix phase holds the reinforcing material in the defined position
and transfers load between them. It also protects the reinforcing
materials from damage throughout the composite processing.
4. Biocomposites : Combination of natural fibers and synthetic epoxy
resin.
5. Natural fiber reinforced biocomposites are captivating interest these
days, owing to their exceptional properties like high specific
strength, renewability and sustainability made them acceptable for
many engineering applications.
6. Major disadvantage: Hydrophilic nature of natural fibers resulting
in poor interfacial properties.
Continued…
7. Alkali treatments of the natural fibers enhance these interfacial
properties by surface modification, which reduces their hydrophilic
nature
8. Research on single natural fiber reinforced bio composites primarily
concentrates on enhancing the physical and chemical properties like
low wettability, inadequate adhesion and high moisture absorption
9. In order to improve the mechanical properties of natural fiber
composites, hybridization is adapted in the composite design.
10. Hybrid Biocomposites : Hybrid Biocomposites are the
combination of two or more natural fibers ingrained in the single
matrix phase
SCOPE OF THE STUDY
1. Cheap rates, hence little investments.
2. No emission of carbon dioxide during production, hence positive
effect towards environment.
3. Natural fibers are completely absorbed in the soil and thereby
provide nourishment in the soil.
4. Applications :
i. Toys
ii. Automobiles, aircrafts, ships.
iii. Casing of electronics applications.
iv. Construction applications like door, ceiling panels, roofing
panels.
OBJECTIVES OF THE STUDY
1. Fabrication of bio-composites from alkali treated uni-
directional Jute and Banana fibers oriented in the directions
90°/45°/-45°/90° and varying hardener & resin ratios (100:10
and 100:20).
2. To evaluate mechanical properties ( Tensile , Flexural and Impact
Strength)
3. To evaluate physical properties ( Hardness and Water Absorption).
4. To analyze mechanical properties using FEM software like ANSYS
APDL.
5. To compare the experimental and ANSYS APDL Results.
REVIEW OF LITERATURE
Continued…
Continued…
MATERIALS, EQUIPMENTS AND
MANUFACTURING PROCESS
1. Materials:
i. Natural fiber such as jute fiber and banana fiber are used for
reinforcement
ii. Epoxy Resin [EPOFINE -230] and Hardener [FINEHARD-951] is
used as matrix. EPOFINE-230 is an electrical grade liquid epoxy
casting resin and FINEHARD-951 is a polyamine hardener
iii. The mixing ratio of the epoxy and hardener is 100:10 and 100:20.
Continued…
2. Equipments:
i. Pycnometer.
ii. Universal tensile testing machine.
iii. Flexural testing machine.
iv. Charpy impact test set-up.
v. Rockwell hardness tester.
vi. Electronic weighing machine.
Continued…
3. Manufacturing Process:
Continued…
All the composite samples fabricated, have the fiber volume fraction
(Vf) of 25.92% calculated using the formula:
Continued…
Constituents of Hybrid Biocomposites
RESESRCH METHODOLOGY
EXPERIMENTATION
1. Determination of Mechanical Properties:
i. Tensile testing: Universal tensile testing machine with
maximum capacity of 1000 Kg has used. Testing has conducted as
per the standard ASTM D-3039 with gauge length of 150 mm.
Continued…
Specimens for Tensile Testing
Tensile testing of HBCs sample
Continued…
ii. Flexural testing: Flexural testing determined on the same machine
with maximum capacity of 225 Kg on the load cell of three point
flexural testing. Testing has conducted as per the standard ASTM D-
790. Specimen was supported horizontally in between two edges 60
mm apart.
Continued…
Specimens for Flexural Testing
Flexural Testing of HBCs sample
Continued…
iii. Impact testing: The impact strength has determined in Charpy
impact test set-up as per the standard ASTM D-256.
Specimens for Impact Testing
Continued…
2. Determination of Physical Properties:
i. Water Absorption Test: The test has conducted as per the
standard ASTM D-570. The composites of size 25 mm x 25mm
has cut and weighted and immersed in water for 72 hours. After
the samples were removed from water and weighted again.
ii. Rockwell Hardness Test: The hardness test determined using
ball indentor of 1/16” with 100 kg load applied as per the standard
ASTM D-785.
Numerical Modeling
1. Rules of mixture (ROM) and Hybrid rules of mixture (HROM) have
used to evaluate orthotropic elastic constants of the composites
shown in below tables.
Orthotropic Properties for Separate Layer of Jute and Banana Fibers
Continued…
Orthotropic Properties for Combined Layers of Jute and Banana Fibers
RESULTS AND DISCUSSIONS
1. Experimental Results:
Continued…
JBBJ-1 BJJB-1
0
50
100
150
200
250
300
350
400
450
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.3
Load(KG)
Displacement (mm)
0
50
100
150
200
250
300
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.68
Load(KG)
Displacement (mm)
Load-Displacement Curves for the Composites
Continued…
JBBJ-2 BJJB-2
0
50
100
150
200
250
300
350
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.66
Load(KG)
Displacement (mm)
0
20
40
60
80
100
120
140
160
180
200
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.71
Load(KG)
Displacement (mm)
Continued…
JBBJ-1 BJJB-1
0
10
20
30
40
50
60
0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.5 2.75 2.84
Load(KG)
Deflection (mm)
0
5
10
15
20
25
30
35
0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.5 2.75 3
Load(KG)
Deflection (mm)
Load-Deflection Curves for the Composites
Continued…
JBBJ-2 BJJB-2
0
5
10
15
20
25
30
0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.35
Load(KG)
Deflection (mm)
0
5
10
15
20
25
30
Load(KG)
Deflection (mm)
Continued…
2. ANSYS Simulation Results:
Deformed Tensile Shape and Von Misses Stress developed in
JBBJ-1 using ROM
Tensile Behavior of HBCs Sample JBBJ-1 using ROM
Deformed Tensile Shape and Von Misses Stress developed in
JBBJ-1 using HROM
Tensile Behavior of HBCs sample JBBJ-1 using HROM
Deformed Flexural Shape and Von Misses Stress developed in
JBBJ-1 using ROM
Flexural Behavior HBCs sample JBBJ-1 using ROM
Deformed Flexural Shape and Von Misses Stress developed in
JBBJ-1 using HROM
Flexural Behavior of HBCs sample JBBJ-1 using HROM
Continued…
Tensile Properties Flexural Properties
0
5
10
15
20
25
30
35
JBBJ-1 BJJB-1 JBBJ-2 BJJB-2
TensileStrength(MPa)
Composite Samples
Experiment
al Values
ANSYS
Values
using ROM
0
10
20
30
40
50
60
70
80
90
JBBJ-1 BJJB-1 JBBJ-2 BJJB-2
FlexuralStrength(MPa)
Composite Samples
Experimental
Values
ANSYS
Values using
ROM
3. Comparison Between Experimental and ANSYS APDL Results:
Continued…
4. Determination of Percentage Error:
It gives the approximation between calculated and known values.
Calculated values = ANSYS Results and Known values =
Experimental Results.
Continued…
% Error in Tensile
Properties
% Error in Flexural
Properties
CONCLUSIONS
i. For the same Vf , the HBCs samples of jute fibers oriented at 900
and banana fibers oriented at 450 and -450 exhibits higher
properties in each case compared to HBCs sample of banana
fibers oriented at 900and jute fibers oriented at 450 and -450.
ii. For the same Vf and similar orientation of jute and banana fibers,
HBCs fabricated with resin and hardener ratio of 100:10 exhibits
maximum mechanical and physical properties in contrast to the
HBCs fabricated with resin and hardener ratio of 100:20.
iii. After evaluation of the properties in each case for all the HBCs
samples, it has observed that the composite sample JBBJ-1
performed maximum mechanical and physical properties in each
case. Therefore, optimal results are obtained with composite
sample JBBJ-1.
iv. The experimental results for the mechanical properties of HBCs
in each case show good agreement with the ANSYS APDL results.
REFERENCES
1. Boopalan M., Niranjanaa M., and Umapathy M. J. (2013), “Study on
the mechanical properties and thermal properties of jute and banana
fiber reinforced epoxy hybrid composites,” Compos. Part B, vol. 51,
pp. 54–57.
2. John M. J. and Thomas S. (2008), “Biofibres and biocomposites,”
Carbohydr. Polym, vol. 71,pp. 343–364.
3. Essabir H., Bensalah M. O., Rodrigue D., Bouhfid R., Qaiss A. (2016),
“Structural , mechanical and thermal properties of bio-based hybrid
composites from waste coir residues : Fibers and shell particles,”
Mech. Mater., vol. 93, pp. 134–144.
Continued…
4. Paul V., Kanny K., and Redhi G. G. (2015), “Mechanical , thermal and
morphological properties of a bio-based composite derived from
banana plant source,” Compos. PART A, vol. 68, pp. 90–100.
5. Merlini C., Soldi V. and Barra G. M. O. (2011), “In fl uence of fiber
surface treatment and length on physico-chemical properties of
short random banana fiber-reinforced castor oil polyurethane
composites,” Polym. Test., vol. 30, pp. 833–840.
6. Wambua P., Ivens I., and Verpoest I. (2003), “Natural fibers : can they
replace glass in fibre reinforced plastics ?,” Composites Science and
Technology, vol. 63, pp. 1259–1264.
THANK YOU

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Hybrid Biocomposites Research

  • 1. Presented By Rahul Kshirsagar (11505619) Under the guidance of Mr.Sumit Shoor
  • 2. OUTLINE  Introduction.  Scope of the study.  Objectives of the study.  Review of Literature.  Materials, Equipments and Manufacturing Process.  Research Methodology.  Experimentation.  Numerical Modeling.  Results and Discussions .  Conclusions.  References
  • 3. INTRODUCTION 1. Composite Materials : A composite material that is “Composition of Materials” consists of reinforcing phase like fibers, particles or sheets ingrained in the matrix phase. 2. Reinforcing material is the main load carrying member. 3. Matrix phase holds the reinforcing material in the defined position and transfers load between them. It also protects the reinforcing materials from damage throughout the composite processing. 4. Biocomposites : Combination of natural fibers and synthetic epoxy resin. 5. Natural fiber reinforced biocomposites are captivating interest these days, owing to their exceptional properties like high specific strength, renewability and sustainability made them acceptable for many engineering applications. 6. Major disadvantage: Hydrophilic nature of natural fibers resulting in poor interfacial properties.
  • 4. Continued… 7. Alkali treatments of the natural fibers enhance these interfacial properties by surface modification, which reduces their hydrophilic nature 8. Research on single natural fiber reinforced bio composites primarily concentrates on enhancing the physical and chemical properties like low wettability, inadequate adhesion and high moisture absorption 9. In order to improve the mechanical properties of natural fiber composites, hybridization is adapted in the composite design. 10. Hybrid Biocomposites : Hybrid Biocomposites are the combination of two or more natural fibers ingrained in the single matrix phase
  • 5. SCOPE OF THE STUDY 1. Cheap rates, hence little investments. 2. No emission of carbon dioxide during production, hence positive effect towards environment. 3. Natural fibers are completely absorbed in the soil and thereby provide nourishment in the soil. 4. Applications : i. Toys ii. Automobiles, aircrafts, ships. iii. Casing of electronics applications. iv. Construction applications like door, ceiling panels, roofing panels.
  • 6. OBJECTIVES OF THE STUDY 1. Fabrication of bio-composites from alkali treated uni- directional Jute and Banana fibers oriented in the directions 90°/45°/-45°/90° and varying hardener & resin ratios (100:10 and 100:20). 2. To evaluate mechanical properties ( Tensile , Flexural and Impact Strength) 3. To evaluate physical properties ( Hardness and Water Absorption). 4. To analyze mechanical properties using FEM software like ANSYS APDL. 5. To compare the experimental and ANSYS APDL Results.
  • 10. MATERIALS, EQUIPMENTS AND MANUFACTURING PROCESS 1. Materials: i. Natural fiber such as jute fiber and banana fiber are used for reinforcement ii. Epoxy Resin [EPOFINE -230] and Hardener [FINEHARD-951] is used as matrix. EPOFINE-230 is an electrical grade liquid epoxy casting resin and FINEHARD-951 is a polyamine hardener iii. The mixing ratio of the epoxy and hardener is 100:10 and 100:20.
  • 11. Continued… 2. Equipments: i. Pycnometer. ii. Universal tensile testing machine. iii. Flexural testing machine. iv. Charpy impact test set-up. v. Rockwell hardness tester. vi. Electronic weighing machine.
  • 13. Continued… All the composite samples fabricated, have the fiber volume fraction (Vf) of 25.92% calculated using the formula:
  • 16. EXPERIMENTATION 1. Determination of Mechanical Properties: i. Tensile testing: Universal tensile testing machine with maximum capacity of 1000 Kg has used. Testing has conducted as per the standard ASTM D-3039 with gauge length of 150 mm.
  • 17. Continued… Specimens for Tensile Testing Tensile testing of HBCs sample
  • 18. Continued… ii. Flexural testing: Flexural testing determined on the same machine with maximum capacity of 225 Kg on the load cell of three point flexural testing. Testing has conducted as per the standard ASTM D- 790. Specimen was supported horizontally in between two edges 60 mm apart.
  • 19. Continued… Specimens for Flexural Testing Flexural Testing of HBCs sample
  • 20. Continued… iii. Impact testing: The impact strength has determined in Charpy impact test set-up as per the standard ASTM D-256. Specimens for Impact Testing
  • 21. Continued… 2. Determination of Physical Properties: i. Water Absorption Test: The test has conducted as per the standard ASTM D-570. The composites of size 25 mm x 25mm has cut and weighted and immersed in water for 72 hours. After the samples were removed from water and weighted again. ii. Rockwell Hardness Test: The hardness test determined using ball indentor of 1/16” with 100 kg load applied as per the standard ASTM D-785.
  • 22. Numerical Modeling 1. Rules of mixture (ROM) and Hybrid rules of mixture (HROM) have used to evaluate orthotropic elastic constants of the composites shown in below tables. Orthotropic Properties for Separate Layer of Jute and Banana Fibers
  • 23. Continued… Orthotropic Properties for Combined Layers of Jute and Banana Fibers
  • 24. RESULTS AND DISCUSSIONS 1. Experimental Results:
  • 25. Continued… JBBJ-1 BJJB-1 0 50 100 150 200 250 300 350 400 450 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.3 Load(KG) Displacement (mm) 0 50 100 150 200 250 300 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.68 Load(KG) Displacement (mm) Load-Displacement Curves for the Composites
  • 26. Continued… JBBJ-2 BJJB-2 0 50 100 150 200 250 300 350 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.66 Load(KG) Displacement (mm) 0 20 40 60 80 100 120 140 160 180 200 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 5.71 Load(KG) Displacement (mm)
  • 27. Continued… JBBJ-1 BJJB-1 0 10 20 30 40 50 60 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.5 2.75 2.84 Load(KG) Deflection (mm) 0 5 10 15 20 25 30 35 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.5 2.75 3 Load(KG) Deflection (mm) Load-Deflection Curves for the Composites
  • 28. Continued… JBBJ-2 BJJB-2 0 5 10 15 20 25 30 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 2.35 Load(KG) Deflection (mm) 0 5 10 15 20 25 30 Load(KG) Deflection (mm)
  • 30. Deformed Tensile Shape and Von Misses Stress developed in JBBJ-1 using ROM
  • 31. Tensile Behavior of HBCs Sample JBBJ-1 using ROM
  • 32. Deformed Tensile Shape and Von Misses Stress developed in JBBJ-1 using HROM
  • 33. Tensile Behavior of HBCs sample JBBJ-1 using HROM
  • 34. Deformed Flexural Shape and Von Misses Stress developed in JBBJ-1 using ROM
  • 35. Flexural Behavior HBCs sample JBBJ-1 using ROM
  • 36. Deformed Flexural Shape and Von Misses Stress developed in JBBJ-1 using HROM
  • 37. Flexural Behavior of HBCs sample JBBJ-1 using HROM
  • 38. Continued… Tensile Properties Flexural Properties 0 5 10 15 20 25 30 35 JBBJ-1 BJJB-1 JBBJ-2 BJJB-2 TensileStrength(MPa) Composite Samples Experiment al Values ANSYS Values using ROM 0 10 20 30 40 50 60 70 80 90 JBBJ-1 BJJB-1 JBBJ-2 BJJB-2 FlexuralStrength(MPa) Composite Samples Experimental Values ANSYS Values using ROM 3. Comparison Between Experimental and ANSYS APDL Results:
  • 39. Continued… 4. Determination of Percentage Error: It gives the approximation between calculated and known values. Calculated values = ANSYS Results and Known values = Experimental Results.
  • 40. Continued… % Error in Tensile Properties % Error in Flexural Properties
  • 41. CONCLUSIONS i. For the same Vf , the HBCs samples of jute fibers oriented at 900 and banana fibers oriented at 450 and -450 exhibits higher properties in each case compared to HBCs sample of banana fibers oriented at 900and jute fibers oriented at 450 and -450. ii. For the same Vf and similar orientation of jute and banana fibers, HBCs fabricated with resin and hardener ratio of 100:10 exhibits maximum mechanical and physical properties in contrast to the HBCs fabricated with resin and hardener ratio of 100:20. iii. After evaluation of the properties in each case for all the HBCs samples, it has observed that the composite sample JBBJ-1 performed maximum mechanical and physical properties in each case. Therefore, optimal results are obtained with composite sample JBBJ-1. iv. The experimental results for the mechanical properties of HBCs in each case show good agreement with the ANSYS APDL results.
  • 42. REFERENCES 1. Boopalan M., Niranjanaa M., and Umapathy M. J. (2013), “Study on the mechanical properties and thermal properties of jute and banana fiber reinforced epoxy hybrid composites,” Compos. Part B, vol. 51, pp. 54–57. 2. John M. J. and Thomas S. (2008), “Biofibres and biocomposites,” Carbohydr. Polym, vol. 71,pp. 343–364. 3. Essabir H., Bensalah M. O., Rodrigue D., Bouhfid R., Qaiss A. (2016), “Structural , mechanical and thermal properties of bio-based hybrid composites from waste coir residues : Fibers and shell particles,” Mech. Mater., vol. 93, pp. 134–144.
  • 43. Continued… 4. Paul V., Kanny K., and Redhi G. G. (2015), “Mechanical , thermal and morphological properties of a bio-based composite derived from banana plant source,” Compos. PART A, vol. 68, pp. 90–100. 5. Merlini C., Soldi V. and Barra G. M. O. (2011), “In fl uence of fiber surface treatment and length on physico-chemical properties of short random banana fiber-reinforced castor oil polyurethane composites,” Polym. Test., vol. 30, pp. 833–840. 6. Wambua P., Ivens I., and Verpoest I. (2003), “Natural fibers : can they replace glass in fibre reinforced plastics ?,” Composites Science and Technology, vol. 63, pp. 1259–1264.