The document describes the specifications and processes involved in annealing and pickling a stainless steel coil. The line can process AISI 200, 300, and 400 grade stainless steel coils that are 0.3-3 mm thick and 600-1300 mm wide. The processes include welding, degreasing, annealing in a furnace, pickling using electrolytic sulfuric acid and mixed acid tanks, skin passing using a two-high mill, tension leveling, and recoiling. The goal is to improve machinability, refine grain size, and remove stresses and surface oxides.
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Annealing and pickling process optimization for stainless steel
1.
2. IntroductionIntroduction
Annealing of a Stainless steel is in order toAnnealing of a Stainless steel is in order to
improve machinability, refine grain size, toimprove machinability, refine grain size, to
remove internal stresses develops duringremove internal stresses develops during
the forming etc.the forming etc.
Whereas pickling is an aggressiveWhereas pickling is an aggressive
chemical removal of oxides scale thatchemical removal of oxides scale that
develops during heat treatment and/ordevelops during heat treatment and/or
surface contaminantssurface contaminants
3. Line SpecificationLine Specification
Material to be Processed AISI 200,300, 400Material to be Processed AISI 200,300, 400
Strip ThicknessStrip Thickness 0.3 mm – 3 mm0.3 mm – 3 mm
Strip WidthStrip Width 600mm – 1300 mm600mm – 1300 mm
Coil ID; (In & Out)Coil ID; (In & Out) 610 mm610 mm
Coil OD; (In & Out)Coil OD; (In & Out) 1800 mm (Max.)1800 mm (Max.)
Coil WeightCoil Weight 28 MT (Max.)28 MT (Max.)
Hand of LineHand of Line Right to LeftRight to Left
Product MixProduct Mix AISI 200 – 60%,AISI 200 – 60%,
AISI 300-30%, AISI 400-10%AISI 300-30%, AISI 400-10%
4. Line SpecificationLine Specification
Total length of line 320 meters
Height of equipment from 10.36 meters
(app.)
+ 0 mill floors level
Depth of cellar from 5 m (exit lopper)
(app.)
+ 0 mill floors level 7.5 m (sump pit)
(app.)
Crane hook height 10.935 m
5. Line specificationLine specification
Product Width 1030mm – 25%
1270 MM-75%
Reference strip 1.2 x 1150 mm
TV Value of Furnace 80 mm.mpm
Max. Line Speeds Entry – 120/160 MPM
Process– 80/120 MPM
Exit – 135/200 MPM
Production at Ref Strip 40.88 Ton / Hr
Annual Production 2,50,000 MTPA
Furnace having Flox Burner by LPG
Pickling by Electrolytic Na2SO4,
Electrolytic HNO3,Mix Acid
7. Line SpecificationLine Specification
2 Hi Skin Pass Mill with Max. 1.5% Reduction
On Line Tension leveller and provision for side
trimmer
Line Bay 30mx350m with adjacent Coil Storage
bay of 24mx350m
8. Line Consists OfLine Consists Of
Entry Equipments with Looper
Welding machine from Guild,USA
Degreasing Unit
Annealing furnace
Pickling section
Skin pass mill with Creep looper
On-line Tension leveller and provision for side trimmer.
Exit equipments with looper
All Auxiliaries which includes Acid Storage, ETP, WT,
DM water plant Etc.
9. PROCESSPROCESS
Uncoiling of CRFH
Coil at uncoiler
Welding Degreasing
Entry looper
Annealing
in furnaceCooling section
Pickling Exit looper Skin pass mill
Tension levellerCreep looper
Recoiling of
CRAP coil
at exit
10.
11. Entry EquipmentEntry Equipment
2 Uncoiler with CPC unit
Paper winder with tension feedback unit
Pinchrolls,5 roll flatteners,Up cut shears,belt conveyors
Flat leader end handling system by vacuum
stacker;Bottom side shiftable
Bridles;deflector,steering rolls;PU coated roll dia 1000
mmx1600 mm
Automatic seam welding machine from Guild USA;
Welding time #4 min..
Coil car, coil centering system
12. WELDING SECTIONWELDING SECTION
Type -Guild Model QMM 125-54, Quick lap Seam Welder
Material 200,300,400 CRSS
Max. Strip Width 1300mm
Min. Strip Width 600 mm
Max. Strip Thickness 3.0mm
Min. Strip Thickness 0.3mm
Electrics 415/3/50
Weld Process Continuous Seam
13. Degreasing sectionDegreasing section
(i) First degreasing stage - Spray
degreasing machine
(ii) Second degreasing stage - Chemical
scrub brush
(iii) Rinsing section - 3 –Stage cascade
rinsing
(iv) Length of degreasing section – 18.15 meters
(approx)
14. ANNEALINGANNEALING
Annealing is done to:
1. To regain grain structure
2. To increase malleability and ductility.
3. To attain mechanical properties.
ANNEALING STAGES
1. Recovery
2. Recrystallization
3. Grain growth
15. Furnace sectionFurnace section
Length of Section is 135 m
10 Air Jet Cooling Chamber
2nd & 9th Jet Cooling chamber is having Mist
cooling also to assist avoiding carbide
precipitation..
Length of Cooling Section 52.5 m
Burners 92 Nos with Turndown ratio 10:1
6 burner control Zone
16. Furnace sectionFurnace section
3 Radiation Pyrometer at Exit of each Chamber.
4 Optical Pyrometer at Jet Cooling Section
Radar Type Furnace sensor.
Burner Flame sensor, Ionization Type
Furnace Pressure Sensor.
Fuel Consumption 22 kg/Ton.
Temperature of Strip AISI 200 – 950 C
AISI 300 – 1020-1140 C
AISI 400 – 740-870 C
Recuperator; Air out temp will be ~ 600 C.
Air Curtains at Exit of Furnace
Threading System
Roll removal Rig
Retraction Cooling Section.
17. Furnace sectionFurnace section
a) TV valve (m/min, mm) for 304 annealing 80
b) TV valve (m/min, mm) for 430 annealing 60
c) Max furnace operating temp 1250ºc
d) Setting range of air/gas ratio 1.1 – 1.6
(i) Total length of the furnace 73,900 m
(ii) Total length of the cooling section 52,500 m
(iii) Length of unfired preheating section 21,000 m
(iv) Height of strip pass line above support floor 2500mm
(v) Furnace chamber 04 chambers
1st chamber: - unfired preheating section
2nd chamber: - unfired + 1st fired zone
3rd chamber: - 02 fired zones
4th chamber: - 03 fired zones
(vi) No. of burner's – 92 (26/36/30)
Burner input / chamber – 22.6 MW (7.6 / 9.2 / 6.1MW)
18. Stable combustion without a flame andStable combustion without a flame and
defined recirculation of hot combustiondefined recirculation of hot combustion
productsproducts
Flox burners
19. Flox and flame temperature fieldFlox and flame temperature field
20. PICKLINGPICKLING
The function of pickling is to dissolve/
remove/ peel off oxide layer on surface of
strip. Such oxide layers are formed during
hot rolling and in case of cold rolled strip
during annealing operation.
IN AP-4 PICKLING IS DONE IN 3 SECTIONS
Neolyte electrolytic pickling section
Nitric electrolytic pickling section
Mixed acid pickling section
21. Neolyte electrolytic pickling sectionNeolyte electrolytic pickling section
Aqueous solution of sodium sulphate is used.
Strip is descaled with help of electric current.
(i) No. of tank - 01
(ii) Length of tank – 50 metes (approx)
(iii) Rectifier - 8 sets(2 x 5500A)
(iv) Electrode - No of sets – 24
(8 anode sets, 16, cathode
sets)
8 Cells with combination of Cathode-Anode-
Cathode.
Tank made of MS lined with Brick & Rubber
Tank covers made of PP
2 Pair of Squeeze roll at Entry & Exit
Support roll arranged such as the strip moves in
23. Nitric electrolytic pickling sectionNitric electrolytic pickling section
HORIZONTAL RUTHNER ZIG ZAG DESIGN
(i) No. of tank - 01
(ii) Length of tank – 14 meters (approx)
(iii) Rectifier - 01 sets (2 x 5500A)
(iv) Electrode - No of sets - 06
(02 anode sets, 04 cathode
sets)
Pickling is effected in nitric acid by alternate anodic and
cathodic polarization of strip.
Low current density is used to just remove the passivation
layer from the strip so that the chemical reaction between
HNO3 and strip surface is enabled.
Disadvantage of the NITRIC acid being electrolyte is that
a higher current density NOx is produced.
DeNOx system is used for NOx emissions.
24. Mixed acid pickling sectionMixed acid pickling section
RUTHNER SHALLOW TANK DESIGN
Little acid amount but with high acid
circulation.
Mixed acid tanks.
(i) No. of tank - 02
(ii) Length of tank – 36 meters
approx (18 meters each)
In this section residual scale is removed,
chromium depleted layer is pickled and
brightening of strip surface is achieved.
HF is used because pure nitric acid would form
a passivation layer, thus preventing further
metal dissolution.
Me + 4HNO3 = Me(NO3)2 + NO + 2H2O
Me(NO3)3 + 3HF = MeF3 + 3HNO3
Me + HNO3 + 3HF = MeF3 + NO + 2H2O
26. Skin Pass MillSkin Pass Mill
Skin passing is done to
1. To improve strip shape
2. To impart the desired surface finish to steel from
2D to 2B
3. To produce desired mechanical properties.
4. To eliminate minor surface blemishes.
5. Masking of yield point
2 Hi Mill
Elongation 1.5%
Roll Cleaning system
Bottom Roll having Hydraulic Gap Control
Quick Roll Changing device;
Roll changing time ~ 8 minutes
Roll changing is possible during running
High Pressure Hydraulic system
2 High roll – 800mm (max.) /
750mm (min.) x 1500mm barrel length.
Roll force – Max. 10,000 KN
27. Tension LevellerTension Leveller
The purpose of tension levelling is to bring all the fibres
in the metal to equal length
To achieve Desired strip elongation(0-2%) and strip flatness
Tension leveller consists of Entry bridle, Tension leveller wet
type process, Exit bridles
Type – wet type.
Design – One set of bending roll cartridge
Two sets of anti cross bow roll cartridge
Tension – 350 KN (max.)
Roll configuration.
Bending roll module: 6 – High
Anti cross bow roll module: 3 – High
Roll sizes.
Bending: - work roll – 35mmØ x 1600mm
Intermediate roll - 50mmØ x 1600mm
Back up roll - 60mmØ x 130mm
Anti cross: - work roll – 150mmØ x 1600mm
Back up roll - 60mmØ x 130mm
29. Hydraulic cylinder
with integrated linear
transducer
Monoblo
c Frame
Passlin
e roll
Dry air
nozzle pipe
Bending
cartridge with
support rolls
protected by
purging air
Anti Cross
Bow
cartridge
with support
rolls
Adjustable
upper
cartridge
Cartridge clamping
cylinders
Servo valves
Fully enclosed Scale Breaker frame
Adjustable in
and outlet
Scale removal motor with
auger conveyor (Option)
LEVELLER IN MONOBLOC DESIGNLEVELLER IN MONOBLOC DESIGN
30. Exit EquipmentsExit Equipments
1 Recoiler with EPC Unit
Paper unwinder with Tension feedback unit
Pinch Rolls, Up Cut Shears, Belt Conveyor.
Bridles, Deflector, Steering rolls; PU coated
Roll dia 1000 mm x 1600mm.
Coil car with a provision to travel in other bay
4 Strands Dolly Type Looper; Storage capacity
566 m.
On line Weighing, Manual Strapping
Hydraulics & Pneumatic Systems