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Manufacture of Di-Methyl Formamide N. Khalid Ahmed & PremAnand A.S. 102106019 & 102106021 Under the Guidance of Dr. T. K. Radhakrishnan, Head of the Department,  Department of Chemical Engineering. National Institute of Technology, Tiruchirrappalli – 620 015 INDIA
Outline Background – Why DMF..?? Uses Structure and Properties Process Considered Chemistry Description Material and Energy Balances Design of Equipments Plant Location Cost Estimation Safety Considerations
Background - Uses 65-75% as solvent for fibers, 15-20% in production of pharmaceutical products. Also used as a laboratory solvent, and in the industry as an intermediate and an additive.
Background – Structure and Properties
Process Considered 4 Step proces involving raw materials methanol, ammonia and carbon monoxide Ammonia, Monomethyl amine and Trimethyl amine are recyclable Feed ratios  are maintained as per stoichiometry, and explained in the thesis.
Material and Energy Balances
Design Of Equipments Summary of Enriching Section Summary of Stripping Section Summary of Re-boiler Design Summary of Condenser Design Distillation Column Enriching Section Stripping Section Condenser Re-boiler
Plant Location Parameters considered: ,[object Object]
Process Requirements
Operation
Maintenance
Safety

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B Tech Project Viva

  • 1. Manufacture of Di-Methyl Formamide N. Khalid Ahmed & PremAnand A.S. 102106019 & 102106021 Under the Guidance of Dr. T. K. Radhakrishnan, Head of the Department, Department of Chemical Engineering. National Institute of Technology, Tiruchirrappalli – 620 015 INDIA
  • 2. Outline Background – Why DMF..?? Uses Structure and Properties Process Considered Chemistry Description Material and Energy Balances Design of Equipments Plant Location Cost Estimation Safety Considerations
  • 3. Background - Uses 65-75% as solvent for fibers, 15-20% in production of pharmaceutical products. Also used as a laboratory solvent, and in the industry as an intermediate and an additive.
  • 4. Background – Structure and Properties
  • 5. Process Considered 4 Step proces involving raw materials methanol, ammonia and carbon monoxide Ammonia, Monomethyl amine and Trimethyl amine are recyclable Feed ratios are maintained as per stoichiometry, and explained in the thesis.
  • 7. Design Of Equipments Summary of Enriching Section Summary of Stripping Section Summary of Re-boiler Design Summary of Condenser Design Distillation Column Enriching Section Stripping Section Condenser Re-boiler
  • 8.
  • 14.
  • 16. References Perry, R.H. and Green, D.W. – “Perry's Chemical Engineers' Handbook” - 7th Edition McGraw-Hill, 1997 Martyn S. Ray David W. Johnstan– “Chemical Engineering Design Project: A Case Study Approach” - 2nd Edition, 1978 McCabe, W., Smith, J. and Harriott, P -“Unit operations in Chemical Engineering” - 5th Edition, McGraw-Hill, 2004 Joshi M.V. and MahajaniV.V.– “Process Equipment Design” - 3rd Edition, MacMillan India Max S. Peters and KalusD.Timmerhaus - “Plant design and economics for chemical engineers” - 4th Edition, McGraw-Hill, 1991 Free patents online – Patent no:US4251460 Process for production of dimethyl formamdie.1981