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John Coupland
                  coupland@psu.edu
                   @JohnNCoupland
Flicker: chotda
Delay line              Sample             Brass Plate

Electrical spike

        Echo 1

        Echo 2



                         0.2



                                                                       Echo time
                         0.1

             Signal /V

                                                                 Echo amplitude
                         0.0




                         -0.1
                                                        Echo 1                      Echo 2


                                    Electrical spike
                         -0.2
                                0       5          10            15        20      25        30

                                                            Time / s
Oscilloscope trace

                               Amplitude=f(t)


                                         FFT


                            Magnitude=f(frequency)
                            Phase=f(frequency)

Magnitude           Phase
                                        Lab View


                            Properties = f(frequency)
Ultrasonic Properties of a Fluid
    Velocity (c)                             Attenuation ( )

                   amplitude (A)
0




                                   0




                    distance (x)
                    or time (t)


       c = d/t                         A = Ao e-   x

       c= f
Ultrasonic
  Measurements
are Not Interesting
              Flicker: jasonr611
Ultrasonic
property

                Physical
               constants


 Correlation
                   FOOD
                  QUALITY
Velocity
                           2
    c
            i       k                       Bulk modulus
                                               K+4/3G
2       f                            E          (K<<G)



    2           1
c                       1/”how many molecules there are
                        per unit volume and how hard is to
                        compress them”
Example: Position and Movement
• “The Lean-Meater can be thought of as
                                    an electronic ruler. Ultrasonic pulses
                                    sent into the animal are reflected back
                                    to the instrument from tissues of
                                    interest. The times until these echoes
                                    are received are translated into
                                    distances in mm. Measurements are
                                    non-invasive—no piercing of the skin
                                    with the consequent danger of
                                    infection. The animals are neither hurt
                                    nor irritated.”

http://www.rencocorp.com/lean-meater.htm
Position and Movement


      (2)



(3)




                (1)

                      Doppler image adapted from: L. Wang , K. L. McCarthy, M. J.
                      McCarthy, Food Research International 37 (2004) 633–642
Example: Liquid Composition




                          Flicker: mikeyexists
Blending Operation
Composition Measurement by Ultrasonic Velocity

                                    1800
       Ultrasonic velocity / ms-1




                                    1700


                                    1600


                                    1500


                                           0   10   20   30   40   50
                                 Concentration / wt%
( Sodium chloride,  ethanol,  glycerol,  sucrose, and  tomato ketchup)
1600
    Ultrasonic velocity /ms-1




                                1500


                                1400


                                1300       T1        T2


                                       0        20         40        60     80   100
                                                          Temperature /°C


() distilled water, () 20% sucrose solution, () corn oil, and a fine corn oil in water
emulsion () =10%, () =50%.
Olive Oil Processing Waste




J. Benedito *, A. Mulet, G. Clemente, J.V. Garcıa-Perez, Food Research International 37 (2004) 595–601
Example: Fat Melting




Flicker: dishevld
100% solid
       Solid Fat Content          Brittle solid


                                                     Hard solid



                                                         Spreadable solid


                                                                  Liquid
100% liquid
                           cold                                             hot
                                                  Temperature
Tristearin, tripalmitin or
 mixtures in paraffin
 oil, 25°C, 1 MHz




                 dc                1
                          3.1 ms
                 d




                                       (McClements and
                               20%     Povey, 1987)
0%
Chocolate
                  2200

                  2000
Velocity /ms -1


                  1800

                  1600

                  1400

                  1200
                         0   10   20   30   40   50   60
                                   Temp /oC
Crystallization cell for emulsions, fats and oils




                                           Chirp

Transducers




                 silvana.martini@usu.edu
Example: Particle Sizing




Flicker: bitzi ☂ ion-bogdan dumitrescu
35

               30
                                                Emulsion 3
               25
Frequency /%




                          Emulsion 5
               20

               15
                                                   Emulsion 1
               10

                5

                0
                    0.1                     1                   10
                                       Diameter / m
Scattering Mechanisms in Emulsions




Compression   Compression   Compression
Scattering from an Emulsion
        1460                                  0.03

        1450
-1




                                                     Np
                                              0.02
c /ms




        1440
                                              0.01
        1430
                                              0.00
               -7 -6 -5 -4 -3 -2 -1 0 1 2 3
                          log rf0.5
90
        1480
                                                                   80

                                                                   70
        1475
                                                                   60




                                                          /Npm-1
-1




                                                                   50
c /ms




        1470
                                                                   40

        1465                                                       30

                                                                   20

        1460                                                       10
               0      1    2     3      4   5         6                 0      1    2     3      4   5         6
                               f /MHz                                                   f /MHz


                   Velocity Spectra                                         Attenuation Spectra          Fig. 4b
                                            Fig. 4a
Particle Size Analysis
Concentrated dispersion characterization




                                             Dispersion Technology Inc DT-1200


            Dukhin AS, Goetz PJ, Advances in Colloid and Interface Science 92 (1-3): 73-132, 2001
Viscosity




 Flicker: Charlie P Barker
Impedance Measurements
                                2
                Ir   ( Z 2 Z1 )
            R                   2
                Ii   ( Z 2 Z1 )
            z    c

            Reflection coefficient
            is a measure of
            acoustic dissimilarity
Ultrasonic Viscometry
Normalized ultrasonic reflectance


                                                                      s20
                                    1.00
                                                                      s60
                                                                      s200
                                                                      s600
                                                                      s2000
                                    0.98



                                    0.96



                                    0.94


                                           0.01   0.1     1      10           100

                                                        / Pa.s
Advantages




             Flicker: monkeyc.net
Disadvantages




                     John Couplan
                     coupland@ps
Flicker: Or Hiltch   @JohnNCoup

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Ultrasonic characterization of foods

  • 1. John Coupland coupland@psu.edu @JohnNCoupland Flicker: chotda
  • 2. Delay line Sample Brass Plate Electrical spike Echo 1 Echo 2 0.2 Echo time 0.1 Signal /V Echo amplitude 0.0 -0.1 Echo 1 Echo 2 Electrical spike -0.2 0 5 10 15 20 25 30 Time / s
  • 3. Oscilloscope trace Amplitude=f(t) FFT Magnitude=f(frequency) Phase=f(frequency) Magnitude Phase Lab View Properties = f(frequency)
  • 4. Ultrasonic Properties of a Fluid Velocity (c) Attenuation ( ) amplitude (A) 0 0 distance (x) or time (t) c = d/t A = Ao e- x c= f
  • 5. Ultrasonic Measurements are Not Interesting Flicker: jasonr611
  • 6. Ultrasonic property Physical constants Correlation FOOD QUALITY
  • 7. Velocity 2 c i k Bulk modulus K+4/3G 2 f E (K<<G) 2 1 c 1/”how many molecules there are per unit volume and how hard is to compress them”
  • 9. • “The Lean-Meater can be thought of as an electronic ruler. Ultrasonic pulses sent into the animal are reflected back to the instrument from tissues of interest. The times until these echoes are received are translated into distances in mm. Measurements are non-invasive—no piercing of the skin with the consequent danger of infection. The animals are neither hurt nor irritated.” http://www.rencocorp.com/lean-meater.htm
  • 10. Position and Movement (2) (3) (1) Doppler image adapted from: L. Wang , K. L. McCarthy, M. J. McCarthy, Food Research International 37 (2004) 633–642
  • 11. Example: Liquid Composition Flicker: mikeyexists
  • 13. Composition Measurement by Ultrasonic Velocity 1800 Ultrasonic velocity / ms-1 1700 1600 1500 0 10 20 30 40 50 Concentration / wt% ( Sodium chloride,  ethanol,  glycerol,  sucrose, and  tomato ketchup)
  • 14. 1600 Ultrasonic velocity /ms-1 1500 1400 1300 T1 T2 0 20 40 60 80 100 Temperature /°C () distilled water, () 20% sucrose solution, () corn oil, and a fine corn oil in water emulsion () =10%, () =50%.
  • 15. Olive Oil Processing Waste J. Benedito *, A. Mulet, G. Clemente, J.V. Garcıa-Perez, Food Research International 37 (2004) 595–601
  • 17. 100% solid Solid Fat Content Brittle solid Hard solid Spreadable solid Liquid 100% liquid cold hot Temperature
  • 18. Tristearin, tripalmitin or mixtures in paraffin oil, 25°C, 1 MHz dc 1 3.1 ms d (McClements and 20% Povey, 1987) 0%
  • 19. Chocolate 2200 2000 Velocity /ms -1 1800 1600 1400 1200 0 10 20 30 40 50 60 Temp /oC
  • 20. Crystallization cell for emulsions, fats and oils Chirp Transducers silvana.martini@usu.edu
  • 21. Example: Particle Sizing Flicker: bitzi ☂ ion-bogdan dumitrescu
  • 22. 35 30 Emulsion 3 25 Frequency /% Emulsion 5 20 15 Emulsion 1 10 5 0 0.1 1 10 Diameter / m
  • 23. Scattering Mechanisms in Emulsions Compression Compression Compression
  • 24. Scattering from an Emulsion 1460 0.03 1450 -1 Np 0.02 c /ms 1440 0.01 1430 0.00 -7 -6 -5 -4 -3 -2 -1 0 1 2 3 log rf0.5
  • 25. 90 1480 80 70 1475 60 /Npm-1 -1 50 c /ms 1470 40 1465 30 20 1460 10 0 1 2 3 4 5 6 0 1 2 3 4 5 6 f /MHz f /MHz Velocity Spectra Attenuation Spectra Fig. 4b Fig. 4a
  • 26. Particle Size Analysis Concentrated dispersion characterization Dispersion Technology Inc DT-1200 Dukhin AS, Goetz PJ, Advances in Colloid and Interface Science 92 (1-3): 73-132, 2001
  • 28. Impedance Measurements 2 Ir ( Z 2 Z1 ) R 2 Ii ( Z 2 Z1 ) z c Reflection coefficient is a measure of acoustic dissimilarity
  • 29. Ultrasonic Viscometry Normalized ultrasonic reflectance s20 1.00 s60 s200 s600 s2000 0.98 0.96 0.94 0.01 0.1 1 10 100 / Pa.s
  • 30. Advantages Flicker: monkeyc.net
  • 31. Disadvantages John Couplan coupland@ps Flicker: Or Hiltch @JohnNCoup