This document provides an agenda for a workshop on scientific instrument design featuring Thermo Scientific products. The workshop will cover topics including mass spectrometry, gas chromatography, sample preparation automation, and applications. Attendees can learn about new technologies, simplify methods, and explore solutions for their research and analytical needs. An afternoon session will include presentations on various applications and allow for discussion.
Key Learning Objectives:
• Identify emerging triple quadrupole Gas Chromatography-Mass Spectrometry/Mass Spectrometry (GC-MS/MS) technology designed to address increasing regulatory demands and requirements
• Explore potential time savings in sample prep, method development/transition, and data analysis
• Demonstrate how to optimize the GC-MS/MS workflow from sample prep to sample analysis to automated data analysis
Overview:
Regulatory lab requirements continue to drive detection limits lower with an ever increasing list of compounds to analyze. These requirements also demand greater precision at these lower limits. Triple quadrupole GC-MS/MS is a viable option for enhanced analysis and increased productivity with an emphasis on simplicity. We discuss emerging trends and technologies designed to ensure that laboratories are well-equipped to address these increased demands with minimal investment in training and method development. Find out how you can adopt triple quadrupole GC-MS/MS technology in your laboratory using existing methods and source parameters in most instances while requiring less sample prep and enjoying the benefits of automated data analysis for increased simplicity and productivity.
For more information: www.thermoscientific.com/tsq8000
Fully Automated High Throughput Ion Channel Screeningstmalcolm
Process Analysis & Automation were commissioned by Biofocus Ltd. To design and build an automated multi-atomic absorption spectrometer system. Using four Thermo Electron SOLAAR AA spectrometers (with associated Gilson autosamplers), a Hamilton Microlab SWAP robot and a Kendro stacker, a fully automated and reliable workcell was produced. OVERLORD dynamic scheduler (Overlord2) was used control the workcell, with NetLORD used to control the four AA control PCs. We believe that this is the only fully commercially available automated AA system.
Cooper Environmental’s Xact® 625i is designed for high time resolution multi-metals monitoring of ambient air, with detection limits that rival those of laboratory analysis. The Xact® 625i comes standard with a solid-state meteorological sensor and Cooper Environmental’s proprietary ADAPT analysis package, making the instrument one of the most powerful air pollution source detection offerings in the industry. ask info here: https://etserv.be/product/cooper-environmental-xact-625i/
Application of Aqsens Technology: Case studies presented at SPE Oilfield Chem...Aqsens Oy
Aqsens novel method for testing polymeric scale inhibitor was presented with two case studies at SPE International Symposium on Oilfield Chemistry 13th-15th April 2015 in Texas.
Polymeric scale inhibitors can be difficult to detect at MED levels even with sophisticated analytical procedures. The necessary equipment is located in remote laboratories causing delays in obtaining results. It can take weeks to know the effectiveness of the scale control program.
Novel Aqsens technology is based on time-resolved-fluorescence method. It opens the possibility to control scale program efficiency infield with portable field lab unit. The results are ready for use in 10-15 minutes depending on the concentration.
The case studies presented at SPE symposium tested how well Aqsens technology performs compared to current testing possibilities such as HPLC. Aqsens effectiveness was demonstrated on more than 90 produced water samples collected from offshore and onshore wells.
See the full case studies on onshore mature heavy oil field and North Sea fields from attached SPE presentation.
Key Learning Objectives:
• Identify emerging triple quadrupole Gas Chromatography-Mass Spectrometry/Mass Spectrometry (GC-MS/MS) technology designed to address increasing regulatory demands and requirements
• Explore potential time savings in sample prep, method development/transition, and data analysis
• Demonstrate how to optimize the GC-MS/MS workflow from sample prep to sample analysis to automated data analysis
Overview:
Regulatory lab requirements continue to drive detection limits lower with an ever increasing list of compounds to analyze. These requirements also demand greater precision at these lower limits. Triple quadrupole GC-MS/MS is a viable option for enhanced analysis and increased productivity with an emphasis on simplicity. We discuss emerging trends and technologies designed to ensure that laboratories are well-equipped to address these increased demands with minimal investment in training and method development. Find out how you can adopt triple quadrupole GC-MS/MS technology in your laboratory using existing methods and source parameters in most instances while requiring less sample prep and enjoying the benefits of automated data analysis for increased simplicity and productivity.
For more information: www.thermoscientific.com/tsq8000
Fully Automated High Throughput Ion Channel Screeningstmalcolm
Process Analysis & Automation were commissioned by Biofocus Ltd. To design and build an automated multi-atomic absorption spectrometer system. Using four Thermo Electron SOLAAR AA spectrometers (with associated Gilson autosamplers), a Hamilton Microlab SWAP robot and a Kendro stacker, a fully automated and reliable workcell was produced. OVERLORD dynamic scheduler (Overlord2) was used control the workcell, with NetLORD used to control the four AA control PCs. We believe that this is the only fully commercially available automated AA system.
Cooper Environmental’s Xact® 625i is designed for high time resolution multi-metals monitoring of ambient air, with detection limits that rival those of laboratory analysis. The Xact® 625i comes standard with a solid-state meteorological sensor and Cooper Environmental’s proprietary ADAPT analysis package, making the instrument one of the most powerful air pollution source detection offerings in the industry. ask info here: https://etserv.be/product/cooper-environmental-xact-625i/
Application of Aqsens Technology: Case studies presented at SPE Oilfield Chem...Aqsens Oy
Aqsens novel method for testing polymeric scale inhibitor was presented with two case studies at SPE International Symposium on Oilfield Chemistry 13th-15th April 2015 in Texas.
Polymeric scale inhibitors can be difficult to detect at MED levels even with sophisticated analytical procedures. The necessary equipment is located in remote laboratories causing delays in obtaining results. It can take weeks to know the effectiveness of the scale control program.
Novel Aqsens technology is based on time-resolved-fluorescence method. It opens the possibility to control scale program efficiency infield with portable field lab unit. The results are ready for use in 10-15 minutes depending on the concentration.
The case studies presented at SPE symposium tested how well Aqsens technology performs compared to current testing possibilities such as HPLC. Aqsens effectiveness was demonstrated on more than 90 produced water samples collected from offshore and onshore wells.
See the full case studies on onshore mature heavy oil field and North Sea fields from attached SPE presentation.
Process monitoring – feedback for water treatment may improve the efficiency of the treatment process – use fewer chemicals to achieve require effluent emission limits
Measurement of Se, As for compliance with Steam Electric Generating Effluent Guidelines
Monitoring of treatment of wastewater by biological based treatment systems
Measurement of Corrosion Products (e.g. Fe, Ni, Cr and Mn) to improve operating efficiency
Measurement of Elements in Nuclear Power Plant Applications (e.g. Pb, Cu, Fe)
Reduce laboratory analysis costs
gSAFT: advanced physical properties for carbon
capture and storage system modelling - Presentation by Javier Rodriguez at the Effects of Impurities on CO2 Properties session at the UKCCSRC Cardiff Biannual Meeting 10-11 September 2014
PA DEP Proposal to Study Radiation Levels Associated with Shale DrillingMarcellus Drilling News
A proposal submitted to and accepted by the PA Dept. of Environmental Protection from Perma-Fix Environmental Services to conduct a 12-14 month in-depth study of naturally occurring radioactivity levels in drilling wastewater, drill cuttings, and the equipment used to transport, store and dispose of drilling wastes.
techniques for detecting nanoparticles in wastewaterAlekhya Golla
techniques for seperating and analysing the metal containing nanoparticles in wastewater. these techniques are helpful in recycling process of industrial effluents containing nanowastes.
IQ Academy Lunch & Learn Webinar | Cost Effective Water Quality Monitoring wi...IQ_UK
Lots of water quality monitoring is undertaken by the quarrying industry as part of demonstrating environmental permit compliance to the Regulator as well as day to day operational control. Cost is a very important driver in monitoring design and implementation but must not be at the expense of quality and effectiveness. This webinar will discuss how to maximise the effectiveness of water quality monitoring whilst also minimising cost.
Delivered by Dr Craig Speed, an Associate Director and Hydrochemist in Wardell Armstrong’s Water team. Craig has over 13 years of water consultancy experience and 4 years’ experience working for the Environment Agency. His expertise includes design, management and review of water quality monitoring (both groundwater and surface water), hydrochemical interpretation, providing lectures on water quality monitoring at Birmingham University, knowledge of UK water legislation (including environmental permits and abstraction licensing) and detailed knowledge of the Water Framework Directive (WFD) including WFD Compliance Assessments.
His recent project experience includes historic metal mine impact assessments, a quarry lake hydrochemistry project, a quarry conceptual model review, hydrogeology lead in major infrastructure projects, key expert in groundwater monitoring for a project in Turkey and conducting an investigation and adjudication following lime stabilisation impacts on water quality for an electrical infrastructure company.
This presentation on Process Analysis using 3D plots was given at Emerson Exchange, 2010. Details are provided on a field trail in which the DeltaV historian was modified to support array parameters and a web enabled interfaces was used to provide a 3D plot of array data. Information is provided on how this was used to look at absorber column and stripper column temperature profiles.
Today’s laboratories want more from their liquid chromatography system: Higher performance. Better reliability. More consistent and comprehensive analytical workflows. And most of all, more predictable and reproducible results. At the same time, you want
Process monitoring – feedback for water treatment may improve the efficiency of the treatment process – use fewer chemicals to achieve require effluent emission limits
Measurement of Se, As for compliance with Steam Electric Generating Effluent Guidelines
Monitoring of treatment of wastewater by biological based treatment systems
Measurement of Corrosion Products (e.g. Fe, Ni, Cr and Mn) to improve operating efficiency
Measurement of Elements in Nuclear Power Plant Applications (e.g. Pb, Cu, Fe)
Reduce laboratory analysis costs
gSAFT: advanced physical properties for carbon
capture and storage system modelling - Presentation by Javier Rodriguez at the Effects of Impurities on CO2 Properties session at the UKCCSRC Cardiff Biannual Meeting 10-11 September 2014
PA DEP Proposal to Study Radiation Levels Associated with Shale DrillingMarcellus Drilling News
A proposal submitted to and accepted by the PA Dept. of Environmental Protection from Perma-Fix Environmental Services to conduct a 12-14 month in-depth study of naturally occurring radioactivity levels in drilling wastewater, drill cuttings, and the equipment used to transport, store and dispose of drilling wastes.
techniques for detecting nanoparticles in wastewaterAlekhya Golla
techniques for seperating and analysing the metal containing nanoparticles in wastewater. these techniques are helpful in recycling process of industrial effluents containing nanowastes.
IQ Academy Lunch & Learn Webinar | Cost Effective Water Quality Monitoring wi...IQ_UK
Lots of water quality monitoring is undertaken by the quarrying industry as part of demonstrating environmental permit compliance to the Regulator as well as day to day operational control. Cost is a very important driver in monitoring design and implementation but must not be at the expense of quality and effectiveness. This webinar will discuss how to maximise the effectiveness of water quality monitoring whilst also minimising cost.
Delivered by Dr Craig Speed, an Associate Director and Hydrochemist in Wardell Armstrong’s Water team. Craig has over 13 years of water consultancy experience and 4 years’ experience working for the Environment Agency. His expertise includes design, management and review of water quality monitoring (both groundwater and surface water), hydrochemical interpretation, providing lectures on water quality monitoring at Birmingham University, knowledge of UK water legislation (including environmental permits and abstraction licensing) and detailed knowledge of the Water Framework Directive (WFD) including WFD Compliance Assessments.
His recent project experience includes historic metal mine impact assessments, a quarry lake hydrochemistry project, a quarry conceptual model review, hydrogeology lead in major infrastructure projects, key expert in groundwater monitoring for a project in Turkey and conducting an investigation and adjudication following lime stabilisation impacts on water quality for an electrical infrastructure company.
This presentation on Process Analysis using 3D plots was given at Emerson Exchange, 2010. Details are provided on a field trail in which the DeltaV historian was modified to support array parameters and a web enabled interfaces was used to provide a 3D plot of array data. Information is provided on how this was used to look at absorber column and stripper column temperature profiles.
Today’s laboratories want more from their liquid chromatography system: Higher performance. Better reliability. More consistent and comprehensive analytical workflows. And most of all, more predictable and reproducible results. At the same time, you want
This webinar will provide pesticides residue analysts with valuable information on the development and optimization of chromatographic separations and mass spectrometry methods for the analysis of pesticide residues in food. The expert speakers will share their knowledge in understanding the critical aspects of the method, assisting analysts in optimizing their methods for the most challenging analyses.
Intercomparison of Different Technologies for the Analysisof Total Mercury in...gurleyuk
Multiple methods promulgated by the EPA for compliance monitoring of mercury in wastewater were investigated and compared to cold vapor inductively coupled plasma mass spectrometry. This study was performed to identify the limitations and benefits associated with each analytical method and to identify how varying waste streams can induce method failures.
Designing, implementing and maintaining a truly universal approach to gas detection.
Protecting your people and your physical plant, while ensuring business continuity, are the most important functions of a xed gas detection solution. Engineering a reliable, high-performance sys- tem that makes it easier and more cost effective to meet this challenge is the driving force behind a truly universal approach to gas detection.
This white paper is about the evolution and bene ts of designing, implementing and maintaining a truly universal approach to gas detection. Our intention is to help you use this information, based on “universal truths,” to evaluate your current system and project the impact of next-generation gas detection on your organization’s safety and productivity in a global economy.
Automatic carbon dioxide methane gas sensor based on the solubility of gases ...Sherry Huang
Biogas methane content is a relevant variable in anaerobic digestion processing where knowledge of process kinetics or an early indicator of digester failure is needed.
Viserion raman spectroscopy for biotechnnology and chemistery (2)Remy Carbonnel 🤖
http://indatech.eu/?utm_source=slideshare Viserion® Raman Analyser will improve financial performance with faster process
development times and enhanced process understanding using a QbD approach. It enables a significant reduction of laboratory analyses, fast in-situ analysis of critical process parameters and attributes, and yield optimisation.
1. Join us to learn about the latest technological advances in scientific instrument design. Expand your laboratory’s capabilities,
improve sensitivity, and simplify method development. Learn how the design features of Thermo Scientific mass spectrometers
enable them to be the best solution for your experimental insert comma after experimental research and routine analytical needs.
Discover how the power of sample preparation automation can be fast, easy and inexpensive. Explore how extraction and instru-
ment consumables can improve sample separation and detection, saving your laboratory money. The afternoon applications
workshop will offer engaging presentations with a variety of topics available for discussion, including converting your GC and GC-MS
from helium to hydrogen carrier gas for cheaper and faster separations, pesticide analysis by triple quadrupole GC-MS technology,
and popular environmental, sample preparation, food safety and pharmaceutical applications.
agenda
8:00 am Welcome and Continental Breakfast
9:00 am Select your track of interest – feel free to move between tracks
9:00 am Trusted Solutions for Reliable Gas Chromatographyy Analyses at
Your Fingertips
Thermo Fisher Scientific has a complete portfolio from sample preparation
to vials and closures to GC columns. We will explore all of the resources
available to you and provide you with all the necessary tools to achieve
repeatable, and predictable results, separation after separation.
9:30 am Eliminate Sample Prep Bottlenecks with the
Power of Automation
This presentation will detail how performing extraction and concentration
using the Thermo Scientific™
Dionex™
ASE™
Accelerated Solvent Extrac-
tor system, the Thermo Scientific™
Dionex™
AutoTrace™
280 Solid-Phase
Extraction instrument and the Rocket™
Evaporator will dramatically increase
laboratory throughput. With the power of automation, complete extraction of
both liquid, solid and semisolid samples saves you time, solvent and money.
10:15 am Break
10:30 am Introducing the Thermo Scientific TSQ 8000: Triple Quadrupole
GC-MS/MS Making Complex MS/MS Analysis Simple
There is currently a surge of interest in GC-MS around the use of triple
quadrupole analyzers for routine quantitation and confirmation. In
particular, a popular application of this technology has become the
screening of hundreds of target compounds in complex matrices.
The interest in triple quadrupole mass spectrometers for this type of
application is due to its excellent sensitivity, linearity and scan speed,
combined with the unique selectivity against matrix enabled by MS/MS
technology. While the selectivity benefit of MS/MS technology is clear, a
need has arisen to make this relatively complex technique more
accessible to laboratories that are too busy to spend weeks with method
development and familiarization. To address this need, several tools have
been developed for the recently launched Thermo Scientific™
TSQ 8000™
Triple Quadrupole GC-MS to simplify MS/MS method development and
daily operation. Examples of such tools range from AutoSRM, software
that greatly simplifies MS/MS method development, to the complete
methodology for the analysis of common target compounds. The tools
developed for the TSQ 8000 MS that simplify complex MS/MS analysis
will be presented using the comprehensive screening of pesticides as
an application example.
11:15 am What’s New with Thermo Scientific GC and GC-MS
The newest Thermo Scientific GC and GC-MS tools provide new
possibilities for your laboratory. Discover the next level of instrument
usability with the next generation GC with engineered miniaturized, instant
connect plug-in injectors and detectors, redefining usability and flexibility
in routine and high throughput laboratories. See how the
Thermo Scientific™
TRACE™
1300 Series GC is the most flexible gas
chromatograph for your laboratory. Attendees will learn how the new
Thermo Scientific™
TriPlus™
300 Headspace Autosampler can provide
sensitivity similar to more complex dynamic range purge and trap
systems. The Thermo Scientific™
TriPlus RSH™
autosampler showcases
new technology in sample handling, and moves beyond automated sample
injections to more advanced tasks, such as dilutions for automated
curve generation, sample derivatiztion and internal standard additions.
Maximize your mass spectrometer’s productivity and flexibility. Learn how
you can tackle today’s challenges with the advanced features of the
Thermo Scientific™
ISQ™
Single Quadrupole GC-MS system with the
innovative Thermo Scientifi™
ExtractaBrite™
ion source which can be
removed in it’s entirety and replaced in less than three minutes without
venting the mass spectrometer. Learn about the newest innovations to
dramatically improve your laboratory’s gas chromatography and mass
spectrometry needs.
12:00 pm Lunch
1:00pm Applications Workshop
*3:00pm Informal Discussion and Wrap-up
Discover new analytical technologies
gas chromatography and mass spectrometry
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2
3
PRODUCTIVITY SERIES
ion chromatography and atomic spectroscopy
gas chromatography and GC/mass spectrometry
liquid chromatography and LC/mass spectrometry
BRING YOUR ANALYTICAL CHALLENGES TO OUR
INTERACTIVE APPLICATIONS WORKSHOP
See page 2-3 for the afternoon Interactive
Applications Workshop abstracts
A Three-Track Learning Opportunity
Feel free to move between tracks.
collaborate with the experts
to solve your toughest analytical
challenges at a city nearby!
2. Automated Solutions to Enhance Static Headspace Gas Chromatography Determinations (Pharmaceutical)
Static headspace is a widely used sampling technique for the analysis of volatiles organic compounds in liquid and solid matrices
by gas chromatography. This technique is accepted worldwide with a set of official norms regulating the determination of residual
volatile species in environmental samples like water and soils, in consumer and pharmaceutical products, and in biological sam-
ples. With the always growing and challenging needs of laboratories in terms of throughput and sensitivity requirements, head-
space instrumentation is constantly evolving. With minimal changes to the GC instrumentation, static headspace systems can
provide sensitivity similar to more complex dynamic purge and trap analysis. The newest technology in sample handling, beyond
automated sample injections, will also be covered. We will demonstrate more advanced tasks, such as dilutions for automated
standard curve generation, internal standard additions and derivatization routines can ultimately improve the quality of data. In
this seminar, data will be presented in the areas of the analysis of halogenated contaminants at ppt levels in drinkable water, as
well as high-throughput forensic, pharma and material characterization analyses run by means of static headspace.
From Helium to Hydrogen: GC-MS Case Study on SVOCs in Water (Environmental)
The analysis of semi-volatile organic compounds (SVOCs) in wastewater by United States Environmental Protection Agency (U.S.
EPA) Method 8270 involves identification and quantitation of more than 120 analytes of varying chemical structure, polarity and
volatility. The diversity of the analytes in this method, along with specific DFTPP tune requirements, presents particular chal-
lenges when migrating from helium to hydrogen carrier gas. We will present and compare data of fast GC-MS analysis of SVOCs
performed in accordance with EPA Method 8270 on the TRACE 1310 GC coupled to an ISQ single quadrupole mass spectrometer
utilizing helium and hydrogen carrier gases. Key modifications to both GC and MS set up in hardware and methods necessary for
successful migration to hydrogen carrier gas will be discussed, and the effect of each parameter on the data quality will be dem-
onstrated. The final, optimized, and validated EPA Method 8270 fully migrated to hydrogen carrier gas with improved peak shape,
resolution, run time, and sensitivity will be presented.
Pesticide Determination Challenges in Food Products with Triple Quadrupole GC-MS (Food Safety)
Triple quadrupole mass spectrometers provide your laboratory with the ability to analyze and confirm in full scan and selected re-
action monitoring (SRM). Full scan in the triple quadrupole works just like the single quadrupole. SRM adds the ability to analyze
to even lower detection limits in heavy matrix. Your lab can take advantage of this in several ways. A smaller sample size can be
used to reach the same detection limit, saving money and giving your lab an analytical advantage. In this presentation, we will
demonstrate the use of the Thermo Scientific GC-MS triple quadrupole mass spectrometers for challenging food safety analyses.
The TSQ 8000 GC-MS/MS provides lower detection limits and flexibility to your laboratory with full scan, SRM, and alternating
Full Scan/SRM. The Thermo Scientific™
TSQ Quantum™
XLS Ultra GC-MS/MS provides even greater sensitivity and a second level
of specificity, above any other GC-MS/MS triple quadrupole. By isolating at 0.1 amu prior to the second quadrupole, this system
can provide even lower detection limits for challenging priority pollutant analyses.
gas chromatography and mass spectrometry
applications workshop topics
This interactive workshop will be driven by attendee preference. A variety of topics will
be available for discussion including new software developments and demonstrations,
sample preparation and GC troubleshooting, method development tips and tricks, and
an overview of popular environmental, forensics, food safety and POP’s applications.
Discover new analytical technologies
Thermo Scientific TRACE 1310 GC - TSQ 8000
MS/MS (with TriPlus RSH autosampler)
Thermo Scientific TRACE 1310 GC
Thermo Scientific ISQ
Single Quadrupole GC-MS
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A variety of
Applications Workshop
Topics available
Register today!
To view the complete agenda, abstracts and extended list
of applications for customizing your workshop visit
www.thermoscientific.com/productivity
This is a FREE event!