The document discusses the formulation and evaluation of a herbal soap made with coffee, cocoa, and chocolate powder. It highlights the benefits of these ingredients for skin health, including antioxidant properties, moisturization, and anti-aging effects. The study covers the preparation methods, evaluation parameters, and results of the soap's effectiveness in various tests.

1. FORMULATION AND EVALUATION OF
SOAP CONTAINING COFFEE COCOA
AND CHOCOLATE POWDER
PRESENTED BY:-
Name Enrollment no.
Suchi patel 202770290012
Yashik patel 202770290024
Priyanshu patel 202770290086
Aditya nath 202770290092
Mansi gohel 202770290093

2. CONTENT

3. CONTENT:-
• Introduction
• Litrature review
• Rationale
• Materials
• Method of preparation
• Evaluation Parameters
• Conclusion
• Reference

4. INTRODUCTION

5. INTRODUCTION: -
 Coffee and cocoa soap is a luxurious, aromatic soap that combines the benefits of coffee and
cocoa for the skin.
 Coffee grounds in the soap provides gentle exfoliation, removing dead skin cells and revealing
smoother skin.
 Cocoa powder is rich in antioxidants, which help fight free radicals and protect the skin from
damage.
 Both coffee and cocoa have anti-inflammatory properties that can soothe irritated skin and
reduce redness.
 The caffeine in coffee can stimulate blood flow, which may help to reduce the appearance of
cellulite and promote overall skin health.
 Coffee and cocoa soaps are made with natural, biodegradable ingredients, making them a
sustainable choice for skincare.

6. BIOLOGICAL
SOURCE AND
FAMILY: -
• Botanical name: -
COFFEA(GENUS)
• Geographical source:
- Latin America,
eastern Africa, Asia,
Arabia
• Family: -
RUBIACEAE

7. LITERATUARE REVIEW

8. Sr.
No.
Author Title of article Abstract
1. Sonali B. Aher*1, Pratiksha
S. Shinde1, Sharddha B.
Bhor2, Asmita K.Ovhal3 , et al
FORMULATION AND
EVALUATION OF COFFEE
SOAP WITH
ANTIOXIDANT,
ANTICARCINOPREVETIVE
, ANTICELLUITES
PROPERTIES
The aim of this study is to formulate a poly herbal soap
with the extracts of Coffee Powder and coconut oil. The
studies and research indicated above show that coffee
soap possesses anti-aging, anti-cancer, and anti-cellulite
characteristics. Glycerine, coconut oil, clear soap base,
steric acid, and sodium hydroxide are some of the
substances employed in medications to treat various skin
conditions.
2. Duangjai A*1, 3,4, Utsintong
M2 , Saokaew S2-7 .
COFFEE (COFFEA
ARABICA L.) PULP
EXTRACTS AS A
POTENTIAL SOURCE OF
WHITENING AGENTS
The aims of this study were to determine antioxidants
and anti-tyrosinase activities of coffee pulp extract, then
stability evaluation of lotion from the extract so that
coffee pulp may be finally used in cosmetic products.
Coffee pulp extracts showed antioxidant activity and
expressed anti-tyrosinase activities 40 % inhibition.
Besides, their active compounds, caffeine and caffeic
acid, revealed strongly inhibit tyrosinase activity with
45- 47 % inhibition.

9. Sr.
No.
Author Title of article Abstract
3. Jadhav Nandini Rajendra,
Jadhav Dnyanada Ravindra,
Jaiswal Roshani Pramod Miss.
Sulbha Patil.
Formulation and
Evaluation of transparent
skin brightening Coffee
soap
Coffee soap was prepared by using coffee powder and
transparent soap base and evaluated by using various
evaluation parameters such as organoleptic
characteristics, pH, foam height retention, skin irritation
and high temperature stability. Prepared coffee soap
having good appearance, better cleansing and foaming
effect and doesn’t have any side effects and have many
face skin benefits including Skin Brightening. and
Evaluation of transparent skin brightening coffee soap.
4. Giovanni Scapagnini 1,2,* ,
Sergio Davinelli 1,2, Laura Di
Renzo3 , Antonino De
Lorenzo3 , Hector Hugo
Olarte4, et al .
Efficacy of cocoa pod
extract as antiwrinkle gel
on human skin surface
Cocoa pods are abundant waste materials of cocoa
plantation, which are usually discarded onto plantation
floors. On the other hand, cocoa pods potentially contain
antioxidant compounds. Antioxidant compounds are
related to the protection of skin from wrinkles and can be
used as functional cosmetic ingredients. Therefore, in this
study, cocoa pods were extracted and to be used as active
ingredients for anti-wrinkles.

10. RATIONALE

11. RATIONALE:-
 Both coffee and cocoa powder are rich in antioxidants, which help fight free radicals that
can damage skin cells and contribute to premature aging. These antioxidants can help reduce
the appearance of fine lines, wrinkles, and age spots, promoting a more youthful
complexion.
 Caffeine is known to stimulate blood flow, which can promote collagen production and
improve skin elasticity, leading to firmer, more toned skin over time.
 The natural oils present in cocoa and coffee can help moisturize and hydrate the skin,
leaving it feeling soft and supple. This can be especially beneficial for dry or dehydrated
skin, as it helps restore the skin's natural moisture barrier.
 The aroma of coffee and cocoa may have anti-bacterial properties, which could help to
reduce the risk of skin infections. coffee and cocoa is often associated with comfort and
relaxation, offering potential stress-relieving benefits.

12. MATERIALS

13. Materials used:

14. SR NO INGREDIENTS QUANTITY USES
1. Sodium Hydroxide (Lye, NaOH) 5.82 gm • For saponification reaction
2. Olive oil 36.4 gm • As emollient
• Soften the skin
3. Coconut oil 6.46 gm • Anti-oxidant
• Foaming agent
4. Coffee 3 gm • Anti-oxidant
• Protecting the skin against harmful bacteria
• Anti-wrinkle
5. Cocoa powder 2 gm • Reduce rashes and soothing relief
• Anti-aging
6. Chocolate powder 1 gm • Gives youthful glow
• Brightens the skin
7. Water 15.55 gm • As solvent
8. Essential oil 2-3 drops • Perfuming agent
Materials used in Oil base soap: -

15. Materials used in Glycerin base soap: -
SR. NO. INGREDIENTS QUANTITY USES
1. Sodium Hydroxide (Lye, NaOH) 4.55 gm • For saponification reaction
2. Olive oil 13.4 gm • As emollient
• Soften the skin
3. Coconut oil 12.6 gm • As cleansing agent
• Anti-oxidant
• Foaming agent
4. Glycerin 5.5 gm • Reduce the loss of moisture
4. Coffee powder 1 gm • Anti-oxidant
• Protecting the skin against harmful bacteria
• Anti-wrinkle
5. Cocoa powder 1 gm • Reduce rashes and soothing relief
• Anti-aging
6. Chocolate powder 1 gm • Gives youthful glow
• Brightens the skin
7. Caster oil 11.08 gm • Reduce the loss of moisture
7. Distilled water 14.46 gm • As solvent
8. Essential oil 2-3 drops • Perfuming agent

16. METHOD OF PREPARATION

17. PREPARATION METHOD OF OIL BASE SOAP: -
Weighed amount of coconut oil, olive oil using scale Tec weighing balance and
poured it into a beaker.
In another beaker, prepare the basic saponification reaction by adding Sodium
Hydroxide in distilled water.
In another beaker, prepare the basic saponification reaction by adding Sodium
Hydroxide in distilled water.
Add the coffee powder , cocoa powder and choco powder in the mixture.
The soap mixture was then allowed to solidify for 24 to 36 hours at room
temperature.

18. PREPARATION METHOD OF GLYCERINE
BASE SOAP
Prepare the basic saponification reaction by adding Sodium Hydroxide in distilled water by heating below
50° C until it become transparent than allow it to cool.
Add the oil mixture in the solution of lye and mixed well with the help of magnetic stirrer without heating
involving the cold process of soap formation.
Heat the mixture until the mixture become translucent.
Pour the ethyl alcohol and glycerin into the translucent mixture.
Allow the mixture to boil for about 30 minutes in double boiler.
Already prepared sugar solution poured into the mixture and add the mixture into the soap
mold.
The soap mixture was then allowed to solidify for 24 to 36 hours at room temperature.

19. EVALUATION PARAMETERS

20. EVALUATION TEST: -
• pH of the soap: - 1% of soap solution was prepared by dissolving 1g of soap in distilled
water in a volumetric flask of 100ml. The pH of soap was measured in triplicate form using
Lab care export Digital pH meter. Electrode was introduced into the solution and the pH was
recorded.
• Foam foaming ability: - 1g of soap was taken and was dissolved in 50ml distilled water
in a 100ml measuring cylinder. Then shake the measuring cylinder for about 2 to 3 minutes
and it was allowed to stand for about 10minutes and measure the foam height.
• Retention time of foam: - Foam retention time refers to the time for which the foam
produced by the soap retains. The above procedure was repeated and the foam interval was
measured for about 5 to 10 minutes.

21. EVAUATION TEST: -
• Saponification value determination: - For the determination of saponification value
about 2g of the soap sample was taken in a conical flask and 0.5ml KOH solution was added
to it. This mixture was heated about 55˚ Celsius along with stirring continuously on a hot
water bath. Then the temperature was further increased 100˚ Celsius and boiling was
continued for about 1hour titration was performed with phenolphthalein was an indicator and
0.5M HCl. The end point observed is pink color disappearance.
• Saponification Value: Average volume of KOH × 28.056/ Weight of oil

22. EVAUATION TEST: -
• Determination of total fatty matter: - The procedure is carried out by the reaction of
the soap with an acid in association of hot water. In this approximately 10g of soap was
taken and dissolved in 150ml distill water. It was dissolved by heating. Then the soap
solution was treated with 20% Sulfuric acid and heated till the solution gets cleared. Fatty
acids would be observed at the surface or the film which were then solidified by the addition
of 7g of bees wax and again heated.
• Odor: - The smell of formulation was checked by applying preparation on hand and feels
the fragrance of perfume.
• Color & shape: - Color and shape was checked by naked eye.

23. RESULT

24. RESULT OF OIL BASE SOAP: -
SR. NO. PARAMETERS SAMPLE
1. pH 7.5
2. Color Brownish black
3. Foam foaming ability 10 ml
4. Retention time of foam 8-10 minute
5. Saponification value 140.5 g/ml
6. Total fatty matter 69 %

25. RESULT OF GLYCERINE BASE SOAP: -
SR. NO. EVALUATION PARAMETERS SAMPLE
1. pH 7.8
2. Color Brown
3. Foam foaming ability 12 ml
4. Retention time of foam 10-13 minute
5. Saponification value 157.5 g/ml
6. Total fatty matter 72 %

26. CONCLUSION

27. CONCLUSION: -
• The herbal soap was prepared by using cold process technique and were found to be without
particle transparent components which are used in formulation having good compatibility
without any changes.
• Cold process method is quick, least expensive in compare to hot process.
• Through cold process method oil base soap can be made and through hot process method
glycerin base soap can be made.
• The present work is a novel herbal soap formulation using coffee contains alkaloids, phenolic
acids, flavonoids, terpenoids and so on.

28. REFERENCE

29. REFERENCE: -

30. THANK YOU