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Heat treatment of alloys
Rajesh Kumar S
AP/Aero
C. Abdul Hakeem College of Engg and Tech
HEAT TREATMENT OF ALUMINIUM ALLOY
• Wrought form of aluminium-pure form- AL1100
• High Degree of corrosion resistance but low strength
• Aluminium becomes stronger
(i) Rolled (ii) Heat treated
Formed (or)
Cold Worked
T4- Solution Heat Treated; H-strain Hardened
O- Soft or Annealed; T6-Solution Heat Treated and then
artificially aged
HEAT TREATMENT OF ALUMINIUM ALLOY
• Alclad Aluminium
• Pure clad
• The sheets consists of an aluminium alloy core coated with a layer of pure aluminium
• The pure aluminium coating give protection to core against corrosive agents, scratching or other
forms of abrasion.
Two types of HEAT TREATMENT to ALUMINIUM ALLOY
• (i) Solution heat treatment –(Al2017, Al2024)
• (ii) Precipitation Heat treatment
(Al2014, Al7075) requires both types
solution heat treatment
• 825 F to 980 F
• RULE: Temperature must be controlled within a very narrow range
(±10 F)
• Low temp: max. strength may not be obtained
• Excessive temp: danger of melting, the low melting constituents.
Process:
(i) Soaking:
time at temperature,
soaking time: measured as the time the coldest metal
reaches the minimum desired temperature range
(i) Quenching:-cold water, Hot water, Spray quenching, Lag b/w
soaking and Quenching (10 sec)
Precipitation hardening
• 3 steps:
• Solution heat treatment
• Quenching
• Precipitation Heat Treatment
Precipitation hardening
Aluminium
Magnesium
Nickel
Titanium
Some steels and stainless steels
Aging:
Alloys can be kept at elevated temperature for hours to allow precipitation to
take place. This time delay is called aging.
SHT: involves formation of a single phase solid solution via quenching
PHT: involves the addition of impurity particles to increase material’s strength.
HEAT TREATMENT OF magnesium ALLOY
• 95% of Mg used in aircraft construction is in cast form
• Heat treatment is similar to Al alloy
(i) Solution heat treatment
(ii) Precipitation heat treatment
• Change in properties is negligible when allowed to age naturally at
room tempratures.
solution heat treatment of MAGNESIUM ALLOY
• Magnesium alloy casting-SHT
• To improve tensile strength, ductility and shock resistance
• T4-
• T6-
• Solution heat treatment
• Solution heat treatment + ARTIFICIAL aging
• Artificial aging is necessary to develop full properties.
• 730 F to 780 F
• Soaking time: 10 to18 hr……………….(longer than 18 hrs…more than
2inch thick)
• NEVER heat a magnesium alloy in a salt bath- explosion
• Fire hazard exists in SHT of magnesium alloy (protective atm of SO2)
precipitation heat treatment of MAGNESIUM ALLOY
• To increase hardness and yield strength
• Relieve stresses
• Stabilize alloys
• Amount of ductility reduced
• Corrosion resistance also improves
• Lower temp range than SHT (325 F to 500 F)
• Soaking time 4 to 18 hrs
HEAT TREATMENT OF TITANIUM ALLOY
PURPOSE
• Relief of internal stresses
• Annealing – to provide maximum ductility
• Thermal Hardening - to improve strength
• Case hardening
Heat treatment of TITANIUM ALLOY
• STRESS RELIEVING
• To remove stress concentration – 650 F to 1000 F
• Time at temperature: (few minute to an hour or more for heavier sections)
• Scales or discoloration removed by pickling in acid solution.
10 to 20% HNO3 and 1 to 3% hydrofluoric acid
• FULL ANNEALING
• Toughness, Ductility at room temperature, dimensional and structural
stability, Improved machinability.
• 1200 F to 1650 F
• Time at temperature: 16 min to several hours
• Scales or discoloration : Use of caustic descaling –sodium hydride salt bath.
• THERMAL HARDENING
• Unalloyed titanium cannot be heat treated.
• Most of alloys strengthed by heat treatment
• Sacrificing ductility
• Water quenching from 1450 F followed by reheating to 900 F , 8 hours
Heat treatment of TITANIUM ALLOY
• CASE HARDENING-
• Nitriding, carburizing and carbonitriding
• Wear Resistance case of 0.0001 to 0.0002 inch
Melting point of ALLOYs
• Carbon – 3540 C
• Titanium – 1650 C
• Aluminium – 660 C
• Magnesium – 650 C
• Mild steel – 1370 C
Soaking
Temperature
Time at temperature
Soaking Time
AL-SHT
AL-PHT
825 F to 980 F 10 min to 12 hours
Mg-SHT
Mg-PHT
730 F to 780 F
325 F to 500 F
10 hours to 18 hours
4 hours to 18 hourss
Ti- SHT
Ti-PHT

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Aircraft materials

  • 1. Heat treatment of alloys Rajesh Kumar S AP/Aero C. Abdul Hakeem College of Engg and Tech
  • 2. HEAT TREATMENT OF ALUMINIUM ALLOY • Wrought form of aluminium-pure form- AL1100 • High Degree of corrosion resistance but low strength • Aluminium becomes stronger (i) Rolled (ii) Heat treated Formed (or) Cold Worked T4- Solution Heat Treated; H-strain Hardened O- Soft or Annealed; T6-Solution Heat Treated and then artificially aged
  • 3. HEAT TREATMENT OF ALUMINIUM ALLOY • Alclad Aluminium • Pure clad • The sheets consists of an aluminium alloy core coated with a layer of pure aluminium • The pure aluminium coating give protection to core against corrosive agents, scratching or other forms of abrasion.
  • 4. Two types of HEAT TREATMENT to ALUMINIUM ALLOY • (i) Solution heat treatment –(Al2017, Al2024) • (ii) Precipitation Heat treatment (Al2014, Al7075) requires both types
  • 5. solution heat treatment • 825 F to 980 F • RULE: Temperature must be controlled within a very narrow range (±10 F) • Low temp: max. strength may not be obtained • Excessive temp: danger of melting, the low melting constituents. Process: (i) Soaking: time at temperature, soaking time: measured as the time the coldest metal reaches the minimum desired temperature range (i) Quenching:-cold water, Hot water, Spray quenching, Lag b/w soaking and Quenching (10 sec)
  • 6. Precipitation hardening • 3 steps: • Solution heat treatment • Quenching • Precipitation Heat Treatment
  • 7. Precipitation hardening Aluminium Magnesium Nickel Titanium Some steels and stainless steels Aging: Alloys can be kept at elevated temperature for hours to allow precipitation to take place. This time delay is called aging. SHT: involves formation of a single phase solid solution via quenching PHT: involves the addition of impurity particles to increase material’s strength.
  • 8. HEAT TREATMENT OF magnesium ALLOY • 95% of Mg used in aircraft construction is in cast form • Heat treatment is similar to Al alloy (i) Solution heat treatment (ii) Precipitation heat treatment • Change in properties is negligible when allowed to age naturally at room tempratures.
  • 9. solution heat treatment of MAGNESIUM ALLOY • Magnesium alloy casting-SHT • To improve tensile strength, ductility and shock resistance • T4- • T6- • Solution heat treatment • Solution heat treatment + ARTIFICIAL aging • Artificial aging is necessary to develop full properties. • 730 F to 780 F • Soaking time: 10 to18 hr……………….(longer than 18 hrs…more than 2inch thick) • NEVER heat a magnesium alloy in a salt bath- explosion • Fire hazard exists in SHT of magnesium alloy (protective atm of SO2)
  • 10. precipitation heat treatment of MAGNESIUM ALLOY • To increase hardness and yield strength • Relieve stresses • Stabilize alloys • Amount of ductility reduced • Corrosion resistance also improves • Lower temp range than SHT (325 F to 500 F) • Soaking time 4 to 18 hrs
  • 11. HEAT TREATMENT OF TITANIUM ALLOY PURPOSE • Relief of internal stresses • Annealing – to provide maximum ductility • Thermal Hardening - to improve strength • Case hardening
  • 12. Heat treatment of TITANIUM ALLOY • STRESS RELIEVING • To remove stress concentration – 650 F to 1000 F • Time at temperature: (few minute to an hour or more for heavier sections) • Scales or discoloration removed by pickling in acid solution. 10 to 20% HNO3 and 1 to 3% hydrofluoric acid • FULL ANNEALING • Toughness, Ductility at room temperature, dimensional and structural stability, Improved machinability. • 1200 F to 1650 F • Time at temperature: 16 min to several hours • Scales or discoloration : Use of caustic descaling –sodium hydride salt bath. • THERMAL HARDENING • Unalloyed titanium cannot be heat treated. • Most of alloys strengthed by heat treatment • Sacrificing ductility • Water quenching from 1450 F followed by reheating to 900 F , 8 hours
  • 13. Heat treatment of TITANIUM ALLOY • CASE HARDENING- • Nitriding, carburizing and carbonitriding • Wear Resistance case of 0.0001 to 0.0002 inch
  • 14. Melting point of ALLOYs • Carbon – 3540 C • Titanium – 1650 C • Aluminium – 660 C • Magnesium – 650 C • Mild steel – 1370 C
  • 15. Soaking Temperature Time at temperature Soaking Time AL-SHT AL-PHT 825 F to 980 F 10 min to 12 hours Mg-SHT Mg-PHT 730 F to 780 F 325 F to 500 F 10 hours to 18 hours 4 hours to 18 hourss Ti- SHT Ti-PHT