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FOOD CONTAMINANTS:
ANALYSIS OF TRACE METAL,
PESTICIDES RESIDUES &
VETERINARY DRUG
RESIDUES.
Sakshi Tawde &
Pratik Kharat
(Submitted for Internal
theory exams of MSc.
Analytical Chemistry )
1
Ramnarian Ruia Autonomous College
Presented by
2
INTRODUCTION
Food Contaminants -Refers to the unwanted material present in food products
introduced either in producing & processing or naturally.
3
CHEMICAL CONTAMINATS
4
Need For Contamination Analysis
5
TRACE METAL ANALYSIS
There are 4 major steps involved in the analysis of foods for the metal contents,
(a) Obtaining a representative sample from the bulk received for testing.
(b) Destruction of organic matter.
(c) Separation and concentration of the element of interest
(d) Determination
6
TRACE METAL ANALYSIS
7
TRACE METAL ANALYSIS
(Ref: - Manual
Methods of Analysis
for Adulterants and
Contaminants in
Foods, I.C.M.R 1990
Pg 153)
Determination of Pb
by ICP-MS.
8
ANALYSIS OF PESTICIDE RESIDUES
9
ANALYSIS OF PESTICIDE RESIDUES
QuEChERS SPE
ANALYSIS OF PESTICIDE RESIDUES 10
ANALYSIS OF PESTICIDE RESIDUES 11
ANALYSIS OF PESTICIDE RESIDUES 12
Drug Veterinary drug
13
Authorities
JECFA FDA-CFSAN USDA-FSIS CCRVDF
14
Major Classes of Drugs used in
Food animals
15
Drug ResidueTesting
Targeted tissue test
STOP
FAST
SOS
16
Choloramphenicol
17
18
Detection of NON-PROTIEN
NITROGEN SUBSTANCES IN MILK
19
20
References
• https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8497835/ :
Determination of chloramphenicol in meat by liquid chromatography
and tandem mass spectrometry
• Manual of methods of analysis of Milk & Milk products by FSSAI
(2015)
• Manual of methods of analysis of Pesticides residues in food by
FSSAI (2015)
• https://www.gerhardt.de/en/know-how/analytical-
methods/kjeldahl-method/
• Evaluation of certain veterinary drug residues in food: 36th Report of
JECFA
22

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Food contaminants.pptx