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Analysis procedure for biooil.pptx
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Analysis procedure for biooil.pptx
1.
Analysis Procedure for
the Bio-oil and Non condensable Gas
2.
Average Area Experiments duration
[hours] H2 Flow [l/min] N2 Flow [l/min] hopper N2 [l/h] total N2 [l/min] 220718_zeoliteY_01_001 7/18/2022 11:44:22 AM 0 0,5 1,5 10 1,666666667 220718_zeoliteY_01_002 7/18/2022 12:04:25 PM 0,333333333 0,5 1,5 10 1,666666667 220719_zeoliteY_01_001 7/19/2022 11:37:57 AM 0,666666667 0,5 1,5 10 1,666666667 220719_zeoliteY_01_002 7/19/2022 11:58:00 AM 1 0,5 1,5 10 1,666666667 220719_zeoliteY_01_003 7/19/2022 12:18:03 PM 1,333333333 0,5 1,5 10 1,666666667 220719_zeoliteY_01_004 7/19/2022 12:38:06 PM 1,666666667 0,5 1,5 10 1,666666667 220719_zeoliteY_01_005 7/19/2022 12:58:09 PM 1,333333333 0,5 1,5 10 1,666666667 H2 N2 CH4 CO CO2 Methane Ethane Ethene Propane Propene Butane Pentane Hexane 0 16091,5 0 0 0 3,5 0 0 0 0 21,9 157 96,8 599,2 16489,6 231,9 1175 823,5 1806,5 0,2319 333,2 990,3 231,9 951,3 816,7 474 618 18077,5 0 144,2 264,6 100,5 0,0064 6,2 0 0 10,9 36,3 22,3 583,5 14780,4 263,2 1322,9 893,5 2170,9 0,3062 383 1132,3 304 1003,8 595,3 282,1 629,7 15246,8 302 1132,9 911,2 2340,9 0,2279 446 965,8 260,7 1070,8 901,5 526,1 596,9 15878,4 402,2 1312 1111,3 3108,4 0,2292 621,1 1015,2 305,7 1159,8 1128,4 749,6 612,7 17799,5 75,5 87,3 61,4 615,4 0,0342 82,1 128,3 21,8 192,4 280,8 371,2 Average TCD Area FID Area Hydrogen and Nitrogen data Gas Analysis data Analysis Procedure for the Non condensable Gas
3.
Analysis Procedure for
the Non condensable Gas Species TCD Eq Coef TCD rf K =fi/fn2 g/mol H2 27,25 0,0367 23,97798165 2 N2 653,4 0,0015 1 28 CH4 726 0,0014 0,9 16 CO 890 0,0011 0,734157303 28 CO2 1194 0,0008 0,547236181 44 TCD Coefficient Species FID eq coef FID rf K=fi/Fmet g/mol Methane 1951,85 0,000512 1,00 16 Ethane 3494 0,000286 0,56 30 Ethene 3666 0,000273 0,53 28 Propane 5570 0,00018 0,35 44 Propene 5500 0,000182 0,35 42 Butane 7314 0,000137 0,27 58 i/x-butane 7314 0,000137 0,27 58 Pentane 9130 0,00011 0,21 72,15 Hexane 11032 9,06E-05 0,18 86,18 FID Coefficient H2 N2 CH4 CO CO2 0 1 0 0 0 0,871313 1 0,012657 0,052314 0,027329 0,819715 1 0 0,005856 0,00801 0,946602 1 0,016027 0,06571 0,033081 0,990302 1 0,017827 0,054551 0,032705 0,901379 1 0,022797 0,060662 0,0383 0,825378 1 0,003818 0,003601 0,001888 TCD ri=Xi/Xn2 H2 N2 CH4 CO CO2 C2 C3 C4 C5 C6 0 4,464286 0 0 0 0 0 0 0 0 3,889791 4,464286 0,056505 0,233544074 0,122006 0,005215 0 0 0,005109 0,002471 3,659441 4,464286 0 0,026143757 0,035758 0 0 0 0 0 4,225901 4,464286 0,071547 0,293347191 0,147685 0,006316 0 0 0,003924 0,00155 4,420991 4,464286 0,079583 0,243530847 0,146003 0,007585 0 0 0,00613 0,002981 4,024014 4,464286 0,101772 0,270812185 0,170982 0,010171 0 0 0,007389 0,00409 3,684722 4,464286 0,017043 0,016074873 0,008427 0,001137 0 0 0,001555 0,001713 F mol/h H2 N2 CH4 CO CO2 C2 C3 C4 C5 C6 0 125 0 0 0 0 0 0 0 0 7,779582 125 0,904076 6,539234 5,368253 0,151225 0 0 0,368618 0,212952 7,318881 125 0 0,732025 1,57337 0 0 0 0 0 8,451801 125 1,144759 8,213721 6,498122 0,183176 0 0 0,283111 0,13354 8,841981 125 1,273335 6,818864 6,424132 0,219971 0 0 0,442254 0,2569 8,048027 125 1,628358 7,582741 7,523225 0,294973 0 0 0,533117 0,352515 7,369443 125 0,27268 0,450096 0,3708 0,032981 0 0 0,112212 0,147652 F g/h
4.
Result of NCG
Analysis gas sampling interval [h] 0,333333333 Feed rate [g/h] 30 CH4 CO CO2 C2 C3 C4 C5 C6 duration 1,23 yield [g] 1,7410695 10,11223 9,252634 0,294109 0 0 0,57977 0,367853 total biomass 36,9 yield [g/gbio] 4,72 % 27,40 % 25,07 % 0,80 % 0,00 % 0,00 % 1,57 % 1,00 % total gas yield [g] 22,34766261 total gas yield [g/gbio] 60,56 %
5.
Peak name Retention time (min) Peak
area Area fraction Response factor weight weight fraction Actual weight g/mol Carbon Hydrogen Oxygen Mol C Carbon selectivity Mol O Mol H Weight C Weight O Weight H methanol 3,74 45 0,01211958 1,32 0,0091815 0,022 4,20622 32 1 4 1 0,00068757 0,014 0,00068757 0,002750279 0,008250837 0,011001117 0,002750279 acetaldehyde 4,28 7 0,001885268 2,75 0,000685552 0,00164 0,31406 46 2 6 1 7,14275E-05 0,001 3,57138E-05 0,000214283 0,00085713 0,00057142 0,000214283 acetone 4,77 235 0,063291139 1,89 0,033487375 0,08025 15,3412 60 2 4 2 0,002674933 0,055 0,002674933 0,005349867 0,032099201 0,042798935 0,005349867 DCM 5,49 4 0,001077296 0,99 0,001091419 0,00262 0,5 14 1 2 0 0,000186817 0,004 0 0,000373634 0,002241805 0 0,000373634 acetic acid 6,44 2070 0,557500673 3,79 0,147097803 0,3525 67,3883 44 2 4 1 0,016022734 0,330 0,008011367 0,032045469 0,192272813 0,128181875 0,032045469 ethanol 8 359 0,096687315 1,32 0,073247966 0,17553 33,5563 58 3 6 1 0,009079082 0,187 0,003026361 0,018158165 0,108948989 0,048421773 0,018158165 2-butanone 11,06 72 0,019391328 1,34 0,01447114 0,03468 6,62951 72 4 8 1 0,001926564 0,040 0,000481641 0,003853127 0,023118764 0,007706255 0,003853127 propanoic acid 12,49 84 0,022623216 2,44 0,00927181 0,02222 4,24759 74 3 6 2 0,000900756 0,019 0,000600504 0,001801512 0,010809072 0,009608064 0,001801512 2-butanone, 3- methyl 13,85 9 0,002423916 1,35 0,001795493 0,0043 0,82255 74 3 6 2 0,000174432 0,004 0,000116288 0,000348864 0,002093185 0,001860609 0,000348864 2-propanone, 1-hydroxy 13,88 226 0,060867223 2,44 0,024945583 0,05978 11,4281 86 5 10 1 0,003475508 0,072 0,000695102 0,006951017 0,041706101 0,011121627 0,006951017 1,2-ethanediol 14,15 8 0,002154592 2,64 0,000816133 0,00196 0,37389 62 2 6 2 6,30888E-05 0,001 6,30888E-05 0,000189267 0,000757066 0,001009421 0,000189267 propanoic acid, 2-methyl 15,1 7 0,001885268 1,87 0,001008165 0,00242 0,46186 88 4 8 2 0,000109815 0,002 5,49075E-05 0,00021963 0,001317781 0,000878521 0,00021963 vinyl crotonate 16,06 67 0,018044708 1,53 0,011793927 0,02826 5,40302 112 6 8 2 0,001514066 0,031 0,000504689 0,002018755 0,018168791 0,008075018 0,002018755 pyridine 16,4 0 0 1,00 0 0 0 88 4 8 2 0 0,000 0 0 0 0 0 butanoic acid 16,59 61 0,016428764 1,87 0,008785435 0,02105 4,02478 65 5 5 0 0,001619471 0,033 0 0,001619471 0,019433647 0 0,001619471 acetic acid, acetyloxy 16,6 0 0 1,00 0 0 0 118 4 6 4 0 0,000 0 0 0 0 0 2-propenoic acid, 2-methyl 17,92 316 0,085106383 1,84 0,046253469 0,11084 21,1896 86 4 6 2 0,00515536 0,106 0,00257768 0,00773304 0,061864317 0,041242878 0,00773304 cyclopentanon e 18,1 15 0,00403986 1,31 0,003083863 0,00739 1,41278 84 5 8 1 0,000439885 0,009 8,79769E-05 0,000703816 0,005278616 0,001407631 0,000703816 furfural 20,22 0 0 2,00 0 0 0 82 5 6 1 0 0,000 0 0 0 0 0 2-cyclopenten- 1-one 20,57 21 0,005655804 1,31 0,004317408 0,01035 1,97789 96 5 4 2 0,000538859 0,011 0,000215544 0,000431087 0,006466305 0,003448696 0,000431087 2-cyclopenten- 1-one, 2- methyl 20,79 0 0 1,17 0 0 0 96 6 8 1 0 0,000 0 0 0 0 0 butyrolactone 22,5 0 0 1,79 0 0 0 86 4 6 2 0 0,000 0 0 0 0 0 2-cyclopenten- 1-one,3- methyl 23,9 11 0,002962564 1,17 0,002532106 0,00607 1,16001 94 6 6 1 0,00038731 0,008 6,45516E-05 0,00038731 0,004647717 0,001032826 0,00038731 phenol 24,08 0 0 1,14 0 0 0 96 6 8 1 0 0,000 0 0 0 0 0 1- propanone,1- cyclopropyl 24,4 0 0 1,52 0 0 0 134 9 10 1 0 0,000 0 0 0 0 0 2-cyclopenten- 1-one, 2- hydroxy-3- methyl 25,87 30 0,00807972 1,20 0,0067331 0,01613 3,08456 112 6 8 2 0,000864373 0,018 0,000288124 0,001152498 0,010372481 0,004609992 0,001152498 phenol, 2- methyl 26,37 10 0,00269324 1,09 0,002470862 0,00592 1,13195 108 7 8 1 0,000383774 0,008 5,48249E-05 0,000438599 0,004605292 0,000877199 0,000438599 p-cresol 26,56 8 0,002154592 1,06 0,002032634 0,00487 0,93119 108 7 8 1 0,000315709 0,007 4,51012E-05 0,00036081 0,003788505 0,00072162 0,00036081 phenol, 3,5- dimethyl 28,8 48 0,012927552 1,06 0,012195804 0,02923 5,58713 122 8 10 1 0,001916433 0,040 0,000239554 0,002395542 0,0229972 0,003832867 0,002395542 phenol, 2- ethyl 29,2 0 0 1,06 0 0 0 122 8 10 1 0 0,000 0 0 0 0 0 catechol 30 0 0 1,53 0 0 0 110 6 6 2 0 0,000 0 0 0 0 0 levoglucosan 32,14 0 0 5,12 0 0 0 162 6 10 5 0 0,000 0 0 0 0 0 3713 0,417298546 191,172 Total mol C total Carbon % Total mol O Total mol H Total weight C Total weight O Total weight H 64,04472 0,048507968 1 0,020525521 0,089496039 0,582095617 0,328408344 0,089496039 Aqueous phase of Bio-Oil
6.
Aqueous phase of
Bio-Oil
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