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EMERGING TECHNOLOGIES                                                                                                                                    BOILING ON NANO-STRUCTURES
           BIO-MICRO-FLUIDICS, MEMS,                                                                POOL BOILING ON                                                      POOL BOILING ON                                                                                                                                                     FLOW BOILING USING
          AND NANO-BIO-TECHNOLOGIES                                                                SILICON NANO-FINS                                                  CARBON NANOTUBES (CNT)                                                                                                                                                 TEMP. NANO-SENSOR
                                                                                                         Student: S.R. Sriraman (M.S.)                           Students: V. Sathyamurthi (M.S., Ph.D.) and H.S. Ahn (Ph.D.)                                                                                                                                           Student: M. Sundar (Ph.D.)
                  LAB-ON-CHIP (LOC) FOR WATER
                   QUALITY MONITORING USING
                        PEPTIDE ASSAY &
                     GOLD NANO-PARTICLES
                                              Student: S. Datta (M.S.)
                     • In-situ gold nano-particle synthesis using peptide assay.
                     Sponsor: Air Force Research Lab. (AFRL) through the
                      Anteon Corporation (General Dynamics)                                    • Pool boiling heat flux improved by 120%     • Pool boiling heat flux improved by ~300%                                                                                                                                   • Study surface temperature transients
                     Collaborator: Dr. R. Nayak (AFRL/ML)                                                                                    • CNT synthesized by CVD: 8-16 nm                                                                                                                                              during flow boiling on nano-structures
                                                                                               • Nanofins nano-fabricated by Step and Flash
                                                                                                                                               diameter, ~ 40 nm pitch                                                                                                                                                      using temperature nano-sensors (e.g.,
                           FILLING EXPERIMENTS FOR                                               Imprint Lithography (SFIL) Process: 200 nm
                                                                                                                                                                                                                                                                                                                            thin film thermocouples or “TFT”, and
                                                                                                                                             Sponsor: TEES (Faculty Start-Up)
                         DESIGNING DNA HYBRIDIZATION                                             diameter, 15 – 600 nm height, 800 nm pitch.
                                                                                                                                             Collaborator: Dr. R. Baughman, Nanotech                                                                                                                                        diode sensor array) on the surface.
                                                                                               Sponsor: National Science Foundation (NSF)
                               MICRO-CHAMBERS                                                                                                  Institute, University of Texas at Dallas                                                                                                                                   Sponsor: Office of Naval Research
                                     Students: S. Gauntt (M.S.), N. Singh (M.S.),                                                   Undergraduate Students: Sonia Bendjemil (ESP), R. Deleon (USRG), M. Harlow, D. Haas, J.R. Koss, and R. Williams
                                V. Sathyamurthi (M.S., Ph.D.), and R. Deleon (USRG)
                      • Experimental validation of lumped models.                                                                                                                                                         BOILING CHAOS: FRACTAL ORDER Dc
                      • Viscosity varies with contact angle!                                                                                                                                                                                                      Student: V. Sathyamurthi (M.S., Ph.D.)
                      • Other Projects: Portable Vaccine Pack.
                                                                                                 MULTI-PHASE FLOWS &
                                                                                                                                                                                          Dc2 – bubble plan area                                                                      Dc1: bubble perimeter                                                                                      Plot of Dc2 vs. Dc1
                      • Lab-CD: Portable DNA Analyzer.                                            HEAT TRANSFER LAB                                                                              3
                                                                                                                                                                                               2.95
                                                                                                                                                                                                2.9
                                                                                                                                                                                               2.85
                                                                                                                                                                                                                                                                                2.5

                                                                                                                                                                                                                                                                               2.45

                                                                                                                                                                                                                                                                                2.4
                                                                                                                                                                                                                                                                                                                                                                                     2.4
                                                                                                                                                                                                                                                                                                                                                                                    2.38

                                                                                                                                                                                                                                                                                                                                                                                    2.36
                                                                                                                                                                                                                                                                                                                                                                                    2.34

                      Sponsors: Defense Advanced Project Agency                                                                                                                                                                                                                2.35



                                                                                                            Dr. Debjyoti Banerjee
                                                                                                                                                                                                2.8                                                                                                                                                                                 2.32
                                                                                                                                                                                                                                                                                2.3
                                                                                                                                                                                               2.75                                                                                                                                                                                  2.3




                                                                                                                                                                                        D c2




                                                                                                                                                                                                                                                                                                                                                                             D c1
                                                                                                                                                                                                                                                                        D c1
                                                                                                                                                                                                                                                                               2.25

                       (DARPA/MF3) and University of California (Irvine)                                                                                                                        2.7
                                                                                                                                                                                               2.65                                                                             2.2
                                                                                                                                                                                                                                                                                                                                                                                    2.28
                                                                                                                                                                                                                                                                                                                                                                                    2.26




                                                                                                            dbanerjee@tamu.edu
                                                                                                                                                                                                2.6                                                                            2.15                                                                                                 2.24
                                                                                                                                                                                               2.55                                                                             2.1                                                                                                 2.22
                                                                                                                                                                                                2.5                                                                            2.05                                                                                                  2.2



                         PORTABLE NANO-CALORIMETER
                                                                                                                                                                                               2.45
                                                                                                                                                                                                                                                                                 2                                                                                                  2.18
                                                                                                                                                                                                      80   82   84   86     88     90     92      94   96    98   100
                                                                                                                                                                                                                                                                                      75   77   79   81    83     85    87    89        91      93   95   97   99



                                                                                                            Phone: 979-845-4500
                                                                                                                                                                                                                                                                                                                                                                                           2.7     2.75     2.8       2.85    2.9   2.95   3
                                                                                                                                                                                                                          Wall Temperature (°C)
                                                                                                                                                                                                                                                                                                                Wall Temperature (°C)                                                                                 D c2


                          FOR EXPLOSIVES DECTECTION                                                                                                                                                   • The results show that pool boiling heat flux depends on the fractal
                          Students: I.C. Nelson (M.S.) and J.R. Koss (Undergraduate)           Research Sponsors: NSF, DARPA-MTO, DARPA-MF3,
                                                                                                ONR, TSGC, NASA (Ureti), AFRL/AFOSR - Anteon                                                            order for bubble contact perimeter (Dc1) while wall superheat depends
                       • Detection of mustard gas, gasoline, alcohol, acetone.                  Corp. (General Dynamics), Nano-MEMS Research                                                            on fractal order for the bubble contact area (Dc2) on the heater.
                       Sponsor: TEES (Faculty Start-Up) and Mary Kay                            LLC/ NSF (SBIR Phase I), and Lynntech Inc./ ARO                                                       Sponsor: TEES (Faculty Start-Up)
                        O’Connor Process Safety Center                                          (SBIR Phase II)                                                                                       Collaborator: Dr. J. Kim, University of Maryland

DPN: DIP PEN NANO-LITHOGRAPHY                                                                                         FOUNTAIN PENS (FPN) &                                                                                                                                    NANOFLUIDS
  CHIRALITY CONTROL OF                                 ROOM TEMPERATURE                                                   CENTIWELLS                                                                                                                        Students: I.C. Nelson (M.S.) and D. Huitink (M.S.)
                                                    SYNTHESIS OF CNT ON MEMS                                              Students: J.A. Rivas-Cardona (M.S.) and
   SINGLE WALLED CNT                                                                                                           V. Sathyamurthi (M.S., Ph.D.)
                                                                                                                                                                                                                                                                                                          Reservoir




           Student: D. Huitink (M.S.)                             Student: R. Gargate (M.S.)                                     PEG                                                                                                                                                                                                          Finned Heater
                                                                                                                                                                                                                                                                                                                                                                      Liquid-Liquid Compact Heat
                                                                                                                                                                                                                                                                                                                                                                               Exchanger
                                                                                                                                 Microbeads   Micro-well Array

                                                                                                                                                                                                                                                                                                                                             Hot Loop (Oil)                                               Cool Loop (Water)




                                                                                                                      Peltier Cooler
                   Tip-to-Tip                                                                                 Micro-well Array
                                                                                                                                                                                                                                                                                                                         Flowmeter                                  Magnetic Gear Pump



                   DPN
                                  SWCNT bundle         Coating with catalyst solution   CNT on AFM Tip
• Chirality (crystal structure) of single walled • CNT synthesis at room temperature
  carbon nanotube (SWCNT) can be controlled (without requiring any furnace or process                                                                                                             • Heat flux improved by 8% - 30% for fin coolers and compact heat
  using DPN and Chemical Vapor Deposition                                                                                                                                                           exchangers using Poly Alpha Olefin (PAO) base fluid (that is used for
                                                   gasses) using micro-heaters.                                                                                                                     cooling aircraft components), seeded with two types of nanoparticles:
  (CVD).                                         • CNT characterized using SEM and
• Raman spectroscopy was found to correlate                                                                   • Integrate microfluidics with DPN.                                                     (A) Exfoliated Graphite (EG-PAO)
                                                   Raman Spectroscopy.                                        • Maximize throughput to 96 -1000 inks.                                                 (B) Carbon Nanotubes (CNT-PAO)
  with TEM/ SEM and XPS.                         • Hand-held/ portable instrument for “on-
Sponsor: Defense Advanced Project Agency                                                                      • Obtained fractal nano-patterns by DPN                                             Sponsor: Air Force Research Lab. (AFRL), Office of Scientific Research
                                                   demand” synthesis of SWCNT.                                  of Poly-Ethylene-Glycol (PEG).                                                    Collaborators: Dr. R. Ponnappan (AOARD), Dr. K. Yerkes (AFRL/PR),
 (DARPA-MTO)
                                                        Sponsor: Defense Advanced Project Agency                                                                                                   Dr. S. Ganguli (AFRL/NRC Fellow), Dr. A. Roy (AFRL/ML), and
Collaborators: Dr. S. Sinha (University of New                                                                Sponsor: Texas Space Grants Consortium
                                                         (DARPA-MTO)                                                                                                                               Dr. K. Lafdi (UDRI)
 Haven) and Dr. S. Ganguli (AFRL/ NRC)                                                                         (TSGC) New Investigator Program (NIP)

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D Banerjee Tamu Poster 2007 V4

  • 1. EMERGING TECHNOLOGIES BOILING ON NANO-STRUCTURES BIO-MICRO-FLUIDICS, MEMS, POOL BOILING ON POOL BOILING ON FLOW BOILING USING AND NANO-BIO-TECHNOLOGIES SILICON NANO-FINS CARBON NANOTUBES (CNT) TEMP. NANO-SENSOR Student: S.R. Sriraman (M.S.) Students: V. Sathyamurthi (M.S., Ph.D.) and H.S. Ahn (Ph.D.) Student: M. Sundar (Ph.D.) LAB-ON-CHIP (LOC) FOR WATER QUALITY MONITORING USING PEPTIDE ASSAY & GOLD NANO-PARTICLES Student: S. Datta (M.S.) • In-situ gold nano-particle synthesis using peptide assay. Sponsor: Air Force Research Lab. (AFRL) through the Anteon Corporation (General Dynamics) • Pool boiling heat flux improved by 120% • Pool boiling heat flux improved by ~300% • Study surface temperature transients Collaborator: Dr. R. Nayak (AFRL/ML) • CNT synthesized by CVD: 8-16 nm during flow boiling on nano-structures • Nanofins nano-fabricated by Step and Flash diameter, ~ 40 nm pitch using temperature nano-sensors (e.g., FILLING EXPERIMENTS FOR Imprint Lithography (SFIL) Process: 200 nm thin film thermocouples or “TFT”, and Sponsor: TEES (Faculty Start-Up) DESIGNING DNA HYBRIDIZATION diameter, 15 – 600 nm height, 800 nm pitch. Collaborator: Dr. R. Baughman, Nanotech diode sensor array) on the surface. Sponsor: National Science Foundation (NSF) MICRO-CHAMBERS Institute, University of Texas at Dallas Sponsor: Office of Naval Research Students: S. Gauntt (M.S.), N. Singh (M.S.), Undergraduate Students: Sonia Bendjemil (ESP), R. Deleon (USRG), M. Harlow, D. Haas, J.R. Koss, and R. Williams V. Sathyamurthi (M.S., Ph.D.), and R. Deleon (USRG) • Experimental validation of lumped models. BOILING CHAOS: FRACTAL ORDER Dc • Viscosity varies with contact angle! Student: V. Sathyamurthi (M.S., Ph.D.) • Other Projects: Portable Vaccine Pack. MULTI-PHASE FLOWS & Dc2 – bubble plan area Dc1: bubble perimeter Plot of Dc2 vs. Dc1 • Lab-CD: Portable DNA Analyzer. HEAT TRANSFER LAB 3 2.95 2.9 2.85 2.5 2.45 2.4 2.4 2.38 2.36 2.34 Sponsors: Defense Advanced Project Agency 2.35 Dr. Debjyoti Banerjee 2.8 2.32 2.3 2.75 2.3 D c2 D c1 D c1 2.25 (DARPA/MF3) and University of California (Irvine) 2.7 2.65 2.2 2.28 2.26 dbanerjee@tamu.edu 2.6 2.15 2.24 2.55 2.1 2.22 2.5 2.05 2.2 PORTABLE NANO-CALORIMETER 2.45 2 2.18 80 82 84 86 88 90 92 94 96 98 100 75 77 79 81 83 85 87 89 91 93 95 97 99 Phone: 979-845-4500 2.7 2.75 2.8 2.85 2.9 2.95 3 Wall Temperature (°C) Wall Temperature (°C) D c2 FOR EXPLOSIVES DECTECTION • The results show that pool boiling heat flux depends on the fractal Students: I.C. Nelson (M.S.) and J.R. Koss (Undergraduate) Research Sponsors: NSF, DARPA-MTO, DARPA-MF3, ONR, TSGC, NASA (Ureti), AFRL/AFOSR - Anteon order for bubble contact perimeter (Dc1) while wall superheat depends • Detection of mustard gas, gasoline, alcohol, acetone. Corp. (General Dynamics), Nano-MEMS Research on fractal order for the bubble contact area (Dc2) on the heater. Sponsor: TEES (Faculty Start-Up) and Mary Kay LLC/ NSF (SBIR Phase I), and Lynntech Inc./ ARO Sponsor: TEES (Faculty Start-Up) O’Connor Process Safety Center (SBIR Phase II) Collaborator: Dr. J. Kim, University of Maryland DPN: DIP PEN NANO-LITHOGRAPHY FOUNTAIN PENS (FPN) & NANOFLUIDS CHIRALITY CONTROL OF ROOM TEMPERATURE CENTIWELLS Students: I.C. Nelson (M.S.) and D. Huitink (M.S.) SYNTHESIS OF CNT ON MEMS Students: J.A. Rivas-Cardona (M.S.) and SINGLE WALLED CNT V. Sathyamurthi (M.S., Ph.D.) Reservoir Student: D. Huitink (M.S.) Student: R. Gargate (M.S.) PEG Finned Heater Liquid-Liquid Compact Heat Exchanger Microbeads Micro-well Array Hot Loop (Oil) Cool Loop (Water) Peltier Cooler Tip-to-Tip Micro-well Array Flowmeter Magnetic Gear Pump DPN SWCNT bundle Coating with catalyst solution CNT on AFM Tip • Chirality (crystal structure) of single walled • CNT synthesis at room temperature carbon nanotube (SWCNT) can be controlled (without requiring any furnace or process • Heat flux improved by 8% - 30% for fin coolers and compact heat using DPN and Chemical Vapor Deposition exchangers using Poly Alpha Olefin (PAO) base fluid (that is used for gasses) using micro-heaters. cooling aircraft components), seeded with two types of nanoparticles: (CVD). • CNT characterized using SEM and • Raman spectroscopy was found to correlate • Integrate microfluidics with DPN. (A) Exfoliated Graphite (EG-PAO) Raman Spectroscopy. • Maximize throughput to 96 -1000 inks. (B) Carbon Nanotubes (CNT-PAO) with TEM/ SEM and XPS. • Hand-held/ portable instrument for “on- Sponsor: Defense Advanced Project Agency • Obtained fractal nano-patterns by DPN Sponsor: Air Force Research Lab. (AFRL), Office of Scientific Research demand” synthesis of SWCNT. of Poly-Ethylene-Glycol (PEG). Collaborators: Dr. R. Ponnappan (AOARD), Dr. K. Yerkes (AFRL/PR), (DARPA-MTO) Sponsor: Defense Advanced Project Agency Dr. S. Ganguli (AFRL/NRC Fellow), Dr. A. Roy (AFRL/ML), and Collaborators: Dr. S. Sinha (University of New Sponsor: Texas Space Grants Consortium (DARPA-MTO) Dr. K. Lafdi (UDRI) Haven) and Dr. S. Ganguli (AFRL/ NRC) (TSGC) New Investigator Program (NIP)