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Water in the circular economy –
innovations for urban water treatment
Reuse of water – Resource recovery – Resource efficiency
www.r3water.eu This project has received funding from the European Union’s
Seventh Programme for research, technological development
and demonstration under grant agreement No 619093.
2
Coordinator:
Uwe Fortkamp	
Email:	uwe.fortkamp@ivl.se	
Phone:	+46 (0)8598 56304	
Klara Westling
Email:	klara.westling@ivl.se
Phone:	+46 (0)8598 56431
IVL Swedish Environmental Research Institute
Vallhallavaegen 81
11427 Stockholm
Sweden
www.ivl.se
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
3
R3Water: Getting all the value from wastewater 6
Policy Brief 4
R3Water Partner 5
Technologies 7
Reuse of Water 7
aquaBio 7
AQUATRACK® & ozone polishing 10
doscontrol® 17
Resource Recovery 19
Hydrothermal Carbonisation (HTC) 19
Sludge ash valorization 22
Resource Efficiency 24
Anammox 24
OptimEDAR 27
Model based predictive control 29
Model-based energy audits in wastewater treatment plants 32
InnoWatt 35
Fluidic oscilliation 37
Experiences with EU ETV Pilot Programme 40
Demo sites 41
Location of technologies at the wastewater treatment plant 41
Demonstration sites in Spain 42
Demonstration sites in Belgium 44
Demonstration site in Sweden 45
Table of Contents
CONTENTS
4
Removing pollutants is of course a priority at wastewater
treatment plants, yet there is a growing awareness that they
could also act as resource facilities, providing energy, nutri-
ents and other valuable resources. This is the goal of the EU
FP7 funded project R3Water (“Demonstration of innovative
solutions for Reuse of water, Recovery of valuables and Re-
source efficiency in urban wastewater treatment“) with the
idea to support the transition from being purely a treatment
plant towards a Water Resource Recovery Facility (WRRF).
Focus in the project is to develop and test solutions for up-
grading existing treatment plants and to improve resource
efficiency combined with the implementation of new tech-
nologies and business models.
In order to reach this target R3 Water developed and demon-
strated innovative technologies at three sites (Belgium, Spain,
Sweden) within 3 areas:
•	 Resource efficient treatment, e.g. by efficient aeration and
optimised process control
•	 Facilitating water reuse, e.g. by improved water quality moni­
toring and efficient disinfection
•	 Recycling of nutrients and other valuables, e.g. by valorisa-
tion of sludge
Facilitating market uptake has been one of the project objec-
tives. All of the technologies and solutions being developed
have made progress during the project. Some of them are al-
most ready to market, and some technologies are being ver-
ified according to the EU ETV-scheme, with one technology
where verification has finished. This innovative “R3 demon-
stration concept (Reviewed – Referenced – Recognized)” se-
cures a more parallel and direct market acceptance in Euro-
pean countries and at the same time reduces the need for
extra testing. Further project results have been disseminated
to relevant stakeholder groups via different channels like
workshops, brochures, homepage, LinkedIn etc.
The strong consortium, led by IVL Swedish Environmental
Research Institute, involves 12 part-
ners from seven European countries
with a well-balanced ratio between
innovative SMEs, research institutes
and a high skilled advisory board.
It ensured a rapid adoption of the
SMEs innovative water and recovery
solutions.
This brochure provides you with the
results out of R3Water.
 
R3Water: Getting all the value from wastewater
Reuse
of water
Demo Spain
Recycling
of valuables
R3Water
Demo Sweden
Resource
efficient treatment
Demo Belgium
Review
Technologies
Demonstration
Environmental
Technology
Verification
(ETV)
Market
acceptance
in ETV
acceptance
countries
Market
acceptance
at global
market
Referenced Recognized
LCA
LCC
ETV
Future wastewater treatment: resource facilities for water, nutrients
and energy
Three areas (3 R’s) and tree demonstration sites in R3Water
Innovative“R3 demonstration concept (Reviewed – Referenced – Recognized)”: technologies
undergo a verification in the EU ET V Pilot programme in parallel to the demonstration at the
demo sites
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
5
	 Common suggestions
•	 Provide incentives to overcome reluctance to make investment caused by short-time operating contracts that act as a barrier for the
market uptake of innovative technologies.
•	 Ease the market uptake of new and innovative technologies
–	by simplifying the permission process for demonstrations at industrial sites, e.g. by using the concept of “transition peri-
ods”. For innovative technologies start with an entry level of requirement, requiring increased level of performance from
the technology to prove its veracity.
–	 by applying a holistic assessment: a better sustainability performance might need less strict (water) thresholds
•	 Use careful wording and terminology in official documents, as certain expressions create positive attitudes, while other with about
the same meaning create rather negative.
	 Reuse of water
•	 Although the benefits of water reclamation and reuse for irrigated agriculture (and other uses) are clear, there are still doubts about
the economic sustainability of reclaimed water services. Consider the reclaimed water as an additional local water resource in the
scope of the integrated urban/regional water cycle, rather than an isolated service provided by the WWTP.
•	 Harmonize quality criteria for water re-use including methods for quality monitoring as a driver for the marketing of water reuse
technologies (e.g. common standard within the EU).
•	 Online water quality monitoring technologies are not properly considered in EU Directives. Allow for innovation in monitoring tech-
nologies within the EU water directives review by taking the available online monitoring/detection technologies and the potential
for an effective combination with water quality monitoring methods (online + conventional sampling/analysis) into consideration.
	 Resource recovery
•	 Support the market for recovered resources by harmonizing legislation and directives. There is a need of for such harmonized
standards for recovered materials and products to make a foothold in the market dominated by virgin materials.
•	 Innovation partnership for the combination of research and procurement: more promotion to be enacted by member states and
public authorities.
	 Resource efficiency
•	 Stimulate the adoption of technologies by using incentives to establish sustainability benchmarks. This will help to balance medium
and long-term sustainability of increased resource efficiency and plant sustainability; with short-term economic cost disadvantages.
The whole“Report about policy and directive implementation”will be available on r3water.eu.
Policy Brief summary
6
R3Water Partner
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
CONSORTIUM
ADASA Sistemas S.A.U., Spain
(www.adasasistemas.com)
Aquafin N.V., Belgium
(www.aquafin.be)
Aqua-Q AB, Sweden
(www.aqua-q.se)
AVA Green Chemistry Development GmbH, Germany
(www.ava-co2.com)
DECHEMA Gesellschaft für Chemische Technik
und Biotechnologie e.V., Germany
(www.dechema.de)
Renotech OY, Finland
(www.renotech.fi)
ICRA Catalan Institute for Water Research, Spain
(www.icra.cat)
IVL Swedish Environmental Institute, Sweden
(www.ivl.se)
Perlemax Ltd, UK
(www.perlemax.com)
Prediktor AS, Norway
(www.prediktor.no)
Teqma Tecnologias y equipos para el medio
ambiente S.L., Spain
(http://teqma.com/)
VTT Technical Research Centre of Finland, Finland
(www.vtt.fi)
7
aquaBio
Description
E. coli is a bacteria widely used as an indicator of fecal con-
tamination. Its presence warns about a potential sanitary
risk. This aspect is reflected in the Directive 2006/7/EC on
the quality of bathing water. The Escherichia coli and total
coliform parameters are also key indicators and essential for
determining the potential uses of reclaimed water from the
tertiary treatment of a WWTP and it is present in existing Na-
tional Water Reuse Directives (ES, IT, FR, GR, CY) as well as in
most of worldwide regulations.
However, traditional sampling plus laboratory method takes
from 24h to 96h to obtain the results, becoming useless for
early warning purposes. aquaBio can provide the results be-
tween 3h and 12h (depending on the microorganism con-
centration) in automatic way, and to transmit this informa-
tion to a local control center or remote on duty staff.
Addressed problems and challanges
The goals in the project were to demonstrate the operational
autonomy, the reliability and robustness of the equipment
running in a continuous way, and to obtain enough lab anal-
ysis to contrast with the automatic results in order to launch
an ETV verification process. During the project, the mainte-
nance requirements were decreased from the initial once a
week to a final once a month.
aquaBio provides an early warning about a potential sanitary risk through the simultaneous measurement of E.coli and
total coliforms in a continuous and automated way, with low maintenance requirements.
Technologies Reuse of Water
8
Applicability and pre-requisites
aquaBio is applicable for reclaimed water uses, bathing water
anddrinkingwater.aquaBiomanagesautomaticallythesample
intake as well the disinfection until the intake point. The pre-
requisites are an electric power connection and one sampling
point.
Features and benefits
Features:
Measurement principle:
•	 Fluorimetric detection for Escherichiacoliex. 365 nm em. 450 nm
•	 Colorimetric detection for total coliforms abs 405 nm
•	 Reagents used: Colilert-18® from IDEXX in liquid form
•	 Biocide solution
Detection limit:
•	 Escherichia coli: <1 bacteria in 100 ml
•	 Total coliforms : <1 bacteria in 100 ml
Minimum analysis time:
From 3 to 12 hours, depending on the microorganism concen-
tration.
Benefits:
•	 Early warning in case of the water reclamation plant malfunc-
tioning.
•	 Efficient production of reclaimed water, avoiding overdosing
of disinfection chemicals and excess of UV power consumption.
•	 Production of fit-for-purpose reclaimed water, according to
the intended water quality for the reuse in irrigation of veg-
etables, wood crops, golf courses or other industrial uses.
Operation and maintenance
aquaBio stands out for its high autonomy and its low cost in
maintenance operations. Only one maintenance operation
per month has to be performed in order to ensure its correct
operation.
Results
The aquaBio has been demonstrated in two different demos-
ites. Castell d’aro water reclamation plant (outlet and inlet), a
Spanish demosite, and in Hammary Sjöstadsverk (MBR outlet),
the Swedish demosite.
Sample testing:
Different samples were compared to the IDEXX laboratory
methodology using colilert- 18® concluding that there are not
significant differences between aquaBio result and the labo-
ratory result.
Independence between samples:
In order to check the independence between samples, sterile
samples were interspersed during the standard operation.
As a result it was demostrated that none cross contamination
exists between one sample and the following one.
Correlation between samples analysed by the aquaBio and laboratory
(colilert-18®)
Sterile samples interspersed during operational period
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
9
Performance:
During all the operational period different operation modes
were tested: by time, by digital imput or alarms. The Castell
Platja d’Aro water reclamation plant runs on demand. The
aquaBio was connected to the valve that starts the process,
and the following graphics shows the low demand in winter
and the increase of demand during spring.
Maintenace operations: Currently the maintenance opera-
tions are performed once per month (30 minutes) thanks to
the improvements implemented during the project in the hy-
draulics and software as well in the maintenance procedures.
Perspectives for the future
One of the key priorities for the EC in the upcoming years is
to increase the ratio of water reuse in the EU, while ensuring
the health and environmental safety of water reuse practices
and the free trade of food products. Nevertheless, this priority
faces several barriers that prevent the adoption of the re-
claimed water for different uses: agriculture, urban, industrial
and recreational.
In order to tackle some of these barriers, the EU has launched
a process for the definition of the guidelines on minimum
quality requirements for water reuse for agriculture and
aquifer recharge, where E. coli is the recommended bacterial
indicator. In this context, the online monitoring of microor-
ganisms with aquaBio can contribute to the efficiency of the
water reclamation processes as well as on building trust on
end-users.
The next goal is to demonstrate the aquaBio for drinking wa-
ter use and to adapt the equipment for measuring Entero-
cocci in bathing waters.
Contact
adasa@adasaproducts.com
AquaBio adaptation to on demand water reuse
aquaBio
Decrease in the frequency of the maintenance operations.
TECHNOLOGIES – REUSE OF WATER
10
Technology 1 – AQUATRACK®
AQUATRACK® is a real time online monitoring and sampling
system for pathogens in treated wastewater for reuse and re-
claimed water. The system consists of multiple conventional
water quality sensors including an optical laser sensor which
detects all possible forms of variations caused by contamina-
tion (natural, human error, process failure) in reclaimed and
recycled water.
The system can commu-
nicate wireless and access
data remotely. The software
creates a dynamic fingerprint
of effluent water based upon
the micro contaminants/mi-
cro particles/micro debris in
the effluent water. When the
fingerprint deviates the sys-
tem automatically captures
relevant water sample
that can be analyzed for
positive identification
of pathogens.
AQUATRACK® is now EU
ETV certified for moni-
toring and sampling of
drinking water, reuse and
reclaimed water.
Addressed problems and challanges
The main source of contamination comes from purified or
insufficiently purified wastewater, both industrial and small-
scale private sewage discharge. It pollutes rivers, lakes, wa-
ter bodies, and coastal waters and creates potential risk of
microbial contamination in drinking water, bathing water,
groundwater, etc.
The emerging environmental problem in the developed coun-
tries is pharmaceutical residues in purified or insufficiently pu-
rified wastewater both from municipality and industries.
To eliminate the contamination and pollution there are con-
ventional wastewater treatment processes. The treatment of
wastewater is a high-energy consuming and releases green-
house gases. Wastewater discharge contains contaminants
like bacteria, parasites, virus and pharmaceutical residues
etc. Contaminated sludge is another problem in wastewater
treatment. The treated wastewater is not fully reused in wa-
ter scarcity areas today.
To solve the above mentioned problem of contamination
in the effluent water many new and modified different tech-
nologies/processes are being developed like MBR, MBBR and
SBR. etc. These membrane technologies have well defined
cut off. The effluent discharge is used for reuse or reclaimed
water in agriculture and ground water recharge.
IntheR3WaterProjectAqua-Qdevelopedanoveluser-friend-
ly, intelligent real time on-line monitoring and sampling sys-
AQUATRACK® & ozone polishing
Online optical monitoring of contaminants and ozone polishing
Aqua-Q developed two separate novel standalone technologies for safe reuse of effluent water:
1)	On-line real time optical (laser) contamination monitoring and automatic sampling system for effluent water coming
out of MBR, MBBR and SBR process. The system, AQUATRACK® - Early Warning System with automatic sampler, is
now EU ETV certified.
2)	Composed an automatic, self-contained modular ozone polishing system for online or batch application to eliminate
pharmaceutical residues and pathogens present in treated waste water (effluent) from MBR, MBBR, and SBR process.
Both of these innovative technologies are performing well as standalone and have been demonstrated successfully.
The idea is now to combine these technologies on a digital platform so that it can internally exchange and gather
information from each other and will act on demand. Ozone polishing will be actuated on demand by AQUATRACK®
to remove contaminants from effluent and provide safe and clean water for reuse.
The novel ozone polishing system is used on the effluent water from the MBR process and differentiates from other
waste water treatment technologies where they use ozone either in the beginning or in the middle of the MBR process.
That is why ozone polishing needs less ozone and there is no need for an active carbon filter (GAC).
Both of the technologies are patented.
AQUATRACK®
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
11
tem, AQUATRACK®, which is used for real time quality moni-
toring of the effluent from a MBR process in Stockholm and
now in Spain. The aim is to give the management of a treat-
ment plant early warning for sudden changes/deviations in
effluent water quality. These changes are having high proba-
bility of microbiological growth due to contamination that is
harmful to environment, rivers, lakes and contains also drug
residues among other organics.
AQUATRACK® is designed to monitor effluent quality 24/7 af-
ter MBS, MBBS, SBR and conventional treatment process and
collection of water sample when there is high risk for patho-
gens in the effluent discharge.
Applicability and pre-requisites
Applicability process of AQUATRACK® is user-friendly and fol-
lows the 4 simple steps, see picture to the right:
1.	 Connect a side flow of the effluent water to the inlet of
AQUATRACK® and get a fingerprint of your water stream
and always access the water quality changes on the lo-
cal monitor or get the results wireless.
2.-3.	Decide a highest amount of water quality variations of
your process water and get alarmed when variation occurs.
4.	 The variation that trigger the alarm is automatically
sampled and stored for further analysis
•	 Monitoring of wastewater effluent from MBR, MBBR, SBR and
after conventional waste water treatment process.
•	 Monitoring and quality control of industrial water treatment
process
•	 Monitoring of drinking water reservoir, networks, source/lake
water
Pre-requisites:
•	 The equipment needs to be placed inside a room having nor-
mal room temp 20°C and 230/240 V AC electrical plug with
floor drain. A partial constant flow of about 4-5 l/min of the
effluent to be monitored with an open/stop valve at a pres-
sure of 2-3 bar.
Features and benefits
Benefits of AQUATRACK®:
1.	 Most cost effective and accurate monitoring system for
immediate detection of MBR, UF, NF and RO filters break
through and alarms operator for the event with time and
date. Records all incidents. Clear economical benefit.
4 steps of the applicability process of AQUATRACK®
TECHNOLOGIES – REUSE OF WATER
12
2.	 Creation of individual fingerprint of different non-con-
taminated water helps preventing building of biofouling
by identifying contamination in time.
3.	 Early warning to an operator of a treatment plant for mi-
cro particles/micro debris exceeding the set limits in the
effluent. Always generate alarm when there is deviation
from stable water quality.
4.	 Operator can establish periodic pollutant profile (e.g. dai-
ly/monthly/yearly profile of micro contaminant presence
in water) and hence optimize treatment process.
5.	 Captures automatically water sample for biological &
chemical analyses: i.e. water sample captured right at the
time of the observed anomaly gives high confidence on
analysing results.
6.	 Helps protecting the environment in a sustainable way.
Safe re use of treated waste water brings value in life.
Operation and maintenance
•	 AQUATRACK® can be easily installed without making any
changes to the existing treatment process. Installation starts
working from day 1 (plug and play).
•	 Maintenance is simple and does not require much time.
Results
The graph below represents an overview of level of contam-
inants as fingerprint in the MBR effluent water and is repre-
sented in two clusters. Cluster 1 represents bacteria size and
cluster 2 represents size of parasites.This graph also indicates
that at about 10.30 am some anomaly happened and that
anomaly returned to normal around 16.30 pm. 10.30 to 16.30
was a critical period for the process.
Overview of level of contaminants as fingerprint in the MBR effluent
water, represented in two clusters
Thegraphbelowillustratesareal-timeexampleofAQUATRACK®
monitoring of treated wastewater. The increased values trig-
gering the automatic sampler is plotted against the number
of Heterotrophs (Total Count) measured by MBS MultiReader.
A correlation of 86% between the triggered alarms and bac-
teria count was found.
Above shows an overview of average mean values collected
by AQUATRACK® from July 2016 until April 2017 from MBR
effluent at WWTP La Bisbal d’Empordà, Spain.
Above shows the variations during one day of the effluent
quality from MBR process at WWTP La Bisbal d’Empordà,
Spain.
Real-time example of AQUATRACK® monitoring of treated wastewater
Overview of average mean values collected by AQUATRACK® from
July 2016 until April 2017 from MBR effluent at WWTP La Bisbal
d’Empordà, Spain.
Variations during one day of the effluent quality from MBR process at
WWTP La Bisbal d’Empordà, Spain.
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
13
Perspectives for the future
The ETV verification shows that AQUATRACK ® can be used to
keep continuous track of biological contaminants in drinking
water, source water, and treated wastewater (MBR effluent).
It can also be used to keep record of contaminants (e.g. mi-
cro-debris, biological contaminants, planned/unplanned dis-
charge of wastewater treatment plant).
This performance can be considered as an important feature
of an environmental monitoring technology.
Information from AQUATRACK® can be used to make intel-
ligent decisions about the amount and kind of disinfection,
hence avoiding over-disinfection and thus saving money.
AQUATRACK® can establish daily, monthly, and seasonal
contamination patterns which can be used to improve the
efficiency of a treatment process, thus saving electricity and
chemical costs.
AQUATRACK® gives real-time warning of possible contamina-
tion events, which can help to avert epidemics, and costs &
liabilities associated with epidemics.
AQUATRACK® can be claimed as an innovative and novel ear-
ly warning system of monitoring and sampling for pathogen
detection in drinking water and reclaimed water.
Technology 2 – Ozone polishing system to
eliminate pharmaceutical residues and
pathogens
Aqua-Q has developed/composed a modular ozone pol-
ishing system and has successfully demonstrated that in a
cost-effective way with a minimum dose of ozone both phar-
maceuticals residues and pathogens can be totally removed
beyond the limit of detection.
This online ozone polishing pilot system is fully automatic
and self-contained. Only a partial flow of effluent water from
MBR process and 230 – 240 V AC electric plug is required for
plug and play.
Local industrial regulations have to be maintained to comply
with government regulations.
Addressed problems and challanges
Water pollution/contamination from pharmaceutical resi-
dues are the major environmental challenge in aquatic envi-
ronment in many developed and emerging countries. Drug
residues from human and animal consumption through the
sewage system reach lakes and rivers that have become a
global environmental problem. Current drugs collide with
the requirements of sustainable development. Pharmaceuti-
cal consumption in society is increasing. 50-60% of this con-
sumption ends up in our water environment. Many of these
drugs are found in our drinking water, source/lake water,
aquatic life, bathing water, and ground water etc.
Even though the concentrations of these pharmaceutical
compounds are low concentrated (nanograms per litre lev-
els), no one really knows exactly the long-term exposure ad-
verse consequences affecting human health and aquatic life.
Scientists still arguing about the current state of the various
drug substances that can interact with each other and form
hazardous substances. Therefore, there is the need to devel-
op methods to eliminate these dangerous drug residues in
each treatment plants before discharging the effluent water
to nature or using it as reclaimed water. Stringent legislation
and control is required.
To solve this challenge, sophisticated technologies have been
developed and are commercially used in the treatment of
wastewater (both municipal and industrial) like MBR (Mem-
brane Bio Reactor) and MBBR (Moving Bed Bio Reactor) etc..
Even though pharmaceutical compounds were found in the
effluent from a MBR process (see below under results).
Ozone polishing system
TECHNOLOGIES – REUSE OF WATER
14
Aqua-Qs innovative solution is online real time monitoring
and sampling of the contaminants (early warning) and in real
time eliminating that by ozone polishing so that safe and
clean treated wastewater can be reused without quick pos-
itive identification of type of contaminants.
Applicability and pre-requisites
To eliminate both the drug residues and pathogens in treat-
ed wastewater (effluent from MBR) Aqua-Q developed /
composed a cost-effective self-contained ozone polishing
process. Ozone is a strong oxidizing gas and spontaneously
reacts with organic substances and eliminates pathogens.
Mixing of ozone gas and effluent water by creating micro
bubbles and obtaining a stable ozone water solution is our
key success factor. This innovative ozone polishing process
treated effluent from the MBR at Hammarby Sjöstadsverk in
Stockholm. The ozone polishing step removes totally drug
residues below the limit of present detection limit and totally
inactivates bacteria and other pathogens found in municipal
and industrial effluent water. The treatment also reduces the
TOC and color of the effluent water (see picture below). The
ozone gas and the effluent water is mixed in a closed circu-
lation tank. Once the dissolved ozone concentration has ob-
tained the pre-determined value the water is discharged to
outlet.
Right: effluent from MBR process. Left: effluent water after after
ozone polishing
This modular ozone polishing system is automatic and
self-contained with oxygen generator, ozone generator, re-
action vessel, off gas destruction, efficient mixing of gas and
water with all the necessary instruments to monitor the pro-
cess stability.
In Combination with AQUATRACK® the ozone polishing tech-
nology is a power full tool to remove pharmaceutical resi-
dues and pathogens with real time online quality control for
reuse of water. The patented novel process set-up is a future
process system.
Pre-requisites:
The equipment needs to be placed inside a well-ventilated
room having normal room temp 20°C and 230/240V AC elec-
trical plug with floor drain. A partial constant flow of about
14-16 l/min of the MBR effluent is fed to the system with an
open/stop valve at a pressure of 2-3 bar. There should be an
ambient monitor for ozone gas leakage.
Features and benefits
Ozone polishing is a most cost-effective system to eliminate
both pharmaceutical residues and pathogens in the same
treatment coming out from a MBR system.
1)	 Our ozone polishing cost effectively eliminates both
pharmaceutical residues and pathogens in effluent water
with minimum dissolved ozone 0.08 ppm.
2)	 Require no secondary treatment with active carbon as no
by products are observed.
3)	 Our empirical experience confirms with that if we main-
tain a stable treatment process no costly pharmaceutical
analyses is required on regular basis for prioritized drug
residues as above.
4)	 Properly applied at correct position on a waste water
treatment process ozone is a most environmental and ef-
fective tool to decompose organic substances and path-
ogens in the effluent and can have GRAS status.
Operation and maintenance
1)	 As ozone, modular system is skid mount and complete with
system set up only electricity 230 – 240V AC is required.
2)	 Effluent water at room temp or if possible lower tempera-
ture is required along with discharge possibilities.
3) 	 Operation is plug and play.
4) 	 The system complies with all national industrial standards
including national environment regulations.
Results
The table and graph below illustrates some of our results of
active pharmaceutical residual substances found in the ef-
fluent of MBR process that has been effectively removed by
ozone polishing step below the limit of detection.
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
15
Before ozone After ozone
Substance Mode of action ng/L ng/L
Diclofenac Anti-inflammatories 601 <14
Furosemide Diuretics 957 <11
Hydrochlorothiazide Antihypertensives 1660 <2.8
Ibuprofen Anti-inflammatories 71 <10
Naproxen Anti-inflammatories 37 <4.6
Ramipril Antihypertensives <5.6 <5.6
Warfarin Anticoagulants 6,9 <4.9
Atenolol Antihypertensives 120 <3.7
Amlodipine Antihypertensives <3.6 <3.6
Bisoprolol Antihypertensives 32 <5.2
Caffeine Stimulant 17 <15
Carbamazepine Sedatives 265 <2.1
Citalopram Antidepressants 216 <6.5
Fluoxetine Antidepressants 8,8 <6.0
Ketoprofen Anti-inflammatories 68 <7.2
Metoprolol Antihypertensives 585 <6.6
Oxazepam Sedatives 402 6,6
Paracetamol Anti-inflammatories 28 <11
Propranolol Antihypertensives 68 <4.4
Ranitidine Antiulcers 72 <21
Risperidone Antipsychotic <22 <22
Sertralin Antidepressants <6.5 <6.5
Simvastatin Lipid-regulating <8.3 <8.3
Terbutaline Asthma medication 13 <2.4
Analysed at IVL Stockholm (<) lowest quantifiable limit (LOQ, S/N=10)
Samples RT 30°C 37°C Organic carbon (mg/l) Color at 410nm
Control 13*10^2 16*10^2 15*10^2 12.5 0.008
Treated 1 0 0 0 10 0.005
Treated 2 0 0 0 10.5 0.004
Treated 3 0 0 0 10 0.005
Removal of bacteria from MBR effluent by ozone polishing
Removal of pharmaceuticals and bacteria from MBR process.
Active pharmaceutical residual substances with/ without ozone polishing.
TECHNOLOGIES – REUSE OF WATER
16
Perspectives for the future
Reuse of water is essential in many parts of the world as pop-
ulation grows and demand for fresh clean and safe water
increases. Reuse of treated wastewater with quality control
provides hope and opportunity for people as water shortage
has become a global problem not only in emerging countries
but also in developed countries. There is a need for future
new EU legislation to ensure high clean and safe reuse water
standard not only a minimum standard for reuse of water as
discussed today.
From innovative technology perspective, Aqua-Q strongly
believes on future European standard for stringent quality
control of reuse of treated wastewater for filling the aquifers,
irrigation and other applications. Real time online monitor-
ing of contaminants of effluent is necessary to protect en-
vironment and our common water bodies. Aqua-Qs contri-
bution is a process set-up (see overview scheme) which will
ensure a cost effective combined processes to monitor the
contaminants in the effluent and eliminate the contaminants
by ozone polishing the effluent.
Membrane Bio
Reactor Effluent
AQUATRACKTM
Quality Assurance
Ozone Polishing
Necessaryparameterswillbe
analysedforprocessoptimization
Final effluent free
from pathogens
and pharmaceutical
residues
Aqua-Qs process set-up
Contact
Sudhir Chowdhury
sudhir@aqua-q.se
Ulla Chowdhury
ulla@aqua-q.se
www.aqua-q.se
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
17
Addressed problems and challanges
Reclaimed water is obtained from treated wastewater, a chal-
lenging effluent strongly influenced by upstream wastewa-
ter treatment processes with a highly variable concentration
and composition in time of the physiscal chemical and mi-
crobiological quality directly affecting the effectiveness and
reliability of disinfection processes. Disinfection agents and
techniques used in water reclamation have been commonly
adopted from drinking water treatment (i.e. Chlorine dioxide,
Sodium Hypochlorite, UV radiation, Ozonation). Combined
disinfection (e.g. synergetic use of UV radiation and chemical
oxidation) is a solution for effective disinfection in drinking
water and reclaimed water and its being used in several full
scale sites. Although the combination of complementary
disinfectant agents generates synergies broadening the dis-
infection spectrum, affecting pathogens that are not inacti-
vated by conventional chemical oxidizers as chlorine at the
normal concentrations (i.e. spore forming bacteria, viruses
and protozoa) while ensuring a residual concentration of dis-
infectant in the disitribution network, these processes lack
an effective and optimal contol system in order to ensure:
•	 Reliable operation, flexible against variable conditions
•	 Maximum synergies, cost optimization delivering the mini-
mum dosage to achieve the requiered disinfection level
•	 Continuous safe water production
doscontrol® is an automatic controller specifically desiged
to ensure effective disinfection in drinking water treatment
and water reclamation delivering the needed amount of
each disinfectant agent to continuously produce safe water
while optimizing the amount of UV dose and chlorine dos-
age reducing costs and environmental footprint.
Applicability and pre-requisites
doscontrol® can be applied into new or existing disinfection
treatments in water reclamation for reuse and other water
disinfection schemes (drinking water, recreational water, ir-
rigation, aquaculture etc).
Features and benefits
•	 Totally automated process
•	 Adjusted dose of disinfectant (physical and chemical) to pro-
duce safe water at the optimal cost.
•	 Fit-for-purpose production of reclaimed water, according to
the required water quality (irrigation, environmental and in-
dustrial uses)
•	 Valuable real time information of the disinfection process
•	 Reduction in O&M associated costs
•	 Reduction of chemical associated risks as disinfection by-
products
doscontrol®
doscontrol® is an innovative technology developed by teqma to control the water disinfection process. Based on the
optimized combination of chemical and physical disinfection, the controller is able to generate positive synergies de-
livering enhanced wide-spectrum microbiology load reduction and substantial operational costs reduction for a safe
reclaimed water production.
doscontrol® system
TECHNOLOGIES – REUSE OF WATER
18
Operation and maintenance
The system provides valuable on-line information and data
management for a proper disinfection equipment (e.g. UV
and chlorination) and a preventive and corrective mainte-
nance management. Besides, the operator can decide to use
doscontrol® or change to the previous operational mode if
desired.
Results
Thanks to doscontrol® 100% of the analyzed water samples
achieved the most strict disinfection level at the Spanish
demo site in Castell-Platja d’Aro (0 cfu E.coli/100ml) allowing
the use of reclaimed water for raw edible crops irrigation un-
der changing influent conditions ➞ Reliability
Additionally, results show a significant reduction of disinfect-
ant used:
•	 30% to 45% less sodium hypochlorite consumption at the
same disinfection level (dosage optimization) avoiding over-
dose and the undesired disinfection by-products formation
•	 15% to 50% (according to the operational conditions) less
power consumption by UV systems by optimizing the nº of
units in service and the power level
As a totally automated process, with doscontrol® less man-
power is needed and maintenance is properly managed al-
lowing appropriate service scheduling and easy equipment
fault diagnosis.
Perspectives for the future
As water reclamation specialized company, teqma is pro-
posing doscontrol® system to water reclamation managers
and water re-users in the Spanish and European market to
promote the positive experiences and results obtained in the
R3Water project demonstration in the Spanish and Swedish
demo sites helping to improve the reliability, efficiency and
effectiveness of water disinfection processes.
Contact
teqma@teqma.com
Chlorination labyrinth at Castell-Platja d’Aro WRP
UV disinfection system at Castell-Platja d’Aro WRP
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
19
Description
In the project different kinds of sewage sludges from differ-
ent plants of Aquafin were tested extensively.The major chal-
lenges were to find optimal and easily reproducible reaction
conditions for a variety of sludges and to develop recovery
technologies for valuables.
Addressed problems and challanges
Costs of treating wastewater treatment sludge with HTC and
AVA cleanphos technologies were assessed and compared
with current sludge treating practices. HTC technology car-
bonizes the sludge and improves its dewaterability. AVA
cleanphos technology recovers phosphorus from carbonized
sludge. Here carbonized sludge was considered to be used as
fuel for the cement industry. Possible higher-value end-uses
for the sludge were not assessed.
Hydrothermal Carbonisation (HTC)
AVA Green Chemistry Development (AVA) offers advanced technologies for the treatment of biomasses and waste
streams, based on the hydrothermal treatment technology (HTC). This technology allows the recovery of the most im-
portant ingredients such as potassium, calcium, magnesium, nitrogen, sulphate and the limited resource phosphate
as fertilizer (fertilizer production) while simultaneously producing high quality biocarbon or activated carbon e.g. as
soil improvement. This integrated approach is called “HTCycle”, showing hydrothermal carbonisation as a platform
technology for the circular economy with a zero waste approach.
Technologies Resource Recovery
TECHNOLOGIES – RESOURCE RECOVERY
20
The highest uncertainty on the costs of HTC and AVA clean-
phos treatments comes from the need of nitrogen retreat-
ment at the wastewater treatment plant. During HTC reac-
tion, around 60% of nitrogen content of the sludge dissolves.
The fraction of this dissolved nitrogen eventually returned to
the waste water treatment and it is one of the highest uncer-
tainties in HTC process and has high impact on total treat-
ment costs.
AVA developed a technical solution to extract nitrogen from
the filtrates, to recover nitrogen as nutrient ammonium sul-
fate. Therefore, costs for nitrogen treatment in WWTP are
reduced substantially. This development is implemented in
first full scale plant.
Features and benefits
During the project AVA achieved several important improve-
ments along the process chain of HTC:
Improvements in the Core process of Hydrothermal Car-
bonisation
•	 Reduction of acid consumption in the core process
•	 Improvement of carbon-efficiency in the core process by re-
cycling process water
•	 Improvement of carbon-efficiency in the core process by re-
cycling process water
•	 Reduction of energy demand through intelligent heat and
material flow management in the core-process
•	 Increased throughput by reducing reaction time in the core
process
•	 Process control by pH-monitoring in the core-process
Phosphorus Recovery:
•	 Increased Phosphorous yield at lower pH-value
•	 Increased phosphorous yield at higher reaction temperature
Process Water Treatment:
•	 Increased efficiency in process water treatment through
pH-value management
•	 Increased efficiency in process water treatment through tem-
perature management
•	 increase in efficiency through intelligent material and Heat
flow management
Results
HTC treated sludge has significantly better mechanical de-
watering properties than the raw sludge. This lowers energy
usage in thermal drying, since there is significantly less wa-
ter to evaporate. This is an additional benefit of HTC and AVA
cleanphos technologies for cases where sludge is dewatered
at one location and transported for drying to another loca-
tion. If sludge was carbonized at the dewatering site, there
would be significantly less matter to be transported for dry-
ing. It should be noted that if the sludge is being dried by
conventional thermal drying, the air emissions differ from
the emissions of the carbonization of the sludge. In conven-
tional thermal drying, volatile organic compounds present in
the sludge are volatilized and subjected to the air, whereas
in carbonization little or no organic volatile compounds are
vaporized. Thus HTC and AVA cleanphos technologies are ex-
pected to have environmental benefits in comparison to the
thermal drying that is not assessed here.
Wastewater
treatment plants
HTCycle
Industry
AgricultureCities
Activated carbon
Energy
Sewage sludge
Wastewater
Energy
Energy
HTC-coal
Adsorbants
Phosphorous
recovered
Fertilizers
AVA’s integrated approach to the use of sewage sludge as a raw material
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
21
In all schemes, sludge treatment costs decrease as the frac-
tion of the sludge subjected to digestion increases. Digest-
ing breaks down one third of the organic matter and leads
to lower treatment costs. On the other hand, AVA has earlier
concluded that sludge with high organic content is best for
carbonization. Sludge with high organic content allows to
produce high quality coal, that is the key in the development
towards added value applications for sludge. Here it should
be kept in mind that the economic model does not assess
possible higher value uses for carbonized sludge.
AVA cleanphos technology extracts phosphorus as phos-
phoric acid from HTC treated sludge. In comparison with
thermal drying, HTC and AVA cleanphos processing introduc-
es added CAPEX but the total sludge treatment costs are at
the same or lower level. There is also an increasing pressure
coming from the legislation that requires phosphorus recov-
ery from sludge prior incineration. Thus it can be conclud-
ed that AVA cleanphos technology
provides a promising solution for
phosphorus recovery that is also
economically competitive.
All these improvements are ad-
ditional benefits to the existing
advantages of AVA’s HTC as a tech-
nology for an integrated sewage
sludge treatment. Economic analy­
sisshows,thatforafullfeaturedHTC
plant (50,000t/a), running 24/7 total
treatment costs for 1t of sewage
sludge (dry matter) are around 150 €,
whereas for a simple dewatering or
drying technology are in the range
of 250 €/t.
Perspectives for the future
The ongoing process in the EU to collect and treat the waste-
water in more and more European municipalities, produces
vast and fast growing amounts of sewage sludge. The last
collected data show a yearly production of 9,637 thousands
of tons in the EU28 countries. Sludge treatment and reuse
issues are getting more important for most European mu-
nicipalities and industries (such as sewage sludge disposal
companies, waste water treatment plants) due to changing
legislation and increasing costs. At present, there is no energy
efficient, environmentally and economically viable process
implemented for sludge disposal and the reuse of valuable
resources as phosphorus.
The most common disposal meth-
ods for sludge are spreading on agricultural soil, composting
and incineration. Spreading on soil entails on average the
lowest cost (around 15 €/ton), but it is not an available op-
tion in every EU28 countries, due to the different legislations
in
force, and its being banned due to safety concerns. Incin-
eration entails the highest costs, but is also considered the
safest disposal method at the moment. Therefore, it is fast
growing and widely adopted. However, it presents also tech-
nical difficulties, such as the low overall efficiency of the pro-
cess (sludge can contain up to 85% water, which renders the
process very inefficient), the
huge logistic efforts required to
transport the sludge to the incineration plants, or the dispos-
al of the ashes after the sludge has been incinerated.
Inthissituation,AVAaimsnotonlytotreatthesewagesludge,
but also to transform it into high value products such as fuel,
activated carbons for water treatment, recovery of phospho-
rus, soil remediation material, carbon sequestration schemes
and other applications (on the base of the circular economy
approach). The HTCycle process will turn the present sewage
sludge disposal from a costly process into an income-gener-
ating activity.

Contact
Stepan Kusche, CEO
s.kusche@ipi.ag
Plant concept with 12 vessels in 2 rows
TECHNOLOGIES – RESOURCE RECOVERY
22
Description
By pre-treating the ash effectively an enhanced leaching can
be obtained. The main challenge with leaching is that about
75% of the material still remains and must be disposed of in
some way. Furthermore, the residue of a leaching process is
acidic or alkaline depending on the process used, which can
change the classification of the waste material. This can have
an impact on the deposition costs. The leaching solution
needs significant processing to produce a clean product, but
since it recovers valuable phosphorus this is a viable route for
recycling nutrients in the future.
The main problem with the ash as a raw material is the small
particle size. In fertilizer applications this can lead to dusting,
and therefore the ash has to be granulated in some way be-
fore use. Sludge ash does not have hydraulic properties in
itself, which necessitates for the use of a hardening agent.
Potentially other ashes could be used as binders in this ap-
plication, further improving the recycling of the process. A
benefit in this application is the form of the phosphates in
the ash. Iron and aluminium phosphates are more sparing-
ly soluble than the calcium phosphates traditionally used in
fertilizers. Since the release of phosphates in forests is taken
care of by fungi the leaching is slower, and phosphate uptake
better.Therefore less eutrophication by run-off is observed. If
the granulation process is further optimized by making light
weight aggregate the particles will hold moisture better and
provide better growth substrate for the microbiota.
In mineral wool manufacture powder raw materials can also
be problematic, and therefore the ash may need to be made
into briquettes or granulated before use. This can raise the
costs for use of the material. Since the main benefit of the
material is its low cost this can be a significant burden. How-
ever, systems exist for the addition of powder raw materials
into the system which may allow for the addition of ash di-
rectly into the process.
Another issue with these types of application for the ash is
that the process must be located fairly close to the facility. If
the ash must be transported long distances the margins of
profit are quickly lost.
Results
Leaching results for the ash were typical for the field. About
80 % of the phosphates were extractable with traditional
Sludge ash valorization
Sludge ash valorization routes:
Traditional methods for leaching ash are enhanced with high impact milling (mechanochemical activation). By produc-
ing new surfaces through activation the leaching process can be accelerated significantly.
The ash may be used in processes where it contributes beneficial properties based on its chemistry. Even though the
ash is not viable as an agricultural fertilizer it can potentially be used as forest fertilizer.
Another process where ashes are beneficial is the manufacture of mineral wool. The melting properties of the ash are
good for this application, and phosphate that is in the ashes improve the properties in the process and the biocompat-
ibility of the product.
Other application fields for sludge ash are refractory materials where it functions as a flux and can contribute a desirable
size fraction for better density of the material. Often sludge ashes have been used in construction materials as a filler.
Milling equipment for the treatment of the ashes
Ash granulate
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
23
heap leaching processes. Grinding of the ash increased the
rate of the leaching and this is a viable pre-treatment of the
ashes in a leaching process. The ash had a high content of
iron (Fe) and aluminum(Al) which are known to be difficult to
remove. Results for the forest fertilization trials and mineral
wool pilot trials are pending.
Perspectives for the future
In the future as costs for deposition of waste materials rise
the incentive to recycle ash will rise. Ashes and slags have
many desirable properties, and an increased use of this type
of materials is both desirable and probable. In the future
manufacture processes will be planned with local raw mate-
rials from wastes in mind, and a more circular economy will
be implemented.
Contact
Renotech Oy, Bob Talling
bt@renotech.fi
Implementation of sludge ash valorization into a production line.
TECHNOLOGIES – RESOURCE RECOVERY
24
Applicability and pre-requisites
Improved control strategies are applicable in all side stream
Anammox reactors. This study is specifically targeted for the
following one-step Anammox treatment reactors operated
with suspended active sludge. The introduction of a more
advanced control strategy requires:
•	 A thorough follow-up of sensor conditions and adequate
maintenance
•	 An acceptable water quality, facilitated by a process that is
more robust and/or achieves better removal efficiencies
compared to simpler control strategies
Anammox
The anoxic ammonia oxidation (Anammox) process is a unique biological process for nitrogen removal, which allows
significant savings (up to 60%) in aeration demand compared to the classical nitrification/denitrification process. The
Anammox process has proven to be successful in ammonium-rich wastewaters at temperatures above 25°C. Reject
water from anaerobic digestion of sludge is an excellent stream to be treated by the Anammox process. Many WWTPs
already have an Anammox reactor to treat reject water from anaerobic digestion, but there is a need for advanced
control strategies to increase process robustness. The main objective within R3water is developing new algorithms for
dynamic Anammox control. These control strategies are tested and demonstrated at two pilot-scale Anammox reac-
tors in Sweden and Belgium, and the results are being compared.
Technologies Resource Efficiency
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
25
Features and benefits
•	 An increase of the process reliability, to reach effluent targets,
to let the biomass better adapt to inflow variations, and to
reduce cases of process failure (pumps or aeration)
•	 An improved know-how of the process, to extract informa-
tion on the biomass activity
•	 A dynamic process control, for a fast and adequate adjust-
ment of the reactor cycle
Operation and maintenance
For the implementation of an advanced control strategy, in-
stallation and maintenance of advanced sensors, connected
to a control system, are needed. Although these advanced
control systems come with their own operation and mainte-
nance needs, the goal is to reduce overall operator efforts by
improving the process robustness. Maintenance of connecting
equipment, such as pumps, stirrers and aerators, might be re-
duced since possible failures of these can be discovered earlier.
Results
Results – Belgian demonstration
For the Belgian demonstration, 5 control strategies were test-
ed and at last integrated:
1.	 Feed control based on ammonia, as baseline control
strategy. Ammonia was first determined by a proxy
measurement (conductivity), and subsequently by direct
measurement.
2.	 Feed control based on ammonia with‘free ammonia (FA)
inhibition’determination and mitigation.
3.	 Aeration control based on nitrite measurements. This
control strategy was implemented on top of the contin-
ued feed control. The aeration time was increased or de-
creased, to limit the build-up of NO2
-N at the end of the
aeration phase, which would favor growth of NOB.
4.	 Aeration time was extended by alkalinity dosage.
5.	 Process control targeting the NOB washout based on free
ammonia shocks.
The Anammox pilot was at first located in Leuven WWTP.
The Leuven centrate waters had a rather high COD/N ratio,
resulting in a poor Anammox performance. In July 2015, the
pilot was moved to Antwerpen-Zuid, resulting into feasible
Anammox operations. Process performances were boosted
by bicarbonate dosing as a source of alkalinity. The process
stability was impacted by sensor failure, which could only be
countered by intensive maintenance and manual follow-up
of the process. The process stability was as well impacted by
fluctuating influent nitrogen loads.
During the baseline period (ammonia-based feed control),
the pilot operated relatively stable with a TN removal of
75-80%. However, frequent NO2
-N accumulations were ob-
served, which can be detrimental to Anammox activity. Dur-
ing the aeration control phase, TN removal was stable at sat-
isfying removal percentages between 77-87%.
Feed control was optimized with more stable effluent ammo-
nia in the reactor. Free ammonia inhibition was also prevent-
ed, targeting the accumulation of NH4-N due to load varia-
tion of the centrifuges.
The application of ammonia shocks was also investigated
with determination of optimal FA exposure levels and con-
tact time. Results were tested in lab scale and implemented
in pilot scale. The purpose of this feature is the reduction of
temporary NOB residual activity.
Results – Swedish demonstration
The aim of the Swedish demonstration was to evaluate the
efficacy of redox potential combined with pH for controlling
the partial nitritation/Anammox process. The testing was
centred on three key variables (pH, ORP, and nitrogen load).
In addition to verification of the control scheme working to
an acceptable level, the study also sought to determine the
optimal set point for each of the three variables. The optimal
point was assessed from a variety of different response varia-
bles such as nitrogen removal efficiency and cost of nitrogen
removed.
No. of test pH Nitrogen load
(gN/m2
/d)
Redox (mV)
I 7 1 -70
II 8 1 -70
III 8 1 70
IV 7 1 70
V 7,5 2,5 0
VI 7 4 -70
VII 8 4 -70
VIII 8 4 70
IX 7 4 70
X 7,5 2,5 0
pH, Redox and nitrogen load in the test runs
Using a standard full-factorial design of experiments, with
two levels for each variable, eight different periods were
deemed necessary. In addition, two middle points were in-
cluded as a reference point for the other tests, which brought
the total number of periods to ten.
TECHNOLOGIES – RESOURCE EFFICIENCY
26
Stable operation and acceptable levels of nitrogen removal
(>80%) were achieved for three periods where the common
factor was an ORP value of 70 mV. The highest nitrogen re-
moval rate (83.7%) was found when the test conditions were
pH 8, nitrogen load 1 gN/m2
/d, and ORP 70 mV. The economic
performance of each period was also evaluated and it was
found that the optimal point, in terms of aeration and of the
three periods with sufficient removal efficiencies, was the
same as the optimal removal conditions except with a pH of 7.
A secondary test was performed in order to directly compare
the performance of ORP with dissolved oxygen (DO) as a
control parameter. It was found that DO significantly outper-
formed ORP under identical test conditions, yielding a higher
nitrogen removal rate (78.2% vs. 65.3%) as well as significant-
ly less aeration energy.
Perspectives for the future
A marketable control algorithm should rely on robust sensors
with a low risk of failure. In the Belgian demonstration case,
the control strategies relied on sensors that required auto-
mated sample filtration and determination of N-compounds,
required intensive maintenance and were prone to failure.
Additionally, an ideal Anammox control process should not
only be based on energy savings and N-removal. As societal
awareness towards environmental themes increases, a pro-
cess control must also be able to incorporate environmental
considerations in its system, such as greenhouse gas (N2
O)
emissions.
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
Contact
Klara Westling
klara.westling@ivl.se
Alessio Fenu
alessio.fenu@aquafin.be
Tom Wambecq
tom.wambecq@aquafin.be
Francis Meerburg
francis.meerburg@aquafin.be
27
Addressed problems and challanges
Between 45 and 75 % of the energy costs in aWWTP are spent
in the aeration of the biological reactor. The optimization of
this process is fundamental to decrease the operational costs
of the whole plant. Additionally, the optimization has to be
done without affecting the quality of the treated water that
has to accomplish with the UWWTD regulations.
OptimEDAR uses DO and Redox measures to determine the
status of the biological reactor calculating the Equivalent Or-
ganic Charge (EOC), a ‘virtual sensor’ that estimates the or-
ganic matter load in the bioreactor. By adjusting the timing
andoperatingconditionsoftheblowersaccordingtothestrin-
gent reactor’s oxygen requirements, the energy consumption
is optimised while allowing longer denitrification cycles.
Applicability and pre-requisites
The OptimEDAR solution is applicable for activated Sludge
WWTPs with biological reactor (concentric or carrousel), aer-
ated with up to 5 blowers (1 or 2 speeds). Better results are
achieved in plants where influent suffers a significant varia-
tion in organic matter load or plants designed for covering a
seasonal peak demand that are normally oversized.
•	 Recommended WWTP constructive features
–– Reactor where it is possible to establish a perfect mixture
hypothesis.
–– Enough power in the aeration system to absorb loads.
–– Stirring system independent from aeration.
–– High hydraulic times or presence of homogeniser.
•	 Conditions of the process
–– WWTP with a cyclical pattern of load.
–– Adequate daily load that does not saturate the operation
of the plant.
–– No optimised control: set points of oxygen, or control by
on-off time.
–– Excess of nitrates in the effluent.
Features and benefits
Features:
•	 Simple and robust.
•	 Add-in solution, easy to install, without interfering with exist-
ing automation
•	 Based on robust probes with low maintenance requirements
•	 It adapts to changes in influent load.
•	 Reliability and easy operation
Benefits:
•	 Reduction of operating costs.
–– Less energy consumption.
–– Less reagents consumption.
–– Less sludge treatment.
•	 Increase the quality of the effluent.
–– Restore balance in case of major changes occur in the influ-
ent or uncontrollable external conditions.
–– Stability of the biological reactor.
–– Removal of carbonic demand.
–– Increased removal of nitrogen content.
–– High performance on phosphorus removal.
•	 Improve operational efficiency.
–– Optimises the energy consumption.
–– Sludge stability, providing an optimal state for water treat-
ment.
Results
Within the R3Water project, the OptimEDAR demonstration
was held in Wijer (Belgium) (1,440 P.E., design flow max. 2470
m3 /day) and in Empuriabrava (Spain) (70.000 P.E., 16.000 m3
/day), as cases of study for a small plant in different climatic
conditions and a big plant with highly seasonality.
Empuriabrava WWTP belongs to Consorci Costa Brava (CCB)
facilities, a water agency in Spain that is in charge of 18 mu-
nicipal wastewater treatment plants, operated by the Em-
presa Mixta d’Aigües Costa Brava (EMACBSA). Empuriabrava
WWTP operators have been testing different control strate-
OptimEDAR
OptimEDAR is a low-cost aeration control system for WWTP, based on virtual sensing techniques that adapts the use
of the blowers to the organic load in the bioreactor, allowing energy savings (20% on average), longer denitrification
cycles, and improving the quality of the effluent.
TECHNOLOGIES – RESOURCE EFFICIENCY
28
gies for the aeration process during the lasts years. Thanks
to this situation, it has been possible to compare the Optim­
EDAR results with 3 other methods in terms of energy con-
sumption as well as the quality of the effluent. The results
obtained shows 20% less use of the blowers related to the
previous year.
After comparing the use of blowers related to flow and the
quality of the effluent we can conclude that the OptimEDAR
control is more efficient than the control by redox or time an
similar to ammonium control in terms of the quality of the
effluent. Nevertheless the operational costs of OptimEDAR
are much lower and robustness much higher compared to
ammonium control.
Wijer WWTP belongs to Aquafin NV that operates in Flanders
and collects & treats the municipal wastewater of around 5.5
million people equivalents, that is treated in 289 plants. Wijer
WWTP is characterized by its diluted charge, and the Optim­
EDAR was optimized to run under these conditions. After
this optimization, the results showed a strong improvement
of the energy balance of the aerators, with a reduction of
energy consumption about 10% compared to the previous
O2
-control method.
Perspectives for the future
OptimEDAR in Wijer and Empuriabrava will be transfered to
the regional agencies to continue with the operation. These
2 experiences will be used as success cases for the future
commercialisation strategy.
Contact
adasa@adasaproducts.com
OptimEDAR structure
Comparision to other control strategies.
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
Energy/Flow Energy/BOD Energy/COD Energy/TN BOD removal COD removal TN removal
Ammonia
control ✸ ✸ ✸ ✸ ✸ ✸ ✸
Redox control ✸ ✸ ✸ ✸ ✸ ✸ ✸
Time control ✸ ✸ ✸ ✸ ✸ ✸ ✸
OptimEDAR ✸ ✸ ✸ ✸ ✸ ✸ ✸
29
Description
The overall aim of the project is to design, implement and
validate a control structure for efficient WWT plant opera-
tion. The control structure will be based upon a Model Pre-
dictive Control (MPC) technology where a simplified process
model together with estimation techniques is used to mini­
mize a cost function. This cost function is represented by a
prediction of defined quality parameters related to a desired
set-point.
Applicability and pre-requisites
In the project setting, the MPC’s objective will be to enhance
the O2
set-point tracking in aerobic biological reactors while
reducing the operation costs (energy). Furthermore, distur-
bance rejection is another important capability of the MPC,
where the goal is to minimize the effect of flow and concen-
tration disturbances entering each aerobic reactor. The MPC
shall replace the existing PID controllers and have direct ac-
cess to the necessary manipulated variables (MV).
Advantages and disadvantages
The solution will optimize the treatment operation both in
a quality (purification) perspective and in terms of resources
usage (energy). The technology (concept) will be applicable
for a range of scenarios, possible with some model re-para­
meterization or re-configuration.
The technology will be relevant for a range of various plant
configurations. However, there will be some plant require-
ments related to instrumentation and actuators.
Typical MPC response into the prediction horizon Prediktor MPC block diagram
Model based predictive control
Model predictive control (MPC) has its roots in optimal control and has become the most popular advanced control
technology in the chemical processing industries. There are many variants of MPC controllers, both in academia and in
industry, but they all share a basic concept which is to use a dynamic model to forecast system behavior, and optimize
the forecast to produce the best decision - the control move at the current time. Models are therefore central to every
form of MPC. Because the optimal control move depends on the present state of the dynamic system, a second basic
concept in MPC is to use the past record of measurements to determine the most likely present state of the system.
Thirdly, most MPC controllers are able to account for constraints both in manipulated variables and states/controlled
variables through the formulation of the optimization problem. The foundation of MPC relies on the computation of
the sequence of future control moves, performed by solving the optimization problem. Only the first computed con-
trol move is implemented. The model based predictions are corrected using feedback information at each sampling
instant, before a new optimal sequence of the future control moves is computed, according to the receding horizon
principle.
TECHNOLOGIES – RESOURCE EFFICIENCY
30
Operation and maintenance
In operation, the solution will require limited O&M activities.
During operation, the solution will need to be monitored
as an integral part of the conventional automation system.
Related to maintenance, some model adaptations could be
required, especially related to changes to the physical plant
configuration.
Implementation and results
PlantSimulator:Alotoftimehasbeenspentonunderstand-
ing the complex dynamics and relations within the WWT and
evaluation of the existing research results and publications
regarding the control issues in WWT. A few available (both
commercial and freeware) simulators such as STOAT and Dy-
namo have been considered as an aid for design of control-
ler structure. However, these provided unsatisfactory results
due to challenging and complex configurations and data
requirements. Thus, the aim of the project changed towards
using in-house software for implementation of a simulator
that could describe the Swedish pilot plant.This has been ac-
complished through application of the well-known Activat-
ed Sludge Model 1 (ASM1).
Estimator: During evaluation of the simulator at site in
Stockholm, it became clear that fitting the simulator to the
plant can be a time-consuming task due to the large number
of parameters and states. With much support from the IVL
group, the simulator was validated through application of Ex-
tended Kalman filtering (EKF) which is a state and parameter
estimation technique. The EKF uses a reduced-order ASM1
model as its internal model in addition to the available on-
line measurements. The reason for this model reduction has
been the lack of observability of the complete ASM1 model,
which is an essential pre-requisite for estimation capability of
the system. Finally, a platform now exists for online real-time
dynamic simulations of the pilot plant, that is a simulation
running in parallel with the plant, and using the same inputs
and outputs. One additional benefit of this is the possibility
to try out new strategies and changes in the way the pilot
plant is operated such as changing the number of reactors,
Comparison of results from bioreactor 5
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
31
where and how the recirculation is done, and other interest-
ing ideas. Furthermore, this platform is the base for applying
advanced control systems with much less effort than before.
Controller design: Several approaches and strategies have
been considered and even partially implemented. These
approaches have mainly focused on finding a proper mod-
el for the model-based controller (MPC). After gaining val-
uable process insight through the simulations, a simplified
model was designed to be used in the MPC with the aim of
controlling the dissolved oxygen level in a single bioreac-
tor. This has been successfully implemented and tested in
closed-loop at Swedish pilot plant. That means, the MPC has
replaced the PID-controller for one reactor using both data
from the simulator (states and parameters) as well as the esti-
mated dissolved oxygen in the same reactor. As the figures in
previous page illustrate, the MPC shows better performance
in terms of set-point tracking (keeping the level of dissolved
oxygen close to 2 mg/L) and disturbance rejection (the same
disturbance occurs for both the PID and the MPC structure).
Future enhancements: Further enhancements of the MPC
have been considered. Examples include control of the oxy-
gen content of bioreactor 4 (BR4), amount of sludge recycled
in the system, and economic optimization of the air blower
volume flow to the aerators in the bioreactors. All these en-
hancements can be implemented within the current frame-
work.
Perspectives for the future
Based on the simulation and experimental results obtained
during this project, it is obvious that using an advanced con-
trol strategy (such as combining nonlinear state and para­
meter estimation technique and nonlinear model predictive
control) can be economically beneficial.That means, keeping
the different material concentrations (such as O2
) at appro-
priate levels while using the energy resources more efficient-
ly. Considering the developed platform by Prediktor during
the R3water project, the commercial potential of such pro­
duct is considerably high, in addition to increased interest
from academic institutes (such as universities) for possible
research studies. Thus, it opens up the possibility for numer-
ous research and commercial activities within WWT, specially
focusing on modelling and controller aspects of the process.
Contact
Thomas Pettersen
thomas@prediktor.no
TECHNOLOGIES – RESOURCE EFFICIENCY
32
Adressed problems and challenges
Aquafin faced some challenges at the Girona WWTP:
•	 A complex blower algorithm needed to be upgraded with a
new parametrization as to increase lifetime.
•	 The primary settling tank was modelled in function of differ-
ent parameters, validated in full scale and its malfunctioning
integrated in the model.
•	 Air distribution through the 4 aerated basins did not seem to
follow the diffusers surface distribution. The data collected in
full scale did not alleviate the uncertainty on this aspect.
•	 Eventually, high saving opportunities were identified due to
the actual continuous aeration in the biological tanks.
•	 A malfunctioning of the sludge thickeners was identified by
establishing a detailed sludge mass balance, and was later
solved by the plant operators.
Applicability and pre-requisites
The model-based energy audit tool can be used to:
•	 Select plant-wide scenarios (pumping strategies, sludge and
water line interactions, etc.) to reduce energy consumption,
costs, and CO2
emissions
•	 Complete realistic cost assessments (peak demands, optimal
contracted power, etc.)
Model-based energy audits in wastewater
treatment plants
The total operation costs of a wastewater treatment plant (WWTP) are, for a large part, determined by its electricity
consumption. Energy audits can identify opportunities to reduce energy use inWWTPs, but they cannot pinpoint ways
to optimize energy use. Only a model based approach with robust multi-variate data analysis can deal with such com-
plexity. Aquafin has developed a model-based energy audit tool that integrates water and sludge dynamic models
with a detailed modelling of all single process units and a correct model parametrization. By means of a detailed data
analysis, the model output can be used to determine: a robust parameter set, critical operations of blowers and other
unit processes, total costs and single cost components, life cycle analysis, and detailed cost- and energy-saving strate-
gies. This whole-plant modeling tool of Aquafin is demonstrated through the R3 Water project at the full-scale WWTP
of Girona (Spain).
(Left) Effect of new blower parametrization on overall plant performance in Girona. (Right) Bivariate plot to screen scatter plots as to improve
parameters set robustness
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
33
The tool requires:
•	 High-quality data of the design and operation of the WWTP
•	 Highly qualified personnel for correct use and interpretation.
Technical support can be offered by the model developers
Features and benefits
•	 Evaluate multiple energy-saving strategies without affecting
the process
•	 Evaluate future scenarios for planning
Operation and maintenance
The model-based approach has to be updated every time
there is a significant change in plant configuration or in envi-
ronmental conditions.
Constrained combinatorial parameters scenario
analysis:
Scenario analysis is pursued by combining several param-
eters that are involved in the modelling, putting constrains
where necessary. The parameters are chosen to pursue op-
timization according to experience and real practice. Para­
meters vary in range and steps to which the model outcomes
are sensitive. Data analysis results in a bi-dimensional scatter
plot with each point representing one simulated year (with a
specific parameters dataset). Scatter plot coordinates repre-
sent process performances, i.e. cost, energy and water quality
performances. All parameter impacts are analyzed towards
each single process unit and overall plant performance.
Multi-variability analysis allows to maximize reliability of unit
processes, choose a robust set of parameters, and optimize
towards specific parameters and overall performance.
Results
To model the Girona WWTP, Aquafin used data from the
year 2013 (January-October). The yearly dynamic data were
fitted with regards to: effluent quality, primary settling tank
effluent concentrations, removal performances, sludge pro-
duced, and power consumption of each different compart-
ment. Data are evaluated considering an overall ‘yearly cost’,
because energy savings can be counterbalanced by, for ex-
ample, increased sludge production or reagents costs.
The evaluated scenarios include actions that are: (I) opera-
tions based, such as solving the thickener malfunctioning, or
reducing the MLSS concentration; (II) control-based, such as
optimizing the blowers algorithm, DO sensor position, exter-
nal recycle control; (III) based on on-line nitrogen control; or
(IV) a combination of these. The outcomes are summarized
in the table above.
Perspectives for the future
The outcomes of the modeling exercise will be communicat-
ed to the operators of the respective WWTPs, to allow them
to make informed decisions to improve the energy and cost
balance of their plant.
Aquafin is bringing their modeling and support service to
the market. Factors that influence the marketability include
(Left) Blowers switch on-off minimization in function of actual parameters. (Right) N controlled scenario results with sensitivity towards NH4-N
TECHNOLOGIES – RESOURCE EFFICIENCY
34
the practical applicability of the outcome to the specific
situation, the risk of failure of the proposed improvements,
the impact of the proposed improvements on effluent water
quality, and the achieved economic benefit.
Contact
Alessio Fenu
alessio.fenu@aquafin.be
Francis Meerburg
francis.meerburg@aquafin.be
Results of the scenario analysis, showing improvements in TN removal and operational costs for different non-invest-
ment and investment measures. The baseline scenario had an operational cost (over 300 days) of € 507,000 Euro and
TN removal of 90.2%.
Scenario description TN
% Removed
Cost
€ 1000
Comment
Process operation improvement
Thickener +1.0 -60 Excluded from all other scenarios
MLSS reductin +1.5 -5 Reduced of 600 mg SS/L
No Investment Cost foreseen
Optimization +(0.0-0.3) -(15-25) External recycle, improved blower control, MLSS reduction
Investment Cost foreseen
N on-line control +(0.5-1.0) -(55-65) External recycle, improved blower
Re-arranging grids -(2.5-3.5) -(35-50) 200 diffusers are placed from AER1 to NOAER3
N on-line control +(1.0-2.0) -(110-125) External recycle, improved blower + MLSS reduction +
Thickener improvement
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
35
Addressed problems and challanges
Wastewater treatment plants spend up to 45% of their op-
erating costs on electricity. Plants generate a lot of data, but
usually don’t have the tools to answer important questions
such as“How much energy do we consume?”,“How could we
save money on electricity?”. ICRA has developed InnoWatt,
a tool that gives you the clear and reliable information you
need to reduce energy costs. The process starts simple by in-
stalling InnoWatt in the electricity counter of your facility. Us-
ing four modules, InnoWatt tells you how much energy you
are using and how you can save money.
•	 Module 1: The first module gives you access to real-time
energy consumption. You can access historical data and
visualize your consumption patterns
•	 Module 2: The second module calculates your energy costs
in real-time, so you don’t need to wait for your monthly bill to
know the cost of energy consumed.
•	 Module 3: The third module gives you the optimal contract-
ed power for your plant, which can allow you to save thou-
sands of Euros without changing any infrastructure. Most
plants have contracted more power than they need, so by
lowering the contracted power, your plant can save money.
•	 Modul 4: Whole plant modeling. In the last module ICRA will
simulate your wastewater treatment plant and run scenario
analyses for energy and cost reduction. We will show you
how to operate the plant with less energy without sacrificing
the quality of treatment.
Applicability and pre-requisites
•	 For small WWTPs we recommend the usage of Modules 1 to 3.
For medium to large WWTPs we recommend the full poten-
tial of InnoWatt (Modules 1 to 4). The return of investment
will be shorter as the size of the facility increases.
•	 For the whole plant modeling (Module 4 of InnoWatt)
high-quality data of the design and operation of the WWTP
is needed. The most tedious step in the modeling exercise is
data collection and verification. The better the quality of the
data, the more reliable the model outcomes and the more re-
alistic the proposed interventions to improve the functioning
of the facility.
•	 For installing InnoWatt in the electricity counter there is no
special pre-requisit, as the technology is compatible to most
of counter brands.
Features and benefits
Thanks to InnoWatt, you have full control of your energy con-
sumption. The main benefit a facility can gain is the reduc-
tion of energy consumption, costs and CO2
emissions while
maintaining good process performance. InnoWatt allows
you to:
•	 Highlight critical situations where peak demand charges are
driving up energy costs.
•	 Develop strategies to reduce energy consumption and maxi-
mize energy production at peak time-of-use periods.
•	 Find the optimal contracted power for a specific plant.
•	 Evaluate aeration and pumping strategies.
•	 Study the interactions between the sludge line (with high
nutrient loads in the return stream) and the liquid line.
InnoWatt
One of the largest urban consumers of energy are wastewater treatment plants. Within a WWTP, electricity consump-
tion accounts for between 25 and 45 % of the facility’s total operating costs.WWTPs are therefore important targets for
reducing energy demand. Energy audits, which identify opportunities to reduce energy use and greenhouse gases in
WWTPs, are typically based on the average energy consumption of a facility; they include benchmarking with similar
plants or comparison against some standard performance indicators. However, current energy audits could potentially
be improved through the use of energy and cost monitoring tools together with dynamic models that integrate water
and sludge lines. Because this potential had not been explored in the European market, ICRA developed InnoWatt, a
novel energy audit tool that was demonstrated through R3Water. The main goal of ICRA’s technology is to minimize
energy consumption while maintaining good process performance.
TECHNOLOGIES – RESOURCE EFFICIENCY
36
•	 Assess the use influent organic content (to maximize either
nutrient removal or biogas production).
•	 Assess the upgrade of the system for biological phosphorus
removal
Operation and maintenance
Hardware and software is needed for the usage of InnoWatt.
An optical sensor is used to connect to the electricity coun-
ter. That sensor is also connected to a data management sys-
tem that allows visualizing all information from the counter
in a web. Once installed, no maintenance is needed for this
device. Module 4 is a service offered by ICRA which requires
large effort the first time the model is built for a specific facil-
ity. Once the model is ready it should be properly maintained
(with little effort) any time there is a significant change in the
configuration of the facility or in the environmental condi-
tions such as influent wastewater composition, electricity
tariffs, etc. If the company managing the WWTP has qualified
personnel to run the model, best is that they maintain the
model following some recommendations from ICRA. If not,
maintenance can be entirely executed by ICRA.
Results
Girona WWTP: A model-based treatment performance and
energy audit of the Girona WWTP in Spain was conducted
using advanced and fully dynamic air supply models. The
focus of the study was on the aeration system, which rep-
resents 63% of the plant’s energy consumption. A dynamic
model consisting of a process, a realistic controller, and a
very detailed air supply model, was developed and calibrat-
ed to be used as the baseline for testing various scenarios.
Results show that the implementation of an ammonia-based
controller and a redistribution of the diffusers led to energy
savings between 12 and 21 %, depending on wastewater
temperature. In addition, the model demonstrated that the
current blower is too large, which causes an intermittent
behaviour, endangering the equipment and shortening its
life-time, plus limiting the minimum air-supply. The applied
aeration system models enable engineers to identify bottle-
necks by modelling equipment constraints (e.g. blower turn-
down). Ignoring the air supply side in an assessment could
result in an overestimation of energy savings or treatment
performance and consequently in non-optimal control solu-
tions or equipment selection. The carbon footprint assess-
ment showed that direct N2
O and CH4
emissions from the
biological reactor are of the same magnitude as indirect CO2
emissions from electricity use. Hence, efforts should not be
only allocated to reduce electricity consumption but also di-
rect emissions.
Harelbeke WWTP: ICRA developed an integrated model of
the Harelbeke WWTP. The model was used to find strategies
to enhance Biological Phosphorus Removal in order for the
plant to reduce resource consumption. Currently phospho-
rus is removed chemically and thus 400 Tn·year-1 of FeCl3
are
used. The evaluated scenarios included decreasing the flow-
rate of return activated sludge, adding an internal recycle
from the aerobic zone to the anaerobic zone and adding an
external source of volatile fatty acids. Based on the simula-
tion results we recommend that the Harelbeke plant imple-
ments the reduction of the return activated sludge flowrate
to 50 % of the influent flowrate. Without any capital invest-
ment or other direct costs to the plant, this modification
could reduce the energy consumption of blowers by about
7 % and the consumption of FeCl3
solution by about 40%,
while maintaining an effluent quality that meets Belgium’s
current regulations.
Contact
Lluís Corominas
lcorominas@icra.cat
Ignasi Rodríguez-Roda
irodriguezroda@icra.cat
Mehlika Ayla Kiser
akiser@icra.cat
InnoWatt installation in the electricity counter Module 4. Whole plant modeling & scenario analysis
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
37
Addressed problems and challanges
Many industrial processes can be improved if the method of
transfer from gas to liquid was more efficient. Wastewater
treatment and Anaerobic Digestion are such processes. Per-
lemax has developed a microbubble technology which has
low power requirements allowing increased gas transfer with
no energy penalty. The R3Water project gave the company
the opportunity to build upon its experience of scaling up
from laboratory and pilot level operations. This was to con-
firm that microbubble technology could allow a significant
reduction in energy comsumption whilst maintaining the re-
quired performance in waterwater treatment plants. The jus-
tification for the experiments was that power requirements
for wastewater treatment across Europe are considerable
and have been estimated at € 750 m per annum.
Anerobic Digestion was also investigated to see if perfor-
mance could be improved whereby more methane gas is
produced and the sludge is more stable. These experiments
were conducted with CO2
instead of Oxygen.
Applicability and pre-requisites
The sites chosen wereWWTP Aarteslaar in Belgium and Ham-
marby Sjösatdsverk in Sweden as being a scale up from ex-
periments already carried out.
However, measurement of power reduction was not been
possible and any measurement has been on the basis of the
KLA technique usually intended for clean water. The basis
for successful implementation was based on several factors
which can vary all of which will vary depending on the waste-
water treatment facility being used. These are feedback loop
length, oscillation frequency, airflow rate. A direct and timely
measurement method is to measure bubble size. This will al-
low optimum of the three factors compared to bubble size.
The technology consumes no additional power as it works on
the airflow used in a process. There is no need for a individu-
al control system as performance will be measured through
SCADA systems.
Operation
The technology uses flu-
idic oscillators which di-
vert the air flow before it
reaches the diffuser and
modifies the bubble cre-
ation.
Results
First experiments were carried out by “above water oscilla-
tion” with the fluidic oscillator positioned outside the waste
water tank.
The results showed little difference in efficiency using this
technique and was considered to be due to a difference in
pipe design between already tested sites in the UK and Aqua-
Fluidic oscilliation
By using fluidic oscillation microbubbles can be generated, which significantly improve gas transfer to liquids.
Picture showing oscillator in centreComparison of the bubble sizes
Schematic diagramme of the
microbubbles technology
TECHNOLOGIES – RESOURCE EFFICIENCY
38
fin’s facility specifically a design that equalizes air flow. Above
water oscillation was originally pursed because it would al-
low retrofit in any wastewater treatment plant.
To overcome the design for air flow equalization an oscilla-
tor design that is not positioned above water but within the
wastewater tank was investigated. The device has been nick-
named the TOAD. It featured all the requirements of a fluidic
oscillator but on a much smaller scale and included 2 diffusers
as part of the device.
This has been tested at the Swedish site and produced a sig-
nificant improvement in oxygen transfer of 53%.
In an anaerobic digestion laboratory experiments, when a
reactor was dosed with CO2
microbubbles the methane pro-
duction increase by over 100% and the stability of the sludge
was improved.
(2.02g DO/m3
air)
(3.08g DO/m3
air)
View of the oscillators
Comparison of dissolved oxygen (DO)
per m3
air
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
39
The over 100% improvement level was not replicated in
the test facility at Aarteselaar, NL, but an improvement was
shown. One of the major differences between laboratory
and the first test was direct dosing of the CO2
directly into the
reactor achieved in the laboratory but not in the test tanks.
This is a major consideration in any retrofit programme as it
is likely to change the design of the AD tanks substantially.
Testing at IVL is ongoing at the time of publication of this
brochure and further research is to be funded by Innovate
UK after the R3Water project is complete.
Perspectives for the future
The potential for this technology is significant but further
larger scale tests are required. These tests are in planning
and will take place later in 2017.
Contact
Graeme Hitchen
graeme@perlemax. com 
Hammarby test facility in Sweden
TECHNOLOGIES – RESOURCE EFFICIENCY
40
Environmental Technology Verification (ETV) is a tool to
help innovative environmental technologies reach the mar-
ket. Special focus is on highly dynamic and innovative Small
and Medium-sized Enterprises (SMEs). Claims about the per-
formance of innovative environmental technologies can be
verified by qualified third parties called “Verification Bodies”.
The “Statement of Verification” delivered at the end of the
ETV process can be used as evidence that the claims made
about the innovation are both credible and scientifically
sound. With proof of performance credibly assured, inno-
vations can expect an easier market access and/or a larger
market share and the technological risk is reduced for tech-
nology purchasers.
The idea of the R3Water project was not only to demonstrate
innovative technologies, but also to show an innovative
“R3 demonstration concept” (Reviewed – Referenced –
Recognized) that makes use of the concept of Environmen-
tal Technology Verification (ETV). Compared to conventional
projects this concept secures a more parallel and direct mar-
ket acceptance in European countries making use of ETV and
LCA (Life cycle assessment)/Life cycle costs (LCC).
The concept of ETV and the links to the EU ETV Pilot Pro-
gramme and ISO standard (ISO 14034) on ETV were directly
integrated in the demonstration of the technologies in the
project, reducing the need for extra testing.
Three verifications were foreseen in the R3Water project. One
technology was already successful: from the field of“Reuse of
water” the technology AQUATRACK® from Aqua-Q, Sweden,
has got the EU ETV“Statement of Verification”.
The online monitoring technology AQUATRACK® has been
demonstrated successfully and was verified at the same time
leading to the Verification statement in dec 2016.
Further aquaBio from ADASA, Spain (monitoring for water
reuse) and HTC (Hydrothermal Carbonisation) for sludge
valorisation, from AVA, Germany (“Resource recovery”) have
started to go through a verification procedure under the EU
ETV Pilot programme.
Experiences with EU ETV Pilot Programme
Review
Technology
Demonstration
EU ETV Pilot-
Programme
International
Working Group ETV
Market Acceptance
in ETV accepting
countries
Referenced Recognised
LCA
LCC
ETV
Recommendations for efficient technology verification:
•	 Spend time to prepare claims and select standards in which the verification will be performed.
•	 Compare quotations from different actors and talk to responsible persons and make clear who will do what.
•	 Make sure that the verification body has no previous connection to the project or any other way to your organisation.
It is important to have an impartial verification body.
•	 Try to answer the EU commissions questions regarding the verification in a simple and friendly manner.
•	 Make sure that the test body is accepted by the Verification body and fulfils requirements by the ETV scheme.
The R3 demonstration concept
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
Microbubbles
Model-based
energy audit
Model predictive
control
AquaBio
Doscontrol
Aquatrack
Anammox
Anammox
control system
Sludge
Sludge Incineration
Ashes
Product processing
concept for
incinerated sludge
ash valorization
HTC
Ozone disinfection
system
Biogas
Quality
controlled
reclaimed water
Treated water
TM
Microbubbles
OptimEDAR
Water reuse
Resource recovery
Resource efficiency
Wastewater
Technologies for:
Removal of
pharmaceutical
residues
41
Demo Sites
Location of technologies at the WWTP
DEMONSTRATION SITES
42
Demonstration has been mainly performed in the Consorci
Costa Brava (CCB) facilities, a water agency in Spain that is in
charge of 20 regional wastewater treatment plants, operated
by the Empresa Mixta d’Aigües Costa Brava (EMACBSA). CCB
is a consortium created in 1971 by the 27 coastal municipal-
ities of Girona’s province in northeastern Spain to provide
services and to manage infrastructures related to the whole
water cycle, from the drinking water supply (as wholesale
purveyor) to the wastewater treatment and to the production
and supply of reclaimed water to cover non-potable demands.
The resident population in the whole area is estimated in
some 250,000 inhabitants, with a seasonal increase in sum-
mer that can reach above 1 million people and that requires
the facilities to be designed to provide the adequate servic-
es in the peak period. Since 1989, one of CCB’s activities is
the reclamation of treated effluents in 14 facilities and their
supply to cover non-potable demands of different kind
(3.1 milion m3
/year in 2012, with a maximum in 2010 reach-
ing 6.4 milion m3
/year).
WWTP Empuriabrava
WWTP Empuriabrava
Empuriabrava WWTP is located in the area of “Aiguamolls
de l’ Empordà”, a national park which is the second largest
wetland in Catalonia between the confluence of the rivers
Muga and Fluvia. It is the prime habitat for wildlife, especially
aquatic birds
This plant has an estimated flow around 16,000 m3
/day to
treat an equivalent population of 70,000 PE and receives the
wastewater from Empuriabrava, a touristic neighbourhood
belonging to Castelló d’Empuries. The treatment carried out
at this facility is a biological treatment with nitrogen removal
and phosphorus removal and a constructed wetland tertiary
treatment.
WWTP Castell – Platja d’Aro
Castell – Platja d’Aro WWTP receives the wastewaters from
the surrounding municipalities of Castell d’Aro, Platja d’Aro,
Sant Feliu de Guixols and Santa Cristina d’Aro.
The plant was designed for an average capacity of 35,000 m3
/
day, and 175,000 PE. However this WWTP is affected by high
seasonality influenced by the tourism in the area. The treat-
ment line in Castell- Platja d’Aro WWTP consists on a primary
treatment, secondary treatment with conventional activated
sludge and a tertiary treatment.
WWTP Castell – Platja d’Aro
The tertiary treatment is designed for a 15.000 m3
/day flow,
meaning that only part of the water from the secondary clar-
ifier is further treated for reuse. The rest of the effluent is dis-
charged into the Ridaura river and the Mediterranean sea.
WWTP Girona
The Girona facility is an activated sludge WWTP that has the
capacity to serve 275,000 PE. The WWTP was constructed in
Demonstration sites in Spain
WWTP Girona
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
43
1986 but was upgraded in 2008. The old biological reactors
and secondary settlers (not used now) were substituted by
new ones. From the three lines for the biological reactors
they are currently using two of them.
The WWTP Girona is operated by Tractament de Residus I
Aigües Residuals de Girona, SA (TRARGISA).
WWTP La Bisbal d’Empordà
La Bisbal d’Empordà Wastewater Treatment Plant belongs to
Water Agency of Catalonia.
La Bisbal d’Empordà WWTP is located in the area of El Baix
Empordà, and receives the water from the municipalities of
La Bisbal d’Empordà, Castell d’Empordà, Corçà, Cruïlles, Mo-
nells, Sant Sadurní de l’Heura and Forrallac.
Plant influent consists of municipal wastewater, and waste-
water from livestock and smaller industries plant has a ca-
pacity to treat waste water from neighbouring counties of
Girona of about 3,200 m3
/d.
The wastewater treatment plant is placed with a container-
ized ZeeWeed MBR system. This MBR ultrafiltration mem-
brane system has a nominal pore size of 0.04 µm, which pro-
vides a physical barrier to bacteria, parasites and viruses.
At La Bisbal d’EmpordàWastewaterTreatment Plant there are
two parallel MBR ultra filtration lines which run sequential as
per a standard operating procedure.
Wastewater is treated on continuous basic day and night
throughout the year. Main treatment consists of ZeeWeed
hollow fibre MBR process.
TheWWTP La Bisbal d’Empordà is operated by AQUAMBIENTE.
Container of ZeeWeed MBR system
Concept of the WWTP La Bisbal d’Empordà
DEMONSTRATION SITES
44
Aquafin owns and operates 298 wastewater plants in Bel-
gium, varying in size and composition. Therefore, each tech-
nique can be demonstrated in an appropriate setup. Seven
innovative solutions for reuse of water, recovery of valuable
substances and resource efficiency are demonstrated.
WWTP Aartselaar, pilot reactors and small-scale
WWTP
The pilot testing will be done in Aquafin’s demo-site in Aart-
selaar, Belgium. For the case of fluidic oscillation, pilot exper-
iments were performed in an 8.6 m³ clean-water pilot tank
(aerobic oscillation tests) and two parallel 1.3 m³ digester
tanks (anaerobic oscillation). The small-scale WWTP, located
parallel to the full-scale WWTP of Aartselaar, has a size of 140
m³, which corresponds to 1,000 PE. This small-scale biore-
actor was used for the case of fluidic oscillation. It was ide-
al to perform aeration tests in a fully operational activated
sludge basin, which require interruption of the process and
can therefore not be performed at a full scale WWTP without
endangering the effluent quality.
Brugge: WWTP and incineration plant
Brugge: Mono-incineration plant
The treatment plant of Brugge treats 265,000 people equiva-
lents, which makes it the largest plant of the Flemish region.
The incineration plant is of the mono-incineration (i.e., only
municipal sludge incinerated), fluidized bed type. The ashes
of the Brugge incineration plant were used for the case of
resource recovery from ashes. Because all practical work was
performed at the Renotech facilities, a container filled with
20 metric tons of ashes was shipped to Finland.
WWTP Antwerpen-Zuid
WWTP Antwerpen-Zuid is connected to household and in-
dustries for about 190.000 people equivalents. The WWTP is
composed of pre-treatment, anaerobic compartment, aero-
bic tanks (4 tanks with alternating scheme), 9 clarifiers. This
is the location of the Anammox pilot plant, which treats the
liquid fraction of the sludge digestate of the plant.
Aeration basins and secondary settlers of WWTP Antwerpen-Zuid
WWTP Harelbeke
The WWTP of Harelbeke (116,000 PE) consists of a classical
activated sludge process. After the usual mechanical screen-
ings, the water is sent through a sand trap, travels through
an anaerobic zone, then undergoes aeration, and is finally
settled in circular settling tanks before being discharged in
the nearby receiving watercourse. This plant is used as a case
study for the whole-plant modeling study.
WWTP Wijer
The tests will be performed at Aquafin’sWWTP inWijer (1,600
PE), a full-scale WWTP that started operating from the end of
2013 onwards. This plant was used to demonstrate the Opti-
mEDAR aeration control system.
WWTP Mechelen-Noord
For the demonstration of hydrothermal carbonization (HTC)
of Aquafin sludges, municipal waste sludge of the WWTP of
Mechelen-Noord was used. This plant treats wastewater of
88,000 PE. The sludge has excellent characteristics for HTC
treatment, because the plant removes phosphorus through
the Bio-P process, there is no anaerobic digestion, and the
sludge has a low silt content. A total of 10 metric tons of sludge
was transported from Mechelen-Noord to the industrial-scale
plant at Karlsruhe (Germany) for the HTC experiments.
Demonstration sites in Belgium
WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
R3 water newsletter_06_2017_final_web
R3 water newsletter_06_2017_final_web
R3 water newsletter_06_2017_final_web
R3 water newsletter_06_2017_final_web

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R3 water newsletter_06_2017_final_web

  • 1. Water in the circular economy – innovations for urban water treatment Reuse of water – Resource recovery – Resource efficiency www.r3water.eu This project has received funding from the European Union’s Seventh Programme for research, technological development and demonstration under grant agreement No 619093.
  • 2. 2 Coordinator: Uwe Fortkamp Email: uwe.fortkamp@ivl.se Phone: +46 (0)8598 56304 Klara Westling Email: klara.westling@ivl.se Phone: +46 (0)8598 56431 IVL Swedish Environmental Research Institute Vallhallavaegen 81 11427 Stockholm Sweden www.ivl.se WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 3. 3 R3Water: Getting all the value from wastewater 6 Policy Brief 4 R3Water Partner 5 Technologies 7 Reuse of Water 7 aquaBio 7 AQUATRACK® & ozone polishing 10 doscontrol® 17 Resource Recovery 19 Hydrothermal Carbonisation (HTC) 19 Sludge ash valorization 22 Resource Efficiency 24 Anammox 24 OptimEDAR 27 Model based predictive control 29 Model-based energy audits in wastewater treatment plants 32 InnoWatt 35 Fluidic oscilliation 37 Experiences with EU ETV Pilot Programme 40 Demo sites 41 Location of technologies at the wastewater treatment plant 41 Demonstration sites in Spain 42 Demonstration sites in Belgium 44 Demonstration site in Sweden 45 Table of Contents CONTENTS
  • 4. 4 Removing pollutants is of course a priority at wastewater treatment plants, yet there is a growing awareness that they could also act as resource facilities, providing energy, nutri- ents and other valuable resources. This is the goal of the EU FP7 funded project R3Water (“Demonstration of innovative solutions for Reuse of water, Recovery of valuables and Re- source efficiency in urban wastewater treatment“) with the idea to support the transition from being purely a treatment plant towards a Water Resource Recovery Facility (WRRF). Focus in the project is to develop and test solutions for up- grading existing treatment plants and to improve resource efficiency combined with the implementation of new tech- nologies and business models. In order to reach this target R3 Water developed and demon- strated innovative technologies at three sites (Belgium, Spain, Sweden) within 3 areas: • Resource efficient treatment, e.g. by efficient aeration and optimised process control • Facilitating water reuse, e.g. by improved water quality moni­ toring and efficient disinfection • Recycling of nutrients and other valuables, e.g. by valorisa- tion of sludge Facilitating market uptake has been one of the project objec- tives. All of the technologies and solutions being developed have made progress during the project. Some of them are al- most ready to market, and some technologies are being ver- ified according to the EU ETV-scheme, with one technology where verification has finished. This innovative “R3 demon- stration concept (Reviewed – Referenced – Recognized)” se- cures a more parallel and direct market acceptance in Euro- pean countries and at the same time reduces the need for extra testing. Further project results have been disseminated to relevant stakeholder groups via different channels like workshops, brochures, homepage, LinkedIn etc. The strong consortium, led by IVL Swedish Environmental Research Institute, involves 12 part- ners from seven European countries with a well-balanced ratio between innovative SMEs, research institutes and a high skilled advisory board. It ensured a rapid adoption of the SMEs innovative water and recovery solutions. This brochure provides you with the results out of R3Water.   R3Water: Getting all the value from wastewater Reuse of water Demo Spain Recycling of valuables R3Water Demo Sweden Resource efficient treatment Demo Belgium Review Technologies Demonstration Environmental Technology Verification (ETV) Market acceptance in ETV acceptance countries Market acceptance at global market Referenced Recognized LCA LCC ETV Future wastewater treatment: resource facilities for water, nutrients and energy Three areas (3 R’s) and tree demonstration sites in R3Water Innovative“R3 demonstration concept (Reviewed – Referenced – Recognized)”: technologies undergo a verification in the EU ET V Pilot programme in parallel to the demonstration at the demo sites WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 5. 5 Common suggestions • Provide incentives to overcome reluctance to make investment caused by short-time operating contracts that act as a barrier for the market uptake of innovative technologies. • Ease the market uptake of new and innovative technologies – by simplifying the permission process for demonstrations at industrial sites, e.g. by using the concept of “transition peri- ods”. For innovative technologies start with an entry level of requirement, requiring increased level of performance from the technology to prove its veracity. – by applying a holistic assessment: a better sustainability performance might need less strict (water) thresholds • Use careful wording and terminology in official documents, as certain expressions create positive attitudes, while other with about the same meaning create rather negative. Reuse of water • Although the benefits of water reclamation and reuse for irrigated agriculture (and other uses) are clear, there are still doubts about the economic sustainability of reclaimed water services. Consider the reclaimed water as an additional local water resource in the scope of the integrated urban/regional water cycle, rather than an isolated service provided by the WWTP. • Harmonize quality criteria for water re-use including methods for quality monitoring as a driver for the marketing of water reuse technologies (e.g. common standard within the EU). • Online water quality monitoring technologies are not properly considered in EU Directives. Allow for innovation in monitoring tech- nologies within the EU water directives review by taking the available online monitoring/detection technologies and the potential for an effective combination with water quality monitoring methods (online + conventional sampling/analysis) into consideration. Resource recovery • Support the market for recovered resources by harmonizing legislation and directives. There is a need of for such harmonized standards for recovered materials and products to make a foothold in the market dominated by virgin materials. • Innovation partnership for the combination of research and procurement: more promotion to be enacted by member states and public authorities. Resource efficiency • Stimulate the adoption of technologies by using incentives to establish sustainability benchmarks. This will help to balance medium and long-term sustainability of increased resource efficiency and plant sustainability; with short-term economic cost disadvantages. The whole“Report about policy and directive implementation”will be available on r3water.eu. Policy Brief summary
  • 6. 6 R3Water Partner WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT CONSORTIUM ADASA Sistemas S.A.U., Spain (www.adasasistemas.com) Aquafin N.V., Belgium (www.aquafin.be) Aqua-Q AB, Sweden (www.aqua-q.se) AVA Green Chemistry Development GmbH, Germany (www.ava-co2.com) DECHEMA Gesellschaft für Chemische Technik und Biotechnologie e.V., Germany (www.dechema.de) Renotech OY, Finland (www.renotech.fi) ICRA Catalan Institute for Water Research, Spain (www.icra.cat) IVL Swedish Environmental Institute, Sweden (www.ivl.se) Perlemax Ltd, UK (www.perlemax.com) Prediktor AS, Norway (www.prediktor.no) Teqma Tecnologias y equipos para el medio ambiente S.L., Spain (http://teqma.com/) VTT Technical Research Centre of Finland, Finland (www.vtt.fi)
  • 7. 7 aquaBio Description E. coli is a bacteria widely used as an indicator of fecal con- tamination. Its presence warns about a potential sanitary risk. This aspect is reflected in the Directive 2006/7/EC on the quality of bathing water. The Escherichia coli and total coliform parameters are also key indicators and essential for determining the potential uses of reclaimed water from the tertiary treatment of a WWTP and it is present in existing Na- tional Water Reuse Directives (ES, IT, FR, GR, CY) as well as in most of worldwide regulations. However, traditional sampling plus laboratory method takes from 24h to 96h to obtain the results, becoming useless for early warning purposes. aquaBio can provide the results be- tween 3h and 12h (depending on the microorganism con- centration) in automatic way, and to transmit this informa- tion to a local control center or remote on duty staff. Addressed problems and challanges The goals in the project were to demonstrate the operational autonomy, the reliability and robustness of the equipment running in a continuous way, and to obtain enough lab anal- ysis to contrast with the automatic results in order to launch an ETV verification process. During the project, the mainte- nance requirements were decreased from the initial once a week to a final once a month. aquaBio provides an early warning about a potential sanitary risk through the simultaneous measurement of E.coli and total coliforms in a continuous and automated way, with low maintenance requirements. Technologies Reuse of Water
  • 8. 8 Applicability and pre-requisites aquaBio is applicable for reclaimed water uses, bathing water anddrinkingwater.aquaBiomanagesautomaticallythesample intake as well the disinfection until the intake point. The pre- requisites are an electric power connection and one sampling point. Features and benefits Features: Measurement principle: • Fluorimetric detection for Escherichiacoliex. 365 nm em. 450 nm • Colorimetric detection for total coliforms abs 405 nm • Reagents used: Colilert-18® from IDEXX in liquid form • Biocide solution Detection limit: • Escherichia coli: <1 bacteria in 100 ml • Total coliforms : <1 bacteria in 100 ml Minimum analysis time: From 3 to 12 hours, depending on the microorganism concen- tration. Benefits: • Early warning in case of the water reclamation plant malfunc- tioning. • Efficient production of reclaimed water, avoiding overdosing of disinfection chemicals and excess of UV power consumption. • Production of fit-for-purpose reclaimed water, according to the intended water quality for the reuse in irrigation of veg- etables, wood crops, golf courses or other industrial uses. Operation and maintenance aquaBio stands out for its high autonomy and its low cost in maintenance operations. Only one maintenance operation per month has to be performed in order to ensure its correct operation. Results The aquaBio has been demonstrated in two different demos- ites. Castell d’aro water reclamation plant (outlet and inlet), a Spanish demosite, and in Hammary Sjöstadsverk (MBR outlet), the Swedish demosite. Sample testing: Different samples were compared to the IDEXX laboratory methodology using colilert- 18® concluding that there are not significant differences between aquaBio result and the labo- ratory result. Independence between samples: In order to check the independence between samples, sterile samples were interspersed during the standard operation. As a result it was demostrated that none cross contamination exists between one sample and the following one. Correlation between samples analysed by the aquaBio and laboratory (colilert-18®) Sterile samples interspersed during operational period WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 9. 9 Performance: During all the operational period different operation modes were tested: by time, by digital imput or alarms. The Castell Platja d’Aro water reclamation plant runs on demand. The aquaBio was connected to the valve that starts the process, and the following graphics shows the low demand in winter and the increase of demand during spring. Maintenace operations: Currently the maintenance opera- tions are performed once per month (30 minutes) thanks to the improvements implemented during the project in the hy- draulics and software as well in the maintenance procedures. Perspectives for the future One of the key priorities for the EC in the upcoming years is to increase the ratio of water reuse in the EU, while ensuring the health and environmental safety of water reuse practices and the free trade of food products. Nevertheless, this priority faces several barriers that prevent the adoption of the re- claimed water for different uses: agriculture, urban, industrial and recreational. In order to tackle some of these barriers, the EU has launched a process for the definition of the guidelines on minimum quality requirements for water reuse for agriculture and aquifer recharge, where E. coli is the recommended bacterial indicator. In this context, the online monitoring of microor- ganisms with aquaBio can contribute to the efficiency of the water reclamation processes as well as on building trust on end-users. The next goal is to demonstrate the aquaBio for drinking wa- ter use and to adapt the equipment for measuring Entero- cocci in bathing waters. Contact adasa@adasaproducts.com AquaBio adaptation to on demand water reuse aquaBio Decrease in the frequency of the maintenance operations. TECHNOLOGIES – REUSE OF WATER
  • 10. 10 Technology 1 – AQUATRACK® AQUATRACK® is a real time online monitoring and sampling system for pathogens in treated wastewater for reuse and re- claimed water. The system consists of multiple conventional water quality sensors including an optical laser sensor which detects all possible forms of variations caused by contamina- tion (natural, human error, process failure) in reclaimed and recycled water. The system can commu- nicate wireless and access data remotely. The software creates a dynamic fingerprint of effluent water based upon the micro contaminants/mi- cro particles/micro debris in the effluent water. When the fingerprint deviates the sys- tem automatically captures relevant water sample that can be analyzed for positive identification of pathogens. AQUATRACK® is now EU ETV certified for moni- toring and sampling of drinking water, reuse and reclaimed water. Addressed problems and challanges The main source of contamination comes from purified or insufficiently purified wastewater, both industrial and small- scale private sewage discharge. It pollutes rivers, lakes, wa- ter bodies, and coastal waters and creates potential risk of microbial contamination in drinking water, bathing water, groundwater, etc. The emerging environmental problem in the developed coun- tries is pharmaceutical residues in purified or insufficiently pu- rified wastewater both from municipality and industries. To eliminate the contamination and pollution there are con- ventional wastewater treatment processes. The treatment of wastewater is a high-energy consuming and releases green- house gases. Wastewater discharge contains contaminants like bacteria, parasites, virus and pharmaceutical residues etc. Contaminated sludge is another problem in wastewater treatment. The treated wastewater is not fully reused in wa- ter scarcity areas today. To solve the above mentioned problem of contamination in the effluent water many new and modified different tech- nologies/processes are being developed like MBR, MBBR and SBR. etc. These membrane technologies have well defined cut off. The effluent discharge is used for reuse or reclaimed water in agriculture and ground water recharge. IntheR3WaterProjectAqua-Qdevelopedanoveluser-friend- ly, intelligent real time on-line monitoring and sampling sys- AQUATRACK® & ozone polishing Online optical monitoring of contaminants and ozone polishing Aqua-Q developed two separate novel standalone technologies for safe reuse of effluent water: 1) On-line real time optical (laser) contamination monitoring and automatic sampling system for effluent water coming out of MBR, MBBR and SBR process. The system, AQUATRACK® - Early Warning System with automatic sampler, is now EU ETV certified. 2) Composed an automatic, self-contained modular ozone polishing system for online or batch application to eliminate pharmaceutical residues and pathogens present in treated waste water (effluent) from MBR, MBBR, and SBR process. Both of these innovative technologies are performing well as standalone and have been demonstrated successfully. The idea is now to combine these technologies on a digital platform so that it can internally exchange and gather information from each other and will act on demand. Ozone polishing will be actuated on demand by AQUATRACK® to remove contaminants from effluent and provide safe and clean water for reuse. The novel ozone polishing system is used on the effluent water from the MBR process and differentiates from other waste water treatment technologies where they use ozone either in the beginning or in the middle of the MBR process. That is why ozone polishing needs less ozone and there is no need for an active carbon filter (GAC). Both of the technologies are patented. AQUATRACK® WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 11. 11 tem, AQUATRACK®, which is used for real time quality moni- toring of the effluent from a MBR process in Stockholm and now in Spain. The aim is to give the management of a treat- ment plant early warning for sudden changes/deviations in effluent water quality. These changes are having high proba- bility of microbiological growth due to contamination that is harmful to environment, rivers, lakes and contains also drug residues among other organics. AQUATRACK® is designed to monitor effluent quality 24/7 af- ter MBS, MBBS, SBR and conventional treatment process and collection of water sample when there is high risk for patho- gens in the effluent discharge. Applicability and pre-requisites Applicability process of AQUATRACK® is user-friendly and fol- lows the 4 simple steps, see picture to the right: 1. Connect a side flow of the effluent water to the inlet of AQUATRACK® and get a fingerprint of your water stream and always access the water quality changes on the lo- cal monitor or get the results wireless. 2.-3. Decide a highest amount of water quality variations of your process water and get alarmed when variation occurs. 4. The variation that trigger the alarm is automatically sampled and stored for further analysis • Monitoring of wastewater effluent from MBR, MBBR, SBR and after conventional waste water treatment process. • Monitoring and quality control of industrial water treatment process • Monitoring of drinking water reservoir, networks, source/lake water Pre-requisites: • The equipment needs to be placed inside a room having nor- mal room temp 20°C and 230/240 V AC electrical plug with floor drain. A partial constant flow of about 4-5 l/min of the effluent to be monitored with an open/stop valve at a pres- sure of 2-3 bar. Features and benefits Benefits of AQUATRACK®: 1. Most cost effective and accurate monitoring system for immediate detection of MBR, UF, NF and RO filters break through and alarms operator for the event with time and date. Records all incidents. Clear economical benefit. 4 steps of the applicability process of AQUATRACK® TECHNOLOGIES – REUSE OF WATER
  • 12. 12 2. Creation of individual fingerprint of different non-con- taminated water helps preventing building of biofouling by identifying contamination in time. 3. Early warning to an operator of a treatment plant for mi- cro particles/micro debris exceeding the set limits in the effluent. Always generate alarm when there is deviation from stable water quality. 4. Operator can establish periodic pollutant profile (e.g. dai- ly/monthly/yearly profile of micro contaminant presence in water) and hence optimize treatment process. 5. Captures automatically water sample for biological & chemical analyses: i.e. water sample captured right at the time of the observed anomaly gives high confidence on analysing results. 6. Helps protecting the environment in a sustainable way. Safe re use of treated waste water brings value in life. Operation and maintenance • AQUATRACK® can be easily installed without making any changes to the existing treatment process. Installation starts working from day 1 (plug and play). • Maintenance is simple and does not require much time. Results The graph below represents an overview of level of contam- inants as fingerprint in the MBR effluent water and is repre- sented in two clusters. Cluster 1 represents bacteria size and cluster 2 represents size of parasites.This graph also indicates that at about 10.30 am some anomaly happened and that anomaly returned to normal around 16.30 pm. 10.30 to 16.30 was a critical period for the process. Overview of level of contaminants as fingerprint in the MBR effluent water, represented in two clusters Thegraphbelowillustratesareal-timeexampleofAQUATRACK® monitoring of treated wastewater. The increased values trig- gering the automatic sampler is plotted against the number of Heterotrophs (Total Count) measured by MBS MultiReader. A correlation of 86% between the triggered alarms and bac- teria count was found. Above shows an overview of average mean values collected by AQUATRACK® from July 2016 until April 2017 from MBR effluent at WWTP La Bisbal d’Empordà, Spain. Above shows the variations during one day of the effluent quality from MBR process at WWTP La Bisbal d’Empordà, Spain. Real-time example of AQUATRACK® monitoring of treated wastewater Overview of average mean values collected by AQUATRACK® from July 2016 until April 2017 from MBR effluent at WWTP La Bisbal d’Empordà, Spain. Variations during one day of the effluent quality from MBR process at WWTP La Bisbal d’Empordà, Spain. WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 13. 13 Perspectives for the future The ETV verification shows that AQUATRACK ® can be used to keep continuous track of biological contaminants in drinking water, source water, and treated wastewater (MBR effluent). It can also be used to keep record of contaminants (e.g. mi- cro-debris, biological contaminants, planned/unplanned dis- charge of wastewater treatment plant). This performance can be considered as an important feature of an environmental monitoring technology. Information from AQUATRACK® can be used to make intel- ligent decisions about the amount and kind of disinfection, hence avoiding over-disinfection and thus saving money. AQUATRACK® can establish daily, monthly, and seasonal contamination patterns which can be used to improve the efficiency of a treatment process, thus saving electricity and chemical costs. AQUATRACK® gives real-time warning of possible contamina- tion events, which can help to avert epidemics, and costs & liabilities associated with epidemics. AQUATRACK® can be claimed as an innovative and novel ear- ly warning system of monitoring and sampling for pathogen detection in drinking water and reclaimed water. Technology 2 – Ozone polishing system to eliminate pharmaceutical residues and pathogens Aqua-Q has developed/composed a modular ozone pol- ishing system and has successfully demonstrated that in a cost-effective way with a minimum dose of ozone both phar- maceuticals residues and pathogens can be totally removed beyond the limit of detection. This online ozone polishing pilot system is fully automatic and self-contained. Only a partial flow of effluent water from MBR process and 230 – 240 V AC electric plug is required for plug and play. Local industrial regulations have to be maintained to comply with government regulations. Addressed problems and challanges Water pollution/contamination from pharmaceutical resi- dues are the major environmental challenge in aquatic envi- ronment in many developed and emerging countries. Drug residues from human and animal consumption through the sewage system reach lakes and rivers that have become a global environmental problem. Current drugs collide with the requirements of sustainable development. Pharmaceuti- cal consumption in society is increasing. 50-60% of this con- sumption ends up in our water environment. Many of these drugs are found in our drinking water, source/lake water, aquatic life, bathing water, and ground water etc. Even though the concentrations of these pharmaceutical compounds are low concentrated (nanograms per litre lev- els), no one really knows exactly the long-term exposure ad- verse consequences affecting human health and aquatic life. Scientists still arguing about the current state of the various drug substances that can interact with each other and form hazardous substances. Therefore, there is the need to devel- op methods to eliminate these dangerous drug residues in each treatment plants before discharging the effluent water to nature or using it as reclaimed water. Stringent legislation and control is required. To solve this challenge, sophisticated technologies have been developed and are commercially used in the treatment of wastewater (both municipal and industrial) like MBR (Mem- brane Bio Reactor) and MBBR (Moving Bed Bio Reactor) etc.. Even though pharmaceutical compounds were found in the effluent from a MBR process (see below under results). Ozone polishing system TECHNOLOGIES – REUSE OF WATER
  • 14. 14 Aqua-Qs innovative solution is online real time monitoring and sampling of the contaminants (early warning) and in real time eliminating that by ozone polishing so that safe and clean treated wastewater can be reused without quick pos- itive identification of type of contaminants. Applicability and pre-requisites To eliminate both the drug residues and pathogens in treat- ed wastewater (effluent from MBR) Aqua-Q developed / composed a cost-effective self-contained ozone polishing process. Ozone is a strong oxidizing gas and spontaneously reacts with organic substances and eliminates pathogens. Mixing of ozone gas and effluent water by creating micro bubbles and obtaining a stable ozone water solution is our key success factor. This innovative ozone polishing process treated effluent from the MBR at Hammarby Sjöstadsverk in Stockholm. The ozone polishing step removes totally drug residues below the limit of present detection limit and totally inactivates bacteria and other pathogens found in municipal and industrial effluent water. The treatment also reduces the TOC and color of the effluent water (see picture below). The ozone gas and the effluent water is mixed in a closed circu- lation tank. Once the dissolved ozone concentration has ob- tained the pre-determined value the water is discharged to outlet. Right: effluent from MBR process. Left: effluent water after after ozone polishing This modular ozone polishing system is automatic and self-contained with oxygen generator, ozone generator, re- action vessel, off gas destruction, efficient mixing of gas and water with all the necessary instruments to monitor the pro- cess stability. In Combination with AQUATRACK® the ozone polishing tech- nology is a power full tool to remove pharmaceutical resi- dues and pathogens with real time online quality control for reuse of water. The patented novel process set-up is a future process system. Pre-requisites: The equipment needs to be placed inside a well-ventilated room having normal room temp 20°C and 230/240V AC elec- trical plug with floor drain. A partial constant flow of about 14-16 l/min of the MBR effluent is fed to the system with an open/stop valve at a pressure of 2-3 bar. There should be an ambient monitor for ozone gas leakage. Features and benefits Ozone polishing is a most cost-effective system to eliminate both pharmaceutical residues and pathogens in the same treatment coming out from a MBR system. 1) Our ozone polishing cost effectively eliminates both pharmaceutical residues and pathogens in effluent water with minimum dissolved ozone 0.08 ppm. 2) Require no secondary treatment with active carbon as no by products are observed. 3) Our empirical experience confirms with that if we main- tain a stable treatment process no costly pharmaceutical analyses is required on regular basis for prioritized drug residues as above. 4) Properly applied at correct position on a waste water treatment process ozone is a most environmental and ef- fective tool to decompose organic substances and path- ogens in the effluent and can have GRAS status. Operation and maintenance 1) As ozone, modular system is skid mount and complete with system set up only electricity 230 – 240V AC is required. 2) Effluent water at room temp or if possible lower tempera- ture is required along with discharge possibilities. 3) Operation is plug and play. 4) The system complies with all national industrial standards including national environment regulations. Results The table and graph below illustrates some of our results of active pharmaceutical residual substances found in the ef- fluent of MBR process that has been effectively removed by ozone polishing step below the limit of detection. WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 15. 15 Before ozone After ozone Substance Mode of action ng/L ng/L Diclofenac Anti-inflammatories 601 <14 Furosemide Diuretics 957 <11 Hydrochlorothiazide Antihypertensives 1660 <2.8 Ibuprofen Anti-inflammatories 71 <10 Naproxen Anti-inflammatories 37 <4.6 Ramipril Antihypertensives <5.6 <5.6 Warfarin Anticoagulants 6,9 <4.9 Atenolol Antihypertensives 120 <3.7 Amlodipine Antihypertensives <3.6 <3.6 Bisoprolol Antihypertensives 32 <5.2 Caffeine Stimulant 17 <15 Carbamazepine Sedatives 265 <2.1 Citalopram Antidepressants 216 <6.5 Fluoxetine Antidepressants 8,8 <6.0 Ketoprofen Anti-inflammatories 68 <7.2 Metoprolol Antihypertensives 585 <6.6 Oxazepam Sedatives 402 6,6 Paracetamol Anti-inflammatories 28 <11 Propranolol Antihypertensives 68 <4.4 Ranitidine Antiulcers 72 <21 Risperidone Antipsychotic <22 <22 Sertralin Antidepressants <6.5 <6.5 Simvastatin Lipid-regulating <8.3 <8.3 Terbutaline Asthma medication 13 <2.4 Analysed at IVL Stockholm (<) lowest quantifiable limit (LOQ, S/N=10) Samples RT 30°C 37°C Organic carbon (mg/l) Color at 410nm Control 13*10^2 16*10^2 15*10^2 12.5 0.008 Treated 1 0 0 0 10 0.005 Treated 2 0 0 0 10.5 0.004 Treated 3 0 0 0 10 0.005 Removal of bacteria from MBR effluent by ozone polishing Removal of pharmaceuticals and bacteria from MBR process. Active pharmaceutical residual substances with/ without ozone polishing. TECHNOLOGIES – REUSE OF WATER
  • 16. 16 Perspectives for the future Reuse of water is essential in many parts of the world as pop- ulation grows and demand for fresh clean and safe water increases. Reuse of treated wastewater with quality control provides hope and opportunity for people as water shortage has become a global problem not only in emerging countries but also in developed countries. There is a need for future new EU legislation to ensure high clean and safe reuse water standard not only a minimum standard for reuse of water as discussed today. From innovative technology perspective, Aqua-Q strongly believes on future European standard for stringent quality control of reuse of treated wastewater for filling the aquifers, irrigation and other applications. Real time online monitor- ing of contaminants of effluent is necessary to protect en- vironment and our common water bodies. Aqua-Qs contri- bution is a process set-up (see overview scheme) which will ensure a cost effective combined processes to monitor the contaminants in the effluent and eliminate the contaminants by ozone polishing the effluent. Membrane Bio Reactor Effluent AQUATRACKTM Quality Assurance Ozone Polishing Necessaryparameterswillbe analysedforprocessoptimization Final effluent free from pathogens and pharmaceutical residues Aqua-Qs process set-up Contact Sudhir Chowdhury sudhir@aqua-q.se Ulla Chowdhury ulla@aqua-q.se www.aqua-q.se WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 17. 17 Addressed problems and challanges Reclaimed water is obtained from treated wastewater, a chal- lenging effluent strongly influenced by upstream wastewa- ter treatment processes with a highly variable concentration and composition in time of the physiscal chemical and mi- crobiological quality directly affecting the effectiveness and reliability of disinfection processes. Disinfection agents and techniques used in water reclamation have been commonly adopted from drinking water treatment (i.e. Chlorine dioxide, Sodium Hypochlorite, UV radiation, Ozonation). Combined disinfection (e.g. synergetic use of UV radiation and chemical oxidation) is a solution for effective disinfection in drinking water and reclaimed water and its being used in several full scale sites. Although the combination of complementary disinfectant agents generates synergies broadening the dis- infection spectrum, affecting pathogens that are not inacti- vated by conventional chemical oxidizers as chlorine at the normal concentrations (i.e. spore forming bacteria, viruses and protozoa) while ensuring a residual concentration of dis- infectant in the disitribution network, these processes lack an effective and optimal contol system in order to ensure: • Reliable operation, flexible against variable conditions • Maximum synergies, cost optimization delivering the mini- mum dosage to achieve the requiered disinfection level • Continuous safe water production doscontrol® is an automatic controller specifically desiged to ensure effective disinfection in drinking water treatment and water reclamation delivering the needed amount of each disinfectant agent to continuously produce safe water while optimizing the amount of UV dose and chlorine dos- age reducing costs and environmental footprint. Applicability and pre-requisites doscontrol® can be applied into new or existing disinfection treatments in water reclamation for reuse and other water disinfection schemes (drinking water, recreational water, ir- rigation, aquaculture etc). Features and benefits • Totally automated process • Adjusted dose of disinfectant (physical and chemical) to pro- duce safe water at the optimal cost. • Fit-for-purpose production of reclaimed water, according to the required water quality (irrigation, environmental and in- dustrial uses) • Valuable real time information of the disinfection process • Reduction in O&M associated costs • Reduction of chemical associated risks as disinfection by- products doscontrol® doscontrol® is an innovative technology developed by teqma to control the water disinfection process. Based on the optimized combination of chemical and physical disinfection, the controller is able to generate positive synergies de- livering enhanced wide-spectrum microbiology load reduction and substantial operational costs reduction for a safe reclaimed water production. doscontrol® system TECHNOLOGIES – REUSE OF WATER
  • 18. 18 Operation and maintenance The system provides valuable on-line information and data management for a proper disinfection equipment (e.g. UV and chlorination) and a preventive and corrective mainte- nance management. Besides, the operator can decide to use doscontrol® or change to the previous operational mode if desired. Results Thanks to doscontrol® 100% of the analyzed water samples achieved the most strict disinfection level at the Spanish demo site in Castell-Platja d’Aro (0 cfu E.coli/100ml) allowing the use of reclaimed water for raw edible crops irrigation un- der changing influent conditions ➞ Reliability Additionally, results show a significant reduction of disinfect- ant used: • 30% to 45% less sodium hypochlorite consumption at the same disinfection level (dosage optimization) avoiding over- dose and the undesired disinfection by-products formation • 15% to 50% (according to the operational conditions) less power consumption by UV systems by optimizing the nº of units in service and the power level As a totally automated process, with doscontrol® less man- power is needed and maintenance is properly managed al- lowing appropriate service scheduling and easy equipment fault diagnosis. Perspectives for the future As water reclamation specialized company, teqma is pro- posing doscontrol® system to water reclamation managers and water re-users in the Spanish and European market to promote the positive experiences and results obtained in the R3Water project demonstration in the Spanish and Swedish demo sites helping to improve the reliability, efficiency and effectiveness of water disinfection processes. Contact teqma@teqma.com Chlorination labyrinth at Castell-Platja d’Aro WRP UV disinfection system at Castell-Platja d’Aro WRP WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 19. 19 Description In the project different kinds of sewage sludges from differ- ent plants of Aquafin were tested extensively.The major chal- lenges were to find optimal and easily reproducible reaction conditions for a variety of sludges and to develop recovery technologies for valuables. Addressed problems and challanges Costs of treating wastewater treatment sludge with HTC and AVA cleanphos technologies were assessed and compared with current sludge treating practices. HTC technology car- bonizes the sludge and improves its dewaterability. AVA cleanphos technology recovers phosphorus from carbonized sludge. Here carbonized sludge was considered to be used as fuel for the cement industry. Possible higher-value end-uses for the sludge were not assessed. Hydrothermal Carbonisation (HTC) AVA Green Chemistry Development (AVA) offers advanced technologies for the treatment of biomasses and waste streams, based on the hydrothermal treatment technology (HTC). This technology allows the recovery of the most im- portant ingredients such as potassium, calcium, magnesium, nitrogen, sulphate and the limited resource phosphate as fertilizer (fertilizer production) while simultaneously producing high quality biocarbon or activated carbon e.g. as soil improvement. This integrated approach is called “HTCycle”, showing hydrothermal carbonisation as a platform technology for the circular economy with a zero waste approach. Technologies Resource Recovery TECHNOLOGIES – RESOURCE RECOVERY
  • 20. 20 The highest uncertainty on the costs of HTC and AVA clean- phos treatments comes from the need of nitrogen retreat- ment at the wastewater treatment plant. During HTC reac- tion, around 60% of nitrogen content of the sludge dissolves. The fraction of this dissolved nitrogen eventually returned to the waste water treatment and it is one of the highest uncer- tainties in HTC process and has high impact on total treat- ment costs. AVA developed a technical solution to extract nitrogen from the filtrates, to recover nitrogen as nutrient ammonium sul- fate. Therefore, costs for nitrogen treatment in WWTP are reduced substantially. This development is implemented in first full scale plant. Features and benefits During the project AVA achieved several important improve- ments along the process chain of HTC: Improvements in the Core process of Hydrothermal Car- bonisation • Reduction of acid consumption in the core process • Improvement of carbon-efficiency in the core process by re- cycling process water • Improvement of carbon-efficiency in the core process by re- cycling process water • Reduction of energy demand through intelligent heat and material flow management in the core-process • Increased throughput by reducing reaction time in the core process • Process control by pH-monitoring in the core-process Phosphorus Recovery: • Increased Phosphorous yield at lower pH-value • Increased phosphorous yield at higher reaction temperature Process Water Treatment: • Increased efficiency in process water treatment through pH-value management • Increased efficiency in process water treatment through tem- perature management • increase in efficiency through intelligent material and Heat flow management Results HTC treated sludge has significantly better mechanical de- watering properties than the raw sludge. This lowers energy usage in thermal drying, since there is significantly less wa- ter to evaporate. This is an additional benefit of HTC and AVA cleanphos technologies for cases where sludge is dewatered at one location and transported for drying to another loca- tion. If sludge was carbonized at the dewatering site, there would be significantly less matter to be transported for dry- ing. It should be noted that if the sludge is being dried by conventional thermal drying, the air emissions differ from the emissions of the carbonization of the sludge. In conven- tional thermal drying, volatile organic compounds present in the sludge are volatilized and subjected to the air, whereas in carbonization little or no organic volatile compounds are vaporized. Thus HTC and AVA cleanphos technologies are ex- pected to have environmental benefits in comparison to the thermal drying that is not assessed here. Wastewater treatment plants HTCycle Industry AgricultureCities Activated carbon Energy Sewage sludge Wastewater Energy Energy HTC-coal Adsorbants Phosphorous recovered Fertilizers AVA’s integrated approach to the use of sewage sludge as a raw material WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 21. 21 In all schemes, sludge treatment costs decrease as the frac- tion of the sludge subjected to digestion increases. Digest- ing breaks down one third of the organic matter and leads to lower treatment costs. On the other hand, AVA has earlier concluded that sludge with high organic content is best for carbonization. Sludge with high organic content allows to produce high quality coal, that is the key in the development towards added value applications for sludge. Here it should be kept in mind that the economic model does not assess possible higher value uses for carbonized sludge. AVA cleanphos technology extracts phosphorus as phos- phoric acid from HTC treated sludge. In comparison with thermal drying, HTC and AVA cleanphos processing introduc- es added CAPEX but the total sludge treatment costs are at the same or lower level. There is also an increasing pressure coming from the legislation that requires phosphorus recov- ery from sludge prior incineration. Thus it can be conclud- ed that AVA cleanphos technology provides a promising solution for phosphorus recovery that is also economically competitive. All these improvements are ad- ditional benefits to the existing advantages of AVA’s HTC as a tech- nology for an integrated sewage sludge treatment. Economic analy­ sisshows,thatforafullfeaturedHTC plant (50,000t/a), running 24/7 total treatment costs for 1t of sewage sludge (dry matter) are around 150 €, whereas for a simple dewatering or drying technology are in the range of 250 €/t. Perspectives for the future The ongoing process in the EU to collect and treat the waste- water in more and more European municipalities, produces vast and fast growing amounts of sewage sludge. The last collected data show a yearly production of 9,637 thousands of tons in the EU28 countries. Sludge treatment and reuse issues are getting more important for most European mu- nicipalities and industries (such as sewage sludge disposal companies, waste water treatment plants) due to changing legislation and increasing costs. At present, there is no energy efficient, environmentally and economically viable process implemented for sludge disposal and the reuse of valuable resources as phosphorus.
The most common disposal meth- ods for sludge are spreading on agricultural soil, composting and incineration. Spreading on soil entails on average the lowest cost (around 15 €/ton), but it is not an available op- tion in every EU28 countries, due to the different legislations in
force, and its being banned due to safety concerns. Incin- eration entails the highest costs, but is also considered the safest disposal method at the moment. Therefore, it is fast growing and widely adopted. However, it presents also tech- nical difficulties, such as the low overall efficiency of the pro- cess (sludge can contain up to 85% water, which renders the process very inefficient), the
huge logistic efforts required to transport the sludge to the incineration plants, or the dispos- al of the ashes after the sludge has been incinerated. Inthissituation,AVAaimsnotonlytotreatthesewagesludge, but also to transform it into high value products such as fuel, activated carbons for water treatment, recovery of phospho- rus, soil remediation material, carbon sequestration schemes and other applications (on the base of the circular economy approach). The HTCycle process will turn the present sewage sludge disposal from a costly process into an income-gener- ating activity.
 Contact Stepan Kusche, CEO s.kusche@ipi.ag Plant concept with 12 vessels in 2 rows TECHNOLOGIES – RESOURCE RECOVERY
  • 22. 22 Description By pre-treating the ash effectively an enhanced leaching can be obtained. The main challenge with leaching is that about 75% of the material still remains and must be disposed of in some way. Furthermore, the residue of a leaching process is acidic or alkaline depending on the process used, which can change the classification of the waste material. This can have an impact on the deposition costs. The leaching solution needs significant processing to produce a clean product, but since it recovers valuable phosphorus this is a viable route for recycling nutrients in the future. The main problem with the ash as a raw material is the small particle size. In fertilizer applications this can lead to dusting, and therefore the ash has to be granulated in some way be- fore use. Sludge ash does not have hydraulic properties in itself, which necessitates for the use of a hardening agent. Potentially other ashes could be used as binders in this ap- plication, further improving the recycling of the process. A benefit in this application is the form of the phosphates in the ash. Iron and aluminium phosphates are more sparing- ly soluble than the calcium phosphates traditionally used in fertilizers. Since the release of phosphates in forests is taken care of by fungi the leaching is slower, and phosphate uptake better.Therefore less eutrophication by run-off is observed. If the granulation process is further optimized by making light weight aggregate the particles will hold moisture better and provide better growth substrate for the microbiota. In mineral wool manufacture powder raw materials can also be problematic, and therefore the ash may need to be made into briquettes or granulated before use. This can raise the costs for use of the material. Since the main benefit of the material is its low cost this can be a significant burden. How- ever, systems exist for the addition of powder raw materials into the system which may allow for the addition of ash di- rectly into the process. Another issue with these types of application for the ash is that the process must be located fairly close to the facility. If the ash must be transported long distances the margins of profit are quickly lost. Results Leaching results for the ash were typical for the field. About 80 % of the phosphates were extractable with traditional Sludge ash valorization Sludge ash valorization routes: Traditional methods for leaching ash are enhanced with high impact milling (mechanochemical activation). By produc- ing new surfaces through activation the leaching process can be accelerated significantly. The ash may be used in processes where it contributes beneficial properties based on its chemistry. Even though the ash is not viable as an agricultural fertilizer it can potentially be used as forest fertilizer. Another process where ashes are beneficial is the manufacture of mineral wool. The melting properties of the ash are good for this application, and phosphate that is in the ashes improve the properties in the process and the biocompat- ibility of the product. Other application fields for sludge ash are refractory materials where it functions as a flux and can contribute a desirable size fraction for better density of the material. Often sludge ashes have been used in construction materials as a filler. Milling equipment for the treatment of the ashes Ash granulate WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 23. 23 heap leaching processes. Grinding of the ash increased the rate of the leaching and this is a viable pre-treatment of the ashes in a leaching process. The ash had a high content of iron (Fe) and aluminum(Al) which are known to be difficult to remove. Results for the forest fertilization trials and mineral wool pilot trials are pending. Perspectives for the future In the future as costs for deposition of waste materials rise the incentive to recycle ash will rise. Ashes and slags have many desirable properties, and an increased use of this type of materials is both desirable and probable. In the future manufacture processes will be planned with local raw mate- rials from wastes in mind, and a more circular economy will be implemented. Contact Renotech Oy, Bob Talling bt@renotech.fi Implementation of sludge ash valorization into a production line. TECHNOLOGIES – RESOURCE RECOVERY
  • 24. 24 Applicability and pre-requisites Improved control strategies are applicable in all side stream Anammox reactors. This study is specifically targeted for the following one-step Anammox treatment reactors operated with suspended active sludge. The introduction of a more advanced control strategy requires: • A thorough follow-up of sensor conditions and adequate maintenance • An acceptable water quality, facilitated by a process that is more robust and/or achieves better removal efficiencies compared to simpler control strategies Anammox The anoxic ammonia oxidation (Anammox) process is a unique biological process for nitrogen removal, which allows significant savings (up to 60%) in aeration demand compared to the classical nitrification/denitrification process. The Anammox process has proven to be successful in ammonium-rich wastewaters at temperatures above 25°C. Reject water from anaerobic digestion of sludge is an excellent stream to be treated by the Anammox process. Many WWTPs already have an Anammox reactor to treat reject water from anaerobic digestion, but there is a need for advanced control strategies to increase process robustness. The main objective within R3water is developing new algorithms for dynamic Anammox control. These control strategies are tested and demonstrated at two pilot-scale Anammox reac- tors in Sweden and Belgium, and the results are being compared. Technologies Resource Efficiency WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 25. 25 Features and benefits • An increase of the process reliability, to reach effluent targets, to let the biomass better adapt to inflow variations, and to reduce cases of process failure (pumps or aeration) • An improved know-how of the process, to extract informa- tion on the biomass activity • A dynamic process control, for a fast and adequate adjust- ment of the reactor cycle Operation and maintenance For the implementation of an advanced control strategy, in- stallation and maintenance of advanced sensors, connected to a control system, are needed. Although these advanced control systems come with their own operation and mainte- nance needs, the goal is to reduce overall operator efforts by improving the process robustness. Maintenance of connecting equipment, such as pumps, stirrers and aerators, might be re- duced since possible failures of these can be discovered earlier. Results Results – Belgian demonstration For the Belgian demonstration, 5 control strategies were test- ed and at last integrated: 1. Feed control based on ammonia, as baseline control strategy. Ammonia was first determined by a proxy measurement (conductivity), and subsequently by direct measurement. 2. Feed control based on ammonia with‘free ammonia (FA) inhibition’determination and mitigation. 3. Aeration control based on nitrite measurements. This control strategy was implemented on top of the contin- ued feed control. The aeration time was increased or de- creased, to limit the build-up of NO2 -N at the end of the aeration phase, which would favor growth of NOB. 4. Aeration time was extended by alkalinity dosage. 5. Process control targeting the NOB washout based on free ammonia shocks. The Anammox pilot was at first located in Leuven WWTP. The Leuven centrate waters had a rather high COD/N ratio, resulting in a poor Anammox performance. In July 2015, the pilot was moved to Antwerpen-Zuid, resulting into feasible Anammox operations. Process performances were boosted by bicarbonate dosing as a source of alkalinity. The process stability was impacted by sensor failure, which could only be countered by intensive maintenance and manual follow-up of the process. The process stability was as well impacted by fluctuating influent nitrogen loads. During the baseline period (ammonia-based feed control), the pilot operated relatively stable with a TN removal of 75-80%. However, frequent NO2 -N accumulations were ob- served, which can be detrimental to Anammox activity. Dur- ing the aeration control phase, TN removal was stable at sat- isfying removal percentages between 77-87%. Feed control was optimized with more stable effluent ammo- nia in the reactor. Free ammonia inhibition was also prevent- ed, targeting the accumulation of NH4-N due to load varia- tion of the centrifuges. The application of ammonia shocks was also investigated with determination of optimal FA exposure levels and con- tact time. Results were tested in lab scale and implemented in pilot scale. The purpose of this feature is the reduction of temporary NOB residual activity. Results – Swedish demonstration The aim of the Swedish demonstration was to evaluate the efficacy of redox potential combined with pH for controlling the partial nitritation/Anammox process. The testing was centred on three key variables (pH, ORP, and nitrogen load). In addition to verification of the control scheme working to an acceptable level, the study also sought to determine the optimal set point for each of the three variables. The optimal point was assessed from a variety of different response varia- bles such as nitrogen removal efficiency and cost of nitrogen removed. No. of test pH Nitrogen load (gN/m2 /d) Redox (mV) I 7 1 -70 II 8 1 -70 III 8 1 70 IV 7 1 70 V 7,5 2,5 0 VI 7 4 -70 VII 8 4 -70 VIII 8 4 70 IX 7 4 70 X 7,5 2,5 0 pH, Redox and nitrogen load in the test runs Using a standard full-factorial design of experiments, with two levels for each variable, eight different periods were deemed necessary. In addition, two middle points were in- cluded as a reference point for the other tests, which brought the total number of periods to ten. TECHNOLOGIES – RESOURCE EFFICIENCY
  • 26. 26 Stable operation and acceptable levels of nitrogen removal (>80%) were achieved for three periods where the common factor was an ORP value of 70 mV. The highest nitrogen re- moval rate (83.7%) was found when the test conditions were pH 8, nitrogen load 1 gN/m2 /d, and ORP 70 mV. The economic performance of each period was also evaluated and it was found that the optimal point, in terms of aeration and of the three periods with sufficient removal efficiencies, was the same as the optimal removal conditions except with a pH of 7. A secondary test was performed in order to directly compare the performance of ORP with dissolved oxygen (DO) as a control parameter. It was found that DO significantly outper- formed ORP under identical test conditions, yielding a higher nitrogen removal rate (78.2% vs. 65.3%) as well as significant- ly less aeration energy. Perspectives for the future A marketable control algorithm should rely on robust sensors with a low risk of failure. In the Belgian demonstration case, the control strategies relied on sensors that required auto- mated sample filtration and determination of N-compounds, required intensive maintenance and were prone to failure. Additionally, an ideal Anammox control process should not only be based on energy savings and N-removal. As societal awareness towards environmental themes increases, a pro- cess control must also be able to incorporate environmental considerations in its system, such as greenhouse gas (N2 O) emissions. WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT Contact Klara Westling klara.westling@ivl.se Alessio Fenu alessio.fenu@aquafin.be Tom Wambecq tom.wambecq@aquafin.be Francis Meerburg francis.meerburg@aquafin.be
  • 27. 27 Addressed problems and challanges Between 45 and 75 % of the energy costs in aWWTP are spent in the aeration of the biological reactor. The optimization of this process is fundamental to decrease the operational costs of the whole plant. Additionally, the optimization has to be done without affecting the quality of the treated water that has to accomplish with the UWWTD regulations. OptimEDAR uses DO and Redox measures to determine the status of the biological reactor calculating the Equivalent Or- ganic Charge (EOC), a ‘virtual sensor’ that estimates the or- ganic matter load in the bioreactor. By adjusting the timing andoperatingconditionsoftheblowersaccordingtothestrin- gent reactor’s oxygen requirements, the energy consumption is optimised while allowing longer denitrification cycles. Applicability and pre-requisites The OptimEDAR solution is applicable for activated Sludge WWTPs with biological reactor (concentric or carrousel), aer- ated with up to 5 blowers (1 or 2 speeds). Better results are achieved in plants where influent suffers a significant varia- tion in organic matter load or plants designed for covering a seasonal peak demand that are normally oversized. • Recommended WWTP constructive features –– Reactor where it is possible to establish a perfect mixture hypothesis. –– Enough power in the aeration system to absorb loads. –– Stirring system independent from aeration. –– High hydraulic times or presence of homogeniser. • Conditions of the process –– WWTP with a cyclical pattern of load. –– Adequate daily load that does not saturate the operation of the plant. –– No optimised control: set points of oxygen, or control by on-off time. –– Excess of nitrates in the effluent. Features and benefits Features: • Simple and robust. • Add-in solution, easy to install, without interfering with exist- ing automation • Based on robust probes with low maintenance requirements • It adapts to changes in influent load. • Reliability and easy operation Benefits: • Reduction of operating costs. –– Less energy consumption. –– Less reagents consumption. –– Less sludge treatment. • Increase the quality of the effluent. –– Restore balance in case of major changes occur in the influ- ent or uncontrollable external conditions. –– Stability of the biological reactor. –– Removal of carbonic demand. –– Increased removal of nitrogen content. –– High performance on phosphorus removal. • Improve operational efficiency. –– Optimises the energy consumption. –– Sludge stability, providing an optimal state for water treat- ment. Results Within the R3Water project, the OptimEDAR demonstration was held in Wijer (Belgium) (1,440 P.E., design flow max. 2470 m3 /day) and in Empuriabrava (Spain) (70.000 P.E., 16.000 m3 /day), as cases of study for a small plant in different climatic conditions and a big plant with highly seasonality. Empuriabrava WWTP belongs to Consorci Costa Brava (CCB) facilities, a water agency in Spain that is in charge of 18 mu- nicipal wastewater treatment plants, operated by the Em- presa Mixta d’Aigües Costa Brava (EMACBSA). Empuriabrava WWTP operators have been testing different control strate- OptimEDAR OptimEDAR is a low-cost aeration control system for WWTP, based on virtual sensing techniques that adapts the use of the blowers to the organic load in the bioreactor, allowing energy savings (20% on average), longer denitrification cycles, and improving the quality of the effluent. TECHNOLOGIES – RESOURCE EFFICIENCY
  • 28. 28 gies for the aeration process during the lasts years. Thanks to this situation, it has been possible to compare the Optim­ EDAR results with 3 other methods in terms of energy con- sumption as well as the quality of the effluent. The results obtained shows 20% less use of the blowers related to the previous year. After comparing the use of blowers related to flow and the quality of the effluent we can conclude that the OptimEDAR control is more efficient than the control by redox or time an similar to ammonium control in terms of the quality of the effluent. Nevertheless the operational costs of OptimEDAR are much lower and robustness much higher compared to ammonium control. Wijer WWTP belongs to Aquafin NV that operates in Flanders and collects & treats the municipal wastewater of around 5.5 million people equivalents, that is treated in 289 plants. Wijer WWTP is characterized by its diluted charge, and the Optim­ EDAR was optimized to run under these conditions. After this optimization, the results showed a strong improvement of the energy balance of the aerators, with a reduction of energy consumption about 10% compared to the previous O2 -control method. Perspectives for the future OptimEDAR in Wijer and Empuriabrava will be transfered to the regional agencies to continue with the operation. These 2 experiences will be used as success cases for the future commercialisation strategy. Contact adasa@adasaproducts.com OptimEDAR structure Comparision to other control strategies. WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT Energy/Flow Energy/BOD Energy/COD Energy/TN BOD removal COD removal TN removal Ammonia control ✸ ✸ ✸ ✸ ✸ ✸ ✸ Redox control ✸ ✸ ✸ ✸ ✸ ✸ ✸ Time control ✸ ✸ ✸ ✸ ✸ ✸ ✸ OptimEDAR ✸ ✸ ✸ ✸ ✸ ✸ ✸
  • 29. 29 Description The overall aim of the project is to design, implement and validate a control structure for efficient WWT plant opera- tion. The control structure will be based upon a Model Pre- dictive Control (MPC) technology where a simplified process model together with estimation techniques is used to mini­ mize a cost function. This cost function is represented by a prediction of defined quality parameters related to a desired set-point. Applicability and pre-requisites In the project setting, the MPC’s objective will be to enhance the O2 set-point tracking in aerobic biological reactors while reducing the operation costs (energy). Furthermore, distur- bance rejection is another important capability of the MPC, where the goal is to minimize the effect of flow and concen- tration disturbances entering each aerobic reactor. The MPC shall replace the existing PID controllers and have direct ac- cess to the necessary manipulated variables (MV). Advantages and disadvantages The solution will optimize the treatment operation both in a quality (purification) perspective and in terms of resources usage (energy). The technology (concept) will be applicable for a range of scenarios, possible with some model re-para­ meterization or re-configuration. The technology will be relevant for a range of various plant configurations. However, there will be some plant require- ments related to instrumentation and actuators. Typical MPC response into the prediction horizon Prediktor MPC block diagram Model based predictive control Model predictive control (MPC) has its roots in optimal control and has become the most popular advanced control technology in the chemical processing industries. There are many variants of MPC controllers, both in academia and in industry, but they all share a basic concept which is to use a dynamic model to forecast system behavior, and optimize the forecast to produce the best decision - the control move at the current time. Models are therefore central to every form of MPC. Because the optimal control move depends on the present state of the dynamic system, a second basic concept in MPC is to use the past record of measurements to determine the most likely present state of the system. Thirdly, most MPC controllers are able to account for constraints both in manipulated variables and states/controlled variables through the formulation of the optimization problem. The foundation of MPC relies on the computation of the sequence of future control moves, performed by solving the optimization problem. Only the first computed con- trol move is implemented. The model based predictions are corrected using feedback information at each sampling instant, before a new optimal sequence of the future control moves is computed, according to the receding horizon principle. TECHNOLOGIES – RESOURCE EFFICIENCY
  • 30. 30 Operation and maintenance In operation, the solution will require limited O&M activities. During operation, the solution will need to be monitored as an integral part of the conventional automation system. Related to maintenance, some model adaptations could be required, especially related to changes to the physical plant configuration. Implementation and results PlantSimulator:Alotoftimehasbeenspentonunderstand- ing the complex dynamics and relations within the WWT and evaluation of the existing research results and publications regarding the control issues in WWT. A few available (both commercial and freeware) simulators such as STOAT and Dy- namo have been considered as an aid for design of control- ler structure. However, these provided unsatisfactory results due to challenging and complex configurations and data requirements. Thus, the aim of the project changed towards using in-house software for implementation of a simulator that could describe the Swedish pilot plant.This has been ac- complished through application of the well-known Activat- ed Sludge Model 1 (ASM1). Estimator: During evaluation of the simulator at site in Stockholm, it became clear that fitting the simulator to the plant can be a time-consuming task due to the large number of parameters and states. With much support from the IVL group, the simulator was validated through application of Ex- tended Kalman filtering (EKF) which is a state and parameter estimation technique. The EKF uses a reduced-order ASM1 model as its internal model in addition to the available on- line measurements. The reason for this model reduction has been the lack of observability of the complete ASM1 model, which is an essential pre-requisite for estimation capability of the system. Finally, a platform now exists for online real-time dynamic simulations of the pilot plant, that is a simulation running in parallel with the plant, and using the same inputs and outputs. One additional benefit of this is the possibility to try out new strategies and changes in the way the pilot plant is operated such as changing the number of reactors, Comparison of results from bioreactor 5 WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 31. 31 where and how the recirculation is done, and other interest- ing ideas. Furthermore, this platform is the base for applying advanced control systems with much less effort than before. Controller design: Several approaches and strategies have been considered and even partially implemented. These approaches have mainly focused on finding a proper mod- el for the model-based controller (MPC). After gaining val- uable process insight through the simulations, a simplified model was designed to be used in the MPC with the aim of controlling the dissolved oxygen level in a single bioreac- tor. This has been successfully implemented and tested in closed-loop at Swedish pilot plant. That means, the MPC has replaced the PID-controller for one reactor using both data from the simulator (states and parameters) as well as the esti- mated dissolved oxygen in the same reactor. As the figures in previous page illustrate, the MPC shows better performance in terms of set-point tracking (keeping the level of dissolved oxygen close to 2 mg/L) and disturbance rejection (the same disturbance occurs for both the PID and the MPC structure). Future enhancements: Further enhancements of the MPC have been considered. Examples include control of the oxy- gen content of bioreactor 4 (BR4), amount of sludge recycled in the system, and economic optimization of the air blower volume flow to the aerators in the bioreactors. All these en- hancements can be implemented within the current frame- work. Perspectives for the future Based on the simulation and experimental results obtained during this project, it is obvious that using an advanced con- trol strategy (such as combining nonlinear state and para­ meter estimation technique and nonlinear model predictive control) can be economically beneficial.That means, keeping the different material concentrations (such as O2 ) at appro- priate levels while using the energy resources more efficient- ly. Considering the developed platform by Prediktor during the R3water project, the commercial potential of such pro­ duct is considerably high, in addition to increased interest from academic institutes (such as universities) for possible research studies. Thus, it opens up the possibility for numer- ous research and commercial activities within WWT, specially focusing on modelling and controller aspects of the process. Contact Thomas Pettersen thomas@prediktor.no TECHNOLOGIES – RESOURCE EFFICIENCY
  • 32. 32 Adressed problems and challenges Aquafin faced some challenges at the Girona WWTP: • A complex blower algorithm needed to be upgraded with a new parametrization as to increase lifetime. • The primary settling tank was modelled in function of differ- ent parameters, validated in full scale and its malfunctioning integrated in the model. • Air distribution through the 4 aerated basins did not seem to follow the diffusers surface distribution. The data collected in full scale did not alleviate the uncertainty on this aspect. • Eventually, high saving opportunities were identified due to the actual continuous aeration in the biological tanks. • A malfunctioning of the sludge thickeners was identified by establishing a detailed sludge mass balance, and was later solved by the plant operators. Applicability and pre-requisites The model-based energy audit tool can be used to: • Select plant-wide scenarios (pumping strategies, sludge and water line interactions, etc.) to reduce energy consumption, costs, and CO2 emissions • Complete realistic cost assessments (peak demands, optimal contracted power, etc.) Model-based energy audits in wastewater treatment plants The total operation costs of a wastewater treatment plant (WWTP) are, for a large part, determined by its electricity consumption. Energy audits can identify opportunities to reduce energy use inWWTPs, but they cannot pinpoint ways to optimize energy use. Only a model based approach with robust multi-variate data analysis can deal with such com- plexity. Aquafin has developed a model-based energy audit tool that integrates water and sludge dynamic models with a detailed modelling of all single process units and a correct model parametrization. By means of a detailed data analysis, the model output can be used to determine: a robust parameter set, critical operations of blowers and other unit processes, total costs and single cost components, life cycle analysis, and detailed cost- and energy-saving strate- gies. This whole-plant modeling tool of Aquafin is demonstrated through the R3 Water project at the full-scale WWTP of Girona (Spain). (Left) Effect of new blower parametrization on overall plant performance in Girona. (Right) Bivariate plot to screen scatter plots as to improve parameters set robustness WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 33. 33 The tool requires: • High-quality data of the design and operation of the WWTP • Highly qualified personnel for correct use and interpretation. Technical support can be offered by the model developers Features and benefits • Evaluate multiple energy-saving strategies without affecting the process • Evaluate future scenarios for planning Operation and maintenance The model-based approach has to be updated every time there is a significant change in plant configuration or in envi- ronmental conditions. Constrained combinatorial parameters scenario analysis: Scenario analysis is pursued by combining several param- eters that are involved in the modelling, putting constrains where necessary. The parameters are chosen to pursue op- timization according to experience and real practice. Para­ meters vary in range and steps to which the model outcomes are sensitive. Data analysis results in a bi-dimensional scatter plot with each point representing one simulated year (with a specific parameters dataset). Scatter plot coordinates repre- sent process performances, i.e. cost, energy and water quality performances. All parameter impacts are analyzed towards each single process unit and overall plant performance. Multi-variability analysis allows to maximize reliability of unit processes, choose a robust set of parameters, and optimize towards specific parameters and overall performance. Results To model the Girona WWTP, Aquafin used data from the year 2013 (January-October). The yearly dynamic data were fitted with regards to: effluent quality, primary settling tank effluent concentrations, removal performances, sludge pro- duced, and power consumption of each different compart- ment. Data are evaluated considering an overall ‘yearly cost’, because energy savings can be counterbalanced by, for ex- ample, increased sludge production or reagents costs. The evaluated scenarios include actions that are: (I) opera- tions based, such as solving the thickener malfunctioning, or reducing the MLSS concentration; (II) control-based, such as optimizing the blowers algorithm, DO sensor position, exter- nal recycle control; (III) based on on-line nitrogen control; or (IV) a combination of these. The outcomes are summarized in the table above. Perspectives for the future The outcomes of the modeling exercise will be communicat- ed to the operators of the respective WWTPs, to allow them to make informed decisions to improve the energy and cost balance of their plant. Aquafin is bringing their modeling and support service to the market. Factors that influence the marketability include (Left) Blowers switch on-off minimization in function of actual parameters. (Right) N controlled scenario results with sensitivity towards NH4-N TECHNOLOGIES – RESOURCE EFFICIENCY
  • 34. 34 the practical applicability of the outcome to the specific situation, the risk of failure of the proposed improvements, the impact of the proposed improvements on effluent water quality, and the achieved economic benefit. Contact Alessio Fenu alessio.fenu@aquafin.be Francis Meerburg francis.meerburg@aquafin.be Results of the scenario analysis, showing improvements in TN removal and operational costs for different non-invest- ment and investment measures. The baseline scenario had an operational cost (over 300 days) of € 507,000 Euro and TN removal of 90.2%. Scenario description TN % Removed Cost € 1000 Comment Process operation improvement Thickener +1.0 -60 Excluded from all other scenarios MLSS reductin +1.5 -5 Reduced of 600 mg SS/L No Investment Cost foreseen Optimization +(0.0-0.3) -(15-25) External recycle, improved blower control, MLSS reduction Investment Cost foreseen N on-line control +(0.5-1.0) -(55-65) External recycle, improved blower Re-arranging grids -(2.5-3.5) -(35-50) 200 diffusers are placed from AER1 to NOAER3 N on-line control +(1.0-2.0) -(110-125) External recycle, improved blower + MLSS reduction + Thickener improvement WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 35. 35 Addressed problems and challanges Wastewater treatment plants spend up to 45% of their op- erating costs on electricity. Plants generate a lot of data, but usually don’t have the tools to answer important questions such as“How much energy do we consume?”,“How could we save money on electricity?”. ICRA has developed InnoWatt, a tool that gives you the clear and reliable information you need to reduce energy costs. The process starts simple by in- stalling InnoWatt in the electricity counter of your facility. Us- ing four modules, InnoWatt tells you how much energy you are using and how you can save money. • Module 1: The first module gives you access to real-time energy consumption. You can access historical data and visualize your consumption patterns • Module 2: The second module calculates your energy costs in real-time, so you don’t need to wait for your monthly bill to know the cost of energy consumed. • Module 3: The third module gives you the optimal contract- ed power for your plant, which can allow you to save thou- sands of Euros without changing any infrastructure. Most plants have contracted more power than they need, so by lowering the contracted power, your plant can save money. • Modul 4: Whole plant modeling. In the last module ICRA will simulate your wastewater treatment plant and run scenario analyses for energy and cost reduction. We will show you how to operate the plant with less energy without sacrificing the quality of treatment. Applicability and pre-requisites • For small WWTPs we recommend the usage of Modules 1 to 3. For medium to large WWTPs we recommend the full poten- tial of InnoWatt (Modules 1 to 4). The return of investment will be shorter as the size of the facility increases. • For the whole plant modeling (Module 4 of InnoWatt) high-quality data of the design and operation of the WWTP is needed. The most tedious step in the modeling exercise is data collection and verification. The better the quality of the data, the more reliable the model outcomes and the more re- alistic the proposed interventions to improve the functioning of the facility. • For installing InnoWatt in the electricity counter there is no special pre-requisit, as the technology is compatible to most of counter brands. Features and benefits Thanks to InnoWatt, you have full control of your energy con- sumption. The main benefit a facility can gain is the reduc- tion of energy consumption, costs and CO2 emissions while maintaining good process performance. InnoWatt allows you to: • Highlight critical situations where peak demand charges are driving up energy costs. • Develop strategies to reduce energy consumption and maxi- mize energy production at peak time-of-use periods. • Find the optimal contracted power for a specific plant. • Evaluate aeration and pumping strategies. • Study the interactions between the sludge line (with high nutrient loads in the return stream) and the liquid line. InnoWatt One of the largest urban consumers of energy are wastewater treatment plants. Within a WWTP, electricity consump- tion accounts for between 25 and 45 % of the facility’s total operating costs.WWTPs are therefore important targets for reducing energy demand. Energy audits, which identify opportunities to reduce energy use and greenhouse gases in WWTPs, are typically based on the average energy consumption of a facility; they include benchmarking with similar plants or comparison against some standard performance indicators. However, current energy audits could potentially be improved through the use of energy and cost monitoring tools together with dynamic models that integrate water and sludge lines. Because this potential had not been explored in the European market, ICRA developed InnoWatt, a novel energy audit tool that was demonstrated through R3Water. The main goal of ICRA’s technology is to minimize energy consumption while maintaining good process performance. TECHNOLOGIES – RESOURCE EFFICIENCY
  • 36. 36 • Assess the use influent organic content (to maximize either nutrient removal or biogas production). • Assess the upgrade of the system for biological phosphorus removal Operation and maintenance Hardware and software is needed for the usage of InnoWatt. An optical sensor is used to connect to the electricity coun- ter. That sensor is also connected to a data management sys- tem that allows visualizing all information from the counter in a web. Once installed, no maintenance is needed for this device. Module 4 is a service offered by ICRA which requires large effort the first time the model is built for a specific facil- ity. Once the model is ready it should be properly maintained (with little effort) any time there is a significant change in the configuration of the facility or in the environmental condi- tions such as influent wastewater composition, electricity tariffs, etc. If the company managing the WWTP has qualified personnel to run the model, best is that they maintain the model following some recommendations from ICRA. If not, maintenance can be entirely executed by ICRA. Results Girona WWTP: A model-based treatment performance and energy audit of the Girona WWTP in Spain was conducted using advanced and fully dynamic air supply models. The focus of the study was on the aeration system, which rep- resents 63% of the plant’s energy consumption. A dynamic model consisting of a process, a realistic controller, and a very detailed air supply model, was developed and calibrat- ed to be used as the baseline for testing various scenarios. Results show that the implementation of an ammonia-based controller and a redistribution of the diffusers led to energy savings between 12 and 21 %, depending on wastewater temperature. In addition, the model demonstrated that the current blower is too large, which causes an intermittent behaviour, endangering the equipment and shortening its life-time, plus limiting the minimum air-supply. The applied aeration system models enable engineers to identify bottle- necks by modelling equipment constraints (e.g. blower turn- down). Ignoring the air supply side in an assessment could result in an overestimation of energy savings or treatment performance and consequently in non-optimal control solu- tions or equipment selection. The carbon footprint assess- ment showed that direct N2 O and CH4 emissions from the biological reactor are of the same magnitude as indirect CO2 emissions from electricity use. Hence, efforts should not be only allocated to reduce electricity consumption but also di- rect emissions. Harelbeke WWTP: ICRA developed an integrated model of the Harelbeke WWTP. The model was used to find strategies to enhance Biological Phosphorus Removal in order for the plant to reduce resource consumption. Currently phospho- rus is removed chemically and thus 400 Tn·year-1 of FeCl3 are used. The evaluated scenarios included decreasing the flow- rate of return activated sludge, adding an internal recycle from the aerobic zone to the anaerobic zone and adding an external source of volatile fatty acids. Based on the simula- tion results we recommend that the Harelbeke plant imple- ments the reduction of the return activated sludge flowrate to 50 % of the influent flowrate. Without any capital invest- ment or other direct costs to the plant, this modification could reduce the energy consumption of blowers by about 7 % and the consumption of FeCl3 solution by about 40%, while maintaining an effluent quality that meets Belgium’s current regulations. Contact Lluís Corominas lcorominas@icra.cat Ignasi Rodríguez-Roda irodriguezroda@icra.cat Mehlika Ayla Kiser akiser@icra.cat InnoWatt installation in the electricity counter Module 4. Whole plant modeling & scenario analysis WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 37. 37 Addressed problems and challanges Many industrial processes can be improved if the method of transfer from gas to liquid was more efficient. Wastewater treatment and Anaerobic Digestion are such processes. Per- lemax has developed a microbubble technology which has low power requirements allowing increased gas transfer with no energy penalty. The R3Water project gave the company the opportunity to build upon its experience of scaling up from laboratory and pilot level operations. This was to con- firm that microbubble technology could allow a significant reduction in energy comsumption whilst maintaining the re- quired performance in waterwater treatment plants. The jus- tification for the experiments was that power requirements for wastewater treatment across Europe are considerable and have been estimated at € 750 m per annum. Anerobic Digestion was also investigated to see if perfor- mance could be improved whereby more methane gas is produced and the sludge is more stable. These experiments were conducted with CO2 instead of Oxygen. Applicability and pre-requisites The sites chosen wereWWTP Aarteslaar in Belgium and Ham- marby Sjösatdsverk in Sweden as being a scale up from ex- periments already carried out. However, measurement of power reduction was not been possible and any measurement has been on the basis of the KLA technique usually intended for clean water. The basis for successful implementation was based on several factors which can vary all of which will vary depending on the waste- water treatment facility being used. These are feedback loop length, oscillation frequency, airflow rate. A direct and timely measurement method is to measure bubble size. This will al- low optimum of the three factors compared to bubble size. The technology consumes no additional power as it works on the airflow used in a process. There is no need for a individu- al control system as performance will be measured through SCADA systems. Operation The technology uses flu- idic oscillators which di- vert the air flow before it reaches the diffuser and modifies the bubble cre- ation. Results First experiments were carried out by “above water oscilla- tion” with the fluidic oscillator positioned outside the waste water tank. The results showed little difference in efficiency using this technique and was considered to be due to a difference in pipe design between already tested sites in the UK and Aqua- Fluidic oscilliation By using fluidic oscillation microbubbles can be generated, which significantly improve gas transfer to liquids. Picture showing oscillator in centreComparison of the bubble sizes Schematic diagramme of the microbubbles technology TECHNOLOGIES – RESOURCE EFFICIENCY
  • 38. 38 fin’s facility specifically a design that equalizes air flow. Above water oscillation was originally pursed because it would al- low retrofit in any wastewater treatment plant. To overcome the design for air flow equalization an oscilla- tor design that is not positioned above water but within the wastewater tank was investigated. The device has been nick- named the TOAD. It featured all the requirements of a fluidic oscillator but on a much smaller scale and included 2 diffusers as part of the device. This has been tested at the Swedish site and produced a sig- nificant improvement in oxygen transfer of 53%. In an anaerobic digestion laboratory experiments, when a reactor was dosed with CO2 microbubbles the methane pro- duction increase by over 100% and the stability of the sludge was improved. (2.02g DO/m3 air) (3.08g DO/m3 air) View of the oscillators Comparison of dissolved oxygen (DO) per m3 air WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 39. 39 The over 100% improvement level was not replicated in the test facility at Aarteselaar, NL, but an improvement was shown. One of the major differences between laboratory and the first test was direct dosing of the CO2 directly into the reactor achieved in the laboratory but not in the test tanks. This is a major consideration in any retrofit programme as it is likely to change the design of the AD tanks substantially. Testing at IVL is ongoing at the time of publication of this brochure and further research is to be funded by Innovate UK after the R3Water project is complete. Perspectives for the future The potential for this technology is significant but further larger scale tests are required. These tests are in planning and will take place later in 2017. Contact Graeme Hitchen graeme@perlemax. com  Hammarby test facility in Sweden TECHNOLOGIES – RESOURCE EFFICIENCY
  • 40. 40 Environmental Technology Verification (ETV) is a tool to help innovative environmental technologies reach the mar- ket. Special focus is on highly dynamic and innovative Small and Medium-sized Enterprises (SMEs). Claims about the per- formance of innovative environmental technologies can be verified by qualified third parties called “Verification Bodies”. The “Statement of Verification” delivered at the end of the ETV process can be used as evidence that the claims made about the innovation are both credible and scientifically sound. With proof of performance credibly assured, inno- vations can expect an easier market access and/or a larger market share and the technological risk is reduced for tech- nology purchasers. The idea of the R3Water project was not only to demonstrate innovative technologies, but also to show an innovative “R3 demonstration concept” (Reviewed – Referenced – Recognized) that makes use of the concept of Environmen- tal Technology Verification (ETV). Compared to conventional projects this concept secures a more parallel and direct mar- ket acceptance in European countries making use of ETV and LCA (Life cycle assessment)/Life cycle costs (LCC). The concept of ETV and the links to the EU ETV Pilot Pro- gramme and ISO standard (ISO 14034) on ETV were directly integrated in the demonstration of the technologies in the project, reducing the need for extra testing. Three verifications were foreseen in the R3Water project. One technology was already successful: from the field of“Reuse of water” the technology AQUATRACK® from Aqua-Q, Sweden, has got the EU ETV“Statement of Verification”. The online monitoring technology AQUATRACK® has been demonstrated successfully and was verified at the same time leading to the Verification statement in dec 2016. Further aquaBio from ADASA, Spain (monitoring for water reuse) and HTC (Hydrothermal Carbonisation) for sludge valorisation, from AVA, Germany (“Resource recovery”) have started to go through a verification procedure under the EU ETV Pilot programme. Experiences with EU ETV Pilot Programme Review Technology Demonstration EU ETV Pilot- Programme International Working Group ETV Market Acceptance in ETV accepting countries Referenced Recognised LCA LCC ETV Recommendations for efficient technology verification: • Spend time to prepare claims and select standards in which the verification will be performed. • Compare quotations from different actors and talk to responsible persons and make clear who will do what. • Make sure that the verification body has no previous connection to the project or any other way to your organisation. It is important to have an impartial verification body. • Try to answer the EU commissions questions regarding the verification in a simple and friendly manner. • Make sure that the test body is accepted by the Verification body and fulfils requirements by the ETV scheme. The R3 demonstration concept WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 41. Microbubbles Model-based energy audit Model predictive control AquaBio Doscontrol Aquatrack Anammox Anammox control system Sludge Sludge Incineration Ashes Product processing concept for incinerated sludge ash valorization HTC Ozone disinfection system Biogas Quality controlled reclaimed water Treated water TM Microbubbles OptimEDAR Water reuse Resource recovery Resource efficiency Wastewater Technologies for: Removal of pharmaceutical residues 41 Demo Sites Location of technologies at the WWTP DEMONSTRATION SITES
  • 42. 42 Demonstration has been mainly performed in the Consorci Costa Brava (CCB) facilities, a water agency in Spain that is in charge of 20 regional wastewater treatment plants, operated by the Empresa Mixta d’Aigües Costa Brava (EMACBSA). CCB is a consortium created in 1971 by the 27 coastal municipal- ities of Girona’s province in northeastern Spain to provide services and to manage infrastructures related to the whole water cycle, from the drinking water supply (as wholesale purveyor) to the wastewater treatment and to the production and supply of reclaimed water to cover non-potable demands. The resident population in the whole area is estimated in some 250,000 inhabitants, with a seasonal increase in sum- mer that can reach above 1 million people and that requires the facilities to be designed to provide the adequate servic- es in the peak period. Since 1989, one of CCB’s activities is the reclamation of treated effluents in 14 facilities and their supply to cover non-potable demands of different kind (3.1 milion m3 /year in 2012, with a maximum in 2010 reach- ing 6.4 milion m3 /year). WWTP Empuriabrava WWTP Empuriabrava Empuriabrava WWTP is located in the area of “Aiguamolls de l’ Empordà”, a national park which is the second largest wetland in Catalonia between the confluence of the rivers Muga and Fluvia. It is the prime habitat for wildlife, especially aquatic birds This plant has an estimated flow around 16,000 m3 /day to treat an equivalent population of 70,000 PE and receives the wastewater from Empuriabrava, a touristic neighbourhood belonging to Castelló d’Empuries. The treatment carried out at this facility is a biological treatment with nitrogen removal and phosphorus removal and a constructed wetland tertiary treatment. WWTP Castell – Platja d’Aro Castell – Platja d’Aro WWTP receives the wastewaters from the surrounding municipalities of Castell d’Aro, Platja d’Aro, Sant Feliu de Guixols and Santa Cristina d’Aro. The plant was designed for an average capacity of 35,000 m3 / day, and 175,000 PE. However this WWTP is affected by high seasonality influenced by the tourism in the area. The treat- ment line in Castell- Platja d’Aro WWTP consists on a primary treatment, secondary treatment with conventional activated sludge and a tertiary treatment. WWTP Castell – Platja d’Aro The tertiary treatment is designed for a 15.000 m3 /day flow, meaning that only part of the water from the secondary clar- ifier is further treated for reuse. The rest of the effluent is dis- charged into the Ridaura river and the Mediterranean sea. WWTP Girona The Girona facility is an activated sludge WWTP that has the capacity to serve 275,000 PE. The WWTP was constructed in Demonstration sites in Spain WWTP Girona WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT
  • 43. 43 1986 but was upgraded in 2008. The old biological reactors and secondary settlers (not used now) were substituted by new ones. From the three lines for the biological reactors they are currently using two of them. The WWTP Girona is operated by Tractament de Residus I Aigües Residuals de Girona, SA (TRARGISA). WWTP La Bisbal d’Empordà La Bisbal d’Empordà Wastewater Treatment Plant belongs to Water Agency of Catalonia. La Bisbal d’Empordà WWTP is located in the area of El Baix Empordà, and receives the water from the municipalities of La Bisbal d’Empordà, Castell d’Empordà, Corçà, Cruïlles, Mo- nells, Sant Sadurní de l’Heura and Forrallac. Plant influent consists of municipal wastewater, and waste- water from livestock and smaller industries plant has a ca- pacity to treat waste water from neighbouring counties of Girona of about 3,200 m3 /d. The wastewater treatment plant is placed with a container- ized ZeeWeed MBR system. This MBR ultrafiltration mem- brane system has a nominal pore size of 0.04 µm, which pro- vides a physical barrier to bacteria, parasites and viruses. At La Bisbal d’EmpordàWastewaterTreatment Plant there are two parallel MBR ultra filtration lines which run sequential as per a standard operating procedure. Wastewater is treated on continuous basic day and night throughout the year. Main treatment consists of ZeeWeed hollow fibre MBR process. TheWWTP La Bisbal d’Empordà is operated by AQUAMBIENTE. Container of ZeeWeed MBR system Concept of the WWTP La Bisbal d’Empordà DEMONSTRATION SITES
  • 44. 44 Aquafin owns and operates 298 wastewater plants in Bel- gium, varying in size and composition. Therefore, each tech- nique can be demonstrated in an appropriate setup. Seven innovative solutions for reuse of water, recovery of valuable substances and resource efficiency are demonstrated. WWTP Aartselaar, pilot reactors and small-scale WWTP The pilot testing will be done in Aquafin’s demo-site in Aart- selaar, Belgium. For the case of fluidic oscillation, pilot exper- iments were performed in an 8.6 m³ clean-water pilot tank (aerobic oscillation tests) and two parallel 1.3 m³ digester tanks (anaerobic oscillation). The small-scale WWTP, located parallel to the full-scale WWTP of Aartselaar, has a size of 140 m³, which corresponds to 1,000 PE. This small-scale biore- actor was used for the case of fluidic oscillation. It was ide- al to perform aeration tests in a fully operational activated sludge basin, which require interruption of the process and can therefore not be performed at a full scale WWTP without endangering the effluent quality. Brugge: WWTP and incineration plant Brugge: Mono-incineration plant The treatment plant of Brugge treats 265,000 people equiva- lents, which makes it the largest plant of the Flemish region. The incineration plant is of the mono-incineration (i.e., only municipal sludge incinerated), fluidized bed type. The ashes of the Brugge incineration plant were used for the case of resource recovery from ashes. Because all practical work was performed at the Renotech facilities, a container filled with 20 metric tons of ashes was shipped to Finland. WWTP Antwerpen-Zuid WWTP Antwerpen-Zuid is connected to household and in- dustries for about 190.000 people equivalents. The WWTP is composed of pre-treatment, anaerobic compartment, aero- bic tanks (4 tanks with alternating scheme), 9 clarifiers. This is the location of the Anammox pilot plant, which treats the liquid fraction of the sludge digestate of the plant. Aeration basins and secondary settlers of WWTP Antwerpen-Zuid WWTP Harelbeke The WWTP of Harelbeke (116,000 PE) consists of a classical activated sludge process. After the usual mechanical screen- ings, the water is sent through a sand trap, travels through an anaerobic zone, then undergoes aeration, and is finally settled in circular settling tanks before being discharged in the nearby receiving watercourse. This plant is used as a case study for the whole-plant modeling study. WWTP Wijer The tests will be performed at Aquafin’sWWTP inWijer (1,600 PE), a full-scale WWTP that started operating from the end of 2013 onwards. This plant was used to demonstrate the Opti- mEDAR aeration control system. WWTP Mechelen-Noord For the demonstration of hydrothermal carbonization (HTC) of Aquafin sludges, municipal waste sludge of the WWTP of Mechelen-Noord was used. This plant treats wastewater of 88,000 PE. The sludge has excellent characteristics for HTC treatment, because the plant removes phosphorus through the Bio-P process, there is no anaerobic digestion, and the sludge has a low silt content. A total of 10 metric tons of sludge was transported from Mechelen-Noord to the industrial-scale plant at Karlsruhe (Germany) for the HTC experiments. Demonstration sites in Belgium WATER IN THE CIRCULAR ECONOMY – INNOVATIONS FOR URBAN WATER TREATMENT