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Improved Mechanical Properties of Aluminium Powder-Carbon Nanotubes and
Epoxy Nanocomposites to Fabricate Blades for Wind Turbines and Different
Components of Machines and Equipment
Jorge Iván Cifuentes Castillo
School of Mechanical Engineering , University of San Carlos of Guatemala, Guatemala.
jicifuentes@ing.usac.edu.gt
kavic.engineering@gmail.com
Introduction
Blades for wind turbines are critical parts in the manufacture, design and operation of wind turbine
power plants, they have to support extreme weather conditions sometimes at the same day like snow,
rain, 50 degrees below 0 and +45 degrees temperatures without suffer any deformation, bending,
crystallization, fracture, wear, support hurricanes and strength winds, have to be light weight or low
density, not to decrease the structural behavior during the rotation and transmission of mechanical
power . The main manufactures of wind turbines have specific research centers to improve the
materials, most of the materials are special composites and affect the design and operation of wind
turbines.
In this study we have fabricated different combinations of aluminium powder, epoxy and carbon nano
tubes to have a novel material with better structural properties, especially for small and medium size
wind turbines in the Rank of 0.100 to 100 Kilowatts, for functionalization we modified the surface of
aluminium powder and nanotubes with 3 aminopropyltriethoxysilane to have a bonding and adhesion
with the epoxy and aluminium-nanotubes in the particulate Nano composite tensile, flexion, hardness
test were performed in Universal testing machine and Vickers hardener tester, stress-strain curves of
different combinations of particles and materials in the Nano composites and also compared with the
standard materials utilized to fabricate the blades like, Nylon 6, carbon fiber, fiber glass are showed
after the results of the different tests. Toughness, ductility, bending were studied to analyze which
materials have better performance in some sizes and powers of wind turbines. Wind turbines blades
were fabricated also to have a real test of the behavior of the materials on site. Cifuentes et al (1)
studied and fabricated aluminium powder epoxy composites with silane surface modified aluminium
powder to improve the mechanical properties, Rhee, Kathi, Lee et al (2) functionalized carbón
nanotubes with 3 aminopropyltriethoxysilane, TPI industries et al (3) show the composites, materials
and different steps to design, fabricate and tests for the blades of medium and big size wind turbines,
up to 1 MW.
Fabrication and Analysis of Nano Composite
Before fabricate the Nano composites the aluminium powder and carbon nanotubes were
functionalized by modifying of the surface with 3 aminopropyltriethoxysilane to have bonding and
adhesion among the particulate materials in Nano composites with different percentages per weight
0.2, 0.5, 1, 1.2, 1.5, 2 % of nanotubes and 2, 5, 7, 8, 10 % of aluminium powder were fabricated by
cast molding method. Tensile and flexion specimens were CNC machined, then tensile, flexion test
were performed, stress-strain curves and toughness, stiffness calculation to compare and analyze the
mechanical properties of the different Nano composites were studied. Fig. 1 show the composites and
Nano composites fabricated, Fig. 2 show the specimens of the different fabricated materials. Fig 3
show the fracture mechanics mode I specimens before the tests.
Tests Performed
Tensile, flexion and bending tests were realized in the Universal Testing Machine, Rockwell hardness
test were realized in different points of the specimens and composites. Fracture mechanics mode 1
tests were performed in the Universal testing machine. Scratch, sand paper and grinding tests were
realized to compare the roughness, surface hardness and consistence of the different materials
fabricated.
Characterization
Samples were observed in the Metallurgical microscope on the fracture surface after the tests, SEM
analysis was performed to see the dispersion of the aluminum powder, carbon Nano tubes and the
bonding among the materials with the epoxy matrix., AFM was performed to analyze the dispersion
and adhesion in the molecular and atomic scale.
Feynman, R. (1960). “There's Plenty of Room at the Bottom”. annual meeting of the West
Coast section of the American Physical Society (págs. 22-36). California: Engineering
and Science,.
Halicioglu, F. H. (2009). The potential benefits of nanotechnology for innovative solutions
in the construction sector. Nanotechnology in Construction 3, 209-214.
Jia, G. W. (2005). Cytotoxicity of Carbon Nanomaterials:  Single-Wall Nanotube, Multi-
Wall Nanotube, and Fullerene. Environ. Sci. Technol., 39(5), 1378–1383.
doi:10.1021/es048729l
H.J. Kim, Dong-Ho Jung, I.H. Jung, J.I. Cifuentes, K.Y. Rhee, D. Hui. Enhancement of
mechanical properties of aluminium/epoxy composites with silane functionalization of
aluminium powder
PII: S1359-8368(11)00552-X DOI: 10.1016/j.compositesb.2011.12.010
Salvetat, J. P. (1999). Mechanical properties of carbon nanotubes. Applied Physics A, 69(3),
255-260. doi:10.1007/s003399900114
Seoktae Kang, M. P. (2007). Single-Walled Carbon Nanotubes Exhibit Strong Antimicrobial
Activity. Langmuir, 23(17), 8670–8673. doi:10.1021/la701067r
Sobolev, K. &. (2005). How nanotechnology can change the concrete world. American
Ceramic Society Bulletin, 84(10), 14.
Soler Illia, G. (2009). Nanotecnología: el desafio del siglo XXI. Eudeba.
https://www.researchgate.net/profile/Jorge_Cifuentes4/publication/275833340_Improved_
Mechanical_Properties_of_Aluminium_Powder-
Carbon_Nanotubes_and_Epoxy_Nanocomposites_to_Fabricate_Blades_for_Wind_Turbine
s_and_Different_Components_of_Machines_and_Equipment/
links/554806ed0cf26a7bf4da9c53.pdf?origin=publication_detail
DOI:10.13140/RG.2.1.4529.8081
Improved mechanical properties of  aluminium-nanotubes-epoxy  nanocomposites blades.

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Improved mechanical properties of aluminium-nanotubes-epoxy nanocomposites blades.

  • 1. Improved Mechanical Properties of Aluminium Powder-Carbon Nanotubes and Epoxy Nanocomposites to Fabricate Blades for Wind Turbines and Different Components of Machines and Equipment Jorge Iván Cifuentes Castillo School of Mechanical Engineering , University of San Carlos of Guatemala, Guatemala. jicifuentes@ing.usac.edu.gt kavic.engineering@gmail.com Introduction Blades for wind turbines are critical parts in the manufacture, design and operation of wind turbine power plants, they have to support extreme weather conditions sometimes at the same day like snow, rain, 50 degrees below 0 and +45 degrees temperatures without suffer any deformation, bending, crystallization, fracture, wear, support hurricanes and strength winds, have to be light weight or low density, not to decrease the structural behavior during the rotation and transmission of mechanical power . The main manufactures of wind turbines have specific research centers to improve the materials, most of the materials are special composites and affect the design and operation of wind turbines. In this study we have fabricated different combinations of aluminium powder, epoxy and carbon nano tubes to have a novel material with better structural properties, especially for small and medium size wind turbines in the Rank of 0.100 to 100 Kilowatts, for functionalization we modified the surface of aluminium powder and nanotubes with 3 aminopropyltriethoxysilane to have a bonding and adhesion with the epoxy and aluminium-nanotubes in the particulate Nano composite tensile, flexion, hardness test were performed in Universal testing machine and Vickers hardener tester, stress-strain curves of different combinations of particles and materials in the Nano composites and also compared with the standard materials utilized to fabricate the blades like, Nylon 6, carbon fiber, fiber glass are showed after the results of the different tests. Toughness, ductility, bending were studied to analyze which materials have better performance in some sizes and powers of wind turbines. Wind turbines blades were fabricated also to have a real test of the behavior of the materials on site. Cifuentes et al (1) studied and fabricated aluminium powder epoxy composites with silane surface modified aluminium powder to improve the mechanical properties, Rhee, Kathi, Lee et al (2) functionalized carbón nanotubes with 3 aminopropyltriethoxysilane, TPI industries et al (3) show the composites, materials and different steps to design, fabricate and tests for the blades of medium and big size wind turbines, up to 1 MW. Fabrication and Analysis of Nano Composite Before fabricate the Nano composites the aluminium powder and carbon nanotubes were functionalized by modifying of the surface with 3 aminopropyltriethoxysilane to have bonding and adhesion among the particulate materials in Nano composites with different percentages per weight 0.2, 0.5, 1, 1.2, 1.5, 2 % of nanotubes and 2, 5, 7, 8, 10 % of aluminium powder were fabricated by cast molding method. Tensile and flexion specimens were CNC machined, then tensile, flexion test were performed, stress-strain curves and toughness, stiffness calculation to compare and analyze the mechanical properties of the different Nano composites were studied. Fig. 1 show the composites and Nano composites fabricated, Fig. 2 show the specimens of the different fabricated materials. Fig 3 show the fracture mechanics mode I specimens before the tests.
  • 2. Tests Performed Tensile, flexion and bending tests were realized in the Universal Testing Machine, Rockwell hardness test were realized in different points of the specimens and composites. Fracture mechanics mode 1 tests were performed in the Universal testing machine. Scratch, sand paper and grinding tests were realized to compare the roughness, surface hardness and consistence of the different materials fabricated. Characterization Samples were observed in the Metallurgical microscope on the fracture surface after the tests, SEM analysis was performed to see the dispersion of the aluminum powder, carbon Nano tubes and the bonding among the materials with the epoxy matrix., AFM was performed to analyze the dispersion and adhesion in the molecular and atomic scale.
  • 3. Feynman, R. (1960). “There's Plenty of Room at the Bottom”. annual meeting of the West Coast section of the American Physical Society (págs. 22-36). California: Engineering and Science,. Halicioglu, F. H. (2009). The potential benefits of nanotechnology for innovative solutions in the construction sector. Nanotechnology in Construction 3, 209-214. Jia, G. W. (2005). Cytotoxicity of Carbon Nanomaterials:  Single-Wall Nanotube, Multi- Wall Nanotube, and Fullerene. Environ. Sci. Technol., 39(5), 1378–1383. doi:10.1021/es048729l H.J. Kim, Dong-Ho Jung, I.H. Jung, J.I. Cifuentes, K.Y. Rhee, D. Hui. Enhancement of mechanical properties of aluminium/epoxy composites with silane functionalization of aluminium powder PII: S1359-8368(11)00552-X DOI: 10.1016/j.compositesb.2011.12.010 Salvetat, J. P. (1999). Mechanical properties of carbon nanotubes. Applied Physics A, 69(3), 255-260. doi:10.1007/s003399900114 Seoktae Kang, M. P. (2007). Single-Walled Carbon Nanotubes Exhibit Strong Antimicrobial Activity. Langmuir, 23(17), 8670–8673. doi:10.1021/la701067r Sobolev, K. &. (2005). How nanotechnology can change the concrete world. American Ceramic Society Bulletin, 84(10), 14. Soler Illia, G. (2009). Nanotecnología: el desafio del siglo XXI. Eudeba. https://www.researchgate.net/profile/Jorge_Cifuentes4/publication/275833340_Improved_ Mechanical_Properties_of_Aluminium_Powder- Carbon_Nanotubes_and_Epoxy_Nanocomposites_to_Fabricate_Blades_for_Wind_Turbine s_and_Different_Components_of_Machines_and_Equipment/ links/554806ed0cf26a7bf4da9c53.pdf?origin=publication_detail DOI:10.13140/RG.2.1.4529.8081