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International Journal of Advanced Engineering Technology E-ISSN 0976-3945
IJAET/Vol.II/ Issue III/July-September,2011/10-13
Research Article
FRICTION STIR WELDED JOINTS OF CAST SCANDIUM
ADDED ALUMINUM-MAGNESIUM ALLOY
K.Subbaiah1
, Geetha Manivasagam2
, Govindarajan3
, S.R.K.Rao4
Address for Correspondence
1
Sri Sivasubramaniya Nadar College of Engineering, Chennai, Tamil Nadu, India.
2
SMBS, VIT University, Vellore, Tamil Nadu, India.
3
Center for Non-Ferrous Technology Development Center, Hyderabad.
4
Tagore Engineering College, Chennai, Tamilnadu , India
E Mail subbaiahk@ssn.edu.in
ABSTRACT:
Cast scandium added aluminum-magnesium alloy was friction stir welded, and the tensile properties of the global joint
and its component parts were examined and analyzed. The weld composed of weld nugget and thermo-mechanically
affected zone exhibited better mechanical properties than the base metal. The global joint fractured in the base material,
and thus possessed slightly greater tensile strength than the base metal. These results clearly show that friction stir
welding is an optimum welding process for cast Al-Mg-Sc alloys.
KEYWORDS: Friction stir welding, cast Al-Mg-Sc alloy, mechanical properties.
INTRODUCTION:
Cast aluminum alloys are widely used in the
transportation industries and can be arc welded
(either Metal Inert Gas or Tungsten Inert Gas
welding) in a protective atmosphere or joined by
brazing.[1] Unfortunately, the welding production
cost is relatively high and some welding defects
such as porosity and slag inclusion are easily
formed in the weld. Friction Stir welding (FSW) is
a promising process that can produce high quality,
low cost joints [2]. This welding process is being
extensively and intensively studied in order to weld
various types of wrought aluminum alloys,
especially Non-heat-treatable aluminum alloys [3-
9]. It is also being developed to weld other
materials such as magnesium, inconel, titanium,
invar, brass, steel, and aluminum matrix
composites [10-18]. Scandium is classified among
3d transition metals and, hence, its reaction with
aluminum has salient features inherent in reaction
of other 3d transition metals with aluminum.
Scandium is one of the most effective modifiers of
a cast grain structure in aluminum alloys.
Continuously cast commercial scandium-bearing
aluminum alloy ingots have, as a rule, a
nondendritic structure which has no internal
structure (its grains are not divided into small
constituents) and shows geometrical equality of
grains and the dendritic parameters. The ability of
scandium to refine grains is used in the case of
fusion welding of aluminum alloys;
susceptibility of the alloys to crack formation
reduces sharply, while mechanical properties of
weld joints increase noticeably [19]. Scandium
tends to formation of anomalous supersaturated
solid solutions at rather low cooling rates
feasible in casting of rather large ingots. In
heating, scandium solid solution in aluminum
decomposes to form Al3Sc dispersed particles,
which makes a great contribution to
strengthening of the alloy [20]. In this study, a
Cast Scandium added Aluminum- Magnesium
alloy was selected as the experimental material
to demonstrate the feasibility of FSW. Emphasis
is placed on the mechanical properties such as
yield stress, ultimate tensile strength and
percentage elongation of the joint.
EXPERIMENTALmPROCEDURE:
The starting materials used in the preparation of
the experimental cast Al-Mg-Sc alloy were AA
5083 alloy and Al-2% master alloy. Appropriate
amounts of the starting materials were melted in
a vacuum induction melted furnace to produce an
Al-Mg-Sc alloy with a nominal composition
similar to AA 5083 with 0.29 wt % Sc addition.
The chemical composition of the alloy was
analyzed by inductively coupled plasma atomic
emission spectroscopy. The aluminum alloy
studied in the present experiment is having
chemical composition of (in wt %) Mg-4.214,
International Journal of Advanced Engineering Technology E-ISSN 0976-3945
IJAET/Vol.II/ Issue III/July-September,2011/10-13
Mn-0.787, Fe- 0.407, Si-0.165, Zn-0.12, Cu- 0.025,
Cr- 0.01, Ti- 0.01, Sc-0.29 and the rest aluminum.
Bead-on-plate Friction Stir Welding was applied to
the 5 mm thick cast Al-Mg-Sc material. Rotation
speed of the welding tool was 650 rpm, and the
traverse speed was 158 mm/min. A vertical plunge
force of 17 KN was applied over the tool. Features
for the welding tool included a shoulder diameter
of 15 mm, a pin diameter of 5 mm on the top and 4
mm on the bottom and a pin length of 4.7 mm
(Fig.1.). The utilized tool was made in M2 steel
having chemical composition of (in wt %) C-0.85,
Cr-4.0, W-6.0, Mo-5.0, V-2.0, and rest iron. The
high speed tool was quenched at 10200
C,
characterized by a 50 ~55 HRc hardness. An
indigenously designed and developed machine (30
KN; 3000 RPM; 15 HP) has been used to fabricate
the joints. After welding, the joints were cross-
sectioned perpendicular to the welding direction
for metallographic analyses. Specimens for tensile
tests were cut using an EDM machine. The tensile
properties of the joint and its component parts were
measured by conducting tensile tests on universal
testing machine. The configuration and size of the
transverse tensile specimens were prepared
according to Fig.2, in which different size
specimens were used to determine the mechanical
properties of the joint and its component parts.
Fig.1. photograph of friction stir welding tool.
Fig. 2 a) Global joint (ASTM-E8 standard
specimen)
Fig. 2 b) component joint part (Small)
Fig. 2 c) component joint part (Very small)
RESULTS AND DISCUSSIONS:
Tensilekproperties:
The average values of the tensile properties of
cast Al-Mg-Sc alloy plate, i.e., yield stress;
ultimate tensile stress and percentage
elongation are 203 MPa, 214MPa and 7%
respectively. With regard to the global joint,
the yield stress, the ultimate tensile strength,
and percentage elongation are 207 MPa, 232
MPa, and 6.8 % respectively. The joint is
fractured in base metal far distant from the
weld. The weld properties are better than the
base metal properties. This correlates well
with the earlier results corresponding to cast
aluminum alloys [21& 22].
In order to further evaluate the tensile
properties of the weld nugget, the gauge length
of the tensile specimens was reduced to 15 mm
(Fig.2). The yield stress, the ultimate tensile
strength, and percentage elongation of the
weld nugget were measured to be 212 MPa,
242 MPa, and 5.6 % respectively. This
indicates that the tensile properties of the weld
nugget are much higher than those of the base
metal. This result also denotes that the weld
nugget is also shown to have higher tensile
International Journal of Advanced Engineering Technology E-ISSN 0976-3945
IJAET/Vol.II/ Issue III/July-September,2011/10-13
properties than the thermo-mechanically affected
zone of the joint.
In order to further evaluate the tensile properties
of the weld, the gauge length of the tensile
specimens was reduced to 4 mm [Fig .2]. The
yield stress, the ultimate tensile strength, and the
percentage of elongation of the weld were
measured to be 232 MPa, 259 MPa, and 11%
respectively. This indicates that the tensile
properties of the weld are much higher than
those of the base metal. The best values for the
FSW welded cast aluminum-magnesium-
scandium alloy were found as 253 MPa, 287
MPa, and 11 % for the yield stress, ultimate
tensile strength, and the percentage of elongation
respectively. When we compare this value with
the highest values obtained for the base metal
values of cast Al-Mg-Sc alloy, the FSW weld
has produced better tensile properties because of
grain refinement in the microstructure and
elimination of casting voids from the welded
portion.
TENSILE PROPERTIES
203 214207
230
212
242232
259
0
50
100
150
200
250
300
YIELD UTS
STRESS,MPa
Base
Global
Small
V.Small
Fig.3.Tensile properties
DUCTILITY PROPERTIES
7 6.8
5.6
11
0
2
4
6
8
10
12
% EL
%,ELONGATION
Base
Global
Small
V.Small
Fig.4. Ductility properties
CONCLUSIONS
1. The tensile properties of the component
parts are better than the tensile properties
of the global joints.
2. The tensile failure occurred in the global
joint at the base metal, whereas, the
failures occurred in the weld nugget in the
case of component joints.
3. The best values of yield stress, ultimate
tensile strength, and percentage elongation
for the Friction Stir Welded cast Al-Mg-
Sc aluminum alloy plates are 253 MPa,
287 MPa, and 11 % respectively.
REFERENCES
1. Lathabai.S, and Lioyd.P.G.,“ The effect
of scandium on the microstructure,
mechanical properties and weldability of
a cast Al-Mg alloy” Acta. Mater., 2002,
50, 4275-4292.
2. Thomas.W.M, Nicholas.E.D,
Needam.J.C, Murch.M.G, Templesmith.P,
and Dawes.C.J., 1991, GB Patent
application No. 9125978.8.
3. Hirata.T, Oguri.T, Hagino.H, Tanaka.T,
Chung.S.W, Takigawa.Y, and Higashi.K,
Mater.Sci.Eng.A 456 (2007) 344-349.
4. Fujii.H, Cui.L,Maeda.M, and Nogi.K,
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6. Shigematsu.I, Kwon.Y.-J, Suzuki.K,
Imai.T, and Saito.N, J.Mater. Sci. Letters.
22 2003, 353-356.
7. Sato.Y.S, Hwan.S, Park.C, and
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8. Svensson.L.-E, Karlsson.L, Larsson.H,
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9. Lombard.H, Hattingh.D.G, Steuwar.A,
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10. Won-Bae Lee, Jong- Woong Kim, Yun-
Mo Yeon, and Seung-Boo Jung “ The
joint Characteristics of friction stir welded
AZ91D Magnesium alloy”
Mater.Trans.Vol.44 No.5 (2003) PP 917-
923.
11. F.Yu, H. Fujii, T. Tsumura, and K.
Nakata " Friction stir welding of Inconel
alloy 600 " J.of Mater. Sci. (2006) 41
5376-5379.
12. W.B.Lee, C.Y.Lee, W.S.Chang,
Y.M.Yeon, and S.B.Jung "
International Journal of Advanced Engineering Technology E-ISSN 0976-3945
IJAET/Vol.II/ Issue III/July-September,2011/10-13
Microstructural investigation of friction stir
welded pure titanium " Mater.Lett. 59
(2005) 3315-3318.
13. K.Reshad Seighalani, M.K.Besharati Givi,
A.M.Nasiri, and P.Bahemmat "
Investigations on the Effects of the Tool
Material, Geometry, and Tilt angle on
Friction Stir Welding of Pure Titanium "
ASM International-Journal of Materials
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online: 10 December 2009.
14. Bharat K. Jasthi, William J. Arbegast, and
Stanley M. Howard " Thermal Expansion
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Friction Stir Welded Invar (Fe-36%Ni) "
ASM International-Journal of Materials
Engineering and Performance, Vol. 18(7)
October 2009, 925-934.
15. C.Meran: ' weldability of brass materials and
determination of available welding
parameters ', PhD Thesis, Pamukkale
University, Denizli, Turkey, 2001. (in
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16. A.P.Reynolds, W.Tang, M.Posada and
J.DeLoach “Friction Stir Welding of DH36
steel” Sci.Technol.Weld.Joi. 2003 Vol.8
No.6 PP 455-460.
17. A.P.Reynolds, Wei Tang, T.Gnaupel-
Herold, and H.Prask “Structure, properties,
and residual stress of 304L stainless steel
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18. M.Amirizad, A.H.Kokabi, M.Abbasi
Gharacheh, R.Sarrafi, B.Shalchi, and
M.Azizieh " Evaluation of microstructure
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Mater.Lett. 60 (2006) 565-568.
19. V.G.Davydov, T.D.Rostova, V.V.Zakharov,
Yu.A.Filatov, and V.I.Yelagin, "Scientific
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Article 2 ijaet volii issue iii july sept 2011

  • 1. International Journal of Advanced Engineering Technology E-ISSN 0976-3945 IJAET/Vol.II/ Issue III/July-September,2011/10-13 Research Article FRICTION STIR WELDED JOINTS OF CAST SCANDIUM ADDED ALUMINUM-MAGNESIUM ALLOY K.Subbaiah1 , Geetha Manivasagam2 , Govindarajan3 , S.R.K.Rao4 Address for Correspondence 1 Sri Sivasubramaniya Nadar College of Engineering, Chennai, Tamil Nadu, India. 2 SMBS, VIT University, Vellore, Tamil Nadu, India. 3 Center for Non-Ferrous Technology Development Center, Hyderabad. 4 Tagore Engineering College, Chennai, Tamilnadu , India E Mail subbaiahk@ssn.edu.in ABSTRACT: Cast scandium added aluminum-magnesium alloy was friction stir welded, and the tensile properties of the global joint and its component parts were examined and analyzed. The weld composed of weld nugget and thermo-mechanically affected zone exhibited better mechanical properties than the base metal. The global joint fractured in the base material, and thus possessed slightly greater tensile strength than the base metal. These results clearly show that friction stir welding is an optimum welding process for cast Al-Mg-Sc alloys. KEYWORDS: Friction stir welding, cast Al-Mg-Sc alloy, mechanical properties. INTRODUCTION: Cast aluminum alloys are widely used in the transportation industries and can be arc welded (either Metal Inert Gas or Tungsten Inert Gas welding) in a protective atmosphere or joined by brazing.[1] Unfortunately, the welding production cost is relatively high and some welding defects such as porosity and slag inclusion are easily formed in the weld. Friction Stir welding (FSW) is a promising process that can produce high quality, low cost joints [2]. This welding process is being extensively and intensively studied in order to weld various types of wrought aluminum alloys, especially Non-heat-treatable aluminum alloys [3- 9]. It is also being developed to weld other materials such as magnesium, inconel, titanium, invar, brass, steel, and aluminum matrix composites [10-18]. Scandium is classified among 3d transition metals and, hence, its reaction with aluminum has salient features inherent in reaction of other 3d transition metals with aluminum. Scandium is one of the most effective modifiers of a cast grain structure in aluminum alloys. Continuously cast commercial scandium-bearing aluminum alloy ingots have, as a rule, a nondendritic structure which has no internal structure (its grains are not divided into small constituents) and shows geometrical equality of grains and the dendritic parameters. The ability of scandium to refine grains is used in the case of fusion welding of aluminum alloys; susceptibility of the alloys to crack formation reduces sharply, while mechanical properties of weld joints increase noticeably [19]. Scandium tends to formation of anomalous supersaturated solid solutions at rather low cooling rates feasible in casting of rather large ingots. In heating, scandium solid solution in aluminum decomposes to form Al3Sc dispersed particles, which makes a great contribution to strengthening of the alloy [20]. In this study, a Cast Scandium added Aluminum- Magnesium alloy was selected as the experimental material to demonstrate the feasibility of FSW. Emphasis is placed on the mechanical properties such as yield stress, ultimate tensile strength and percentage elongation of the joint. EXPERIMENTALmPROCEDURE: The starting materials used in the preparation of the experimental cast Al-Mg-Sc alloy were AA 5083 alloy and Al-2% master alloy. Appropriate amounts of the starting materials were melted in a vacuum induction melted furnace to produce an Al-Mg-Sc alloy with a nominal composition similar to AA 5083 with 0.29 wt % Sc addition. The chemical composition of the alloy was analyzed by inductively coupled plasma atomic emission spectroscopy. The aluminum alloy studied in the present experiment is having chemical composition of (in wt %) Mg-4.214,
  • 2. International Journal of Advanced Engineering Technology E-ISSN 0976-3945 IJAET/Vol.II/ Issue III/July-September,2011/10-13 Mn-0.787, Fe- 0.407, Si-0.165, Zn-0.12, Cu- 0.025, Cr- 0.01, Ti- 0.01, Sc-0.29 and the rest aluminum. Bead-on-plate Friction Stir Welding was applied to the 5 mm thick cast Al-Mg-Sc material. Rotation speed of the welding tool was 650 rpm, and the traverse speed was 158 mm/min. A vertical plunge force of 17 KN was applied over the tool. Features for the welding tool included a shoulder diameter of 15 mm, a pin diameter of 5 mm on the top and 4 mm on the bottom and a pin length of 4.7 mm (Fig.1.). The utilized tool was made in M2 steel having chemical composition of (in wt %) C-0.85, Cr-4.0, W-6.0, Mo-5.0, V-2.0, and rest iron. The high speed tool was quenched at 10200 C, characterized by a 50 ~55 HRc hardness. An indigenously designed and developed machine (30 KN; 3000 RPM; 15 HP) has been used to fabricate the joints. After welding, the joints were cross- sectioned perpendicular to the welding direction for metallographic analyses. Specimens for tensile tests were cut using an EDM machine. The tensile properties of the joint and its component parts were measured by conducting tensile tests on universal testing machine. The configuration and size of the transverse tensile specimens were prepared according to Fig.2, in which different size specimens were used to determine the mechanical properties of the joint and its component parts. Fig.1. photograph of friction stir welding tool. Fig. 2 a) Global joint (ASTM-E8 standard specimen) Fig. 2 b) component joint part (Small) Fig. 2 c) component joint part (Very small) RESULTS AND DISCUSSIONS: Tensilekproperties: The average values of the tensile properties of cast Al-Mg-Sc alloy plate, i.e., yield stress; ultimate tensile stress and percentage elongation are 203 MPa, 214MPa and 7% respectively. With regard to the global joint, the yield stress, the ultimate tensile strength, and percentage elongation are 207 MPa, 232 MPa, and 6.8 % respectively. The joint is fractured in base metal far distant from the weld. The weld properties are better than the base metal properties. This correlates well with the earlier results corresponding to cast aluminum alloys [21& 22]. In order to further evaluate the tensile properties of the weld nugget, the gauge length of the tensile specimens was reduced to 15 mm (Fig.2). The yield stress, the ultimate tensile strength, and percentage elongation of the weld nugget were measured to be 212 MPa, 242 MPa, and 5.6 % respectively. This indicates that the tensile properties of the weld nugget are much higher than those of the base metal. This result also denotes that the weld nugget is also shown to have higher tensile
  • 3. International Journal of Advanced Engineering Technology E-ISSN 0976-3945 IJAET/Vol.II/ Issue III/July-September,2011/10-13 properties than the thermo-mechanically affected zone of the joint. In order to further evaluate the tensile properties of the weld, the gauge length of the tensile specimens was reduced to 4 mm [Fig .2]. The yield stress, the ultimate tensile strength, and the percentage of elongation of the weld were measured to be 232 MPa, 259 MPa, and 11% respectively. This indicates that the tensile properties of the weld are much higher than those of the base metal. The best values for the FSW welded cast aluminum-magnesium- scandium alloy were found as 253 MPa, 287 MPa, and 11 % for the yield stress, ultimate tensile strength, and the percentage of elongation respectively. When we compare this value with the highest values obtained for the base metal values of cast Al-Mg-Sc alloy, the FSW weld has produced better tensile properties because of grain refinement in the microstructure and elimination of casting voids from the welded portion. TENSILE PROPERTIES 203 214207 230 212 242232 259 0 50 100 150 200 250 300 YIELD UTS STRESS,MPa Base Global Small V.Small Fig.3.Tensile properties DUCTILITY PROPERTIES 7 6.8 5.6 11 0 2 4 6 8 10 12 % EL %,ELONGATION Base Global Small V.Small Fig.4. Ductility properties CONCLUSIONS 1. The tensile properties of the component parts are better than the tensile properties of the global joints. 2. The tensile failure occurred in the global joint at the base metal, whereas, the failures occurred in the weld nugget in the case of component joints. 3. The best values of yield stress, ultimate tensile strength, and percentage elongation for the Friction Stir Welded cast Al-Mg- Sc aluminum alloy plates are 253 MPa, 287 MPa, and 11 % respectively. REFERENCES 1. Lathabai.S, and Lioyd.P.G.,“ The effect of scandium on the microstructure, mechanical properties and weldability of a cast Al-Mg alloy” Acta. Mater., 2002, 50, 4275-4292. 2. Thomas.W.M, Nicholas.E.D, Needam.J.C, Murch.M.G, Templesmith.P, and Dawes.C.J., 1991, GB Patent application No. 9125978.8. 3. Hirata.T, Oguri.T, Hagino.H, Tanaka.T, Chung.S.W, Takigawa.Y, and Higashi.K, Mater.Sci.Eng.A 456 (2007) 344-349. 4. Fujii.H, Cui.L,Maeda.M, and Nogi.K, Mater. Sci. Eng. A 419 (2006) 25-31. 5. Watanabe.T, Takayama.H, and Yanagisawa.A, J.Mater. Process. Technol. 178 (2006) 342-349. 6. Shigematsu.I, Kwon.Y.-J, Suzuki.K, Imai.T, and Saito.N, J.Mater. Sci. Letters. 22 2003, 353-356. 7. Sato.Y.S, Hwan.S, Park.C, and Kokawa.H, Metall.Mater.Trans.A 2001; 32 A: 3033. 8. Svensson.L.-E, Karlsson.L, Larsson.H, Karlsson.B, and Fazzini.M, Karlsson.J. Sci.Technol.Weld. Joi. 2000, vol.5, No.5, 285-296. 9. Lombard.H, Hattingh.D.G, Steuwar.A, and James.M.N. Eng. Fra. Mech.75 (2008), 341-354. 10. Won-Bae Lee, Jong- Woong Kim, Yun- Mo Yeon, and Seung-Boo Jung “ The joint Characteristics of friction stir welded AZ91D Magnesium alloy” Mater.Trans.Vol.44 No.5 (2003) PP 917- 923. 11. F.Yu, H. Fujii, T. Tsumura, and K. Nakata " Friction stir welding of Inconel alloy 600 " J.of Mater. Sci. (2006) 41 5376-5379. 12. W.B.Lee, C.Y.Lee, W.S.Chang, Y.M.Yeon, and S.B.Jung "
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