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Linkam Scientific Instruments Ltd
Tel: +44 (O) 1737 363 476
Fax: +44 (O) 1737363480
support@linkam.co.uk
Unit 8, Epsom Downs Metro Centre
Tadworth,Surrey, KT20 5lR, UK
f-/ww.iinkam.co.uk
V1.0.2.1609
LNP95
Liquid Nitrogen Pump Cooling System
USER GUIDE
I
Contents
LNP95 Liquid Nitrogen Pump Cooling System...............................................................................7
Remove Transit Screws.....................................................................................................7
Front Panel Tubing Connections........................................................................................8
Back Panel Cable Connections..........................................................................................8
Filling the Dewar with Liquid Nitrogen............................................................................................9
~§i1~:'.~~"o~~;j~
2
IUDltiiiil Declaration of Conformity
Manufacturers Name:
Manufacturers Address:
Linkam Scientific Instruments Ltd
8 Epsom Downs Metro Centre
Waterfield
Tadworth
Surrey
KT205LR
UK
Declares that the product as originally delivered:
Product Name:
Product Number:
Liquid Nitrogen Pump
LNP95
has been independently tested and found to comply w,ith the following
European Directives, and carries the CE marking accordingly:
EMC Directive 2004/108IEC using product standard EN 61326-1:2006
Low Voltage Directive 2006/95IEC using product stai;idard EN 61010-1:2001
and also carries the additional certification:
EMC
Safety
FCC CFR47 Part 15
CB IEC 61010-11 EN 61010-1
MET UL 61010-11 CSA C22.2 No.61010-1 under listing EI12928
28th August 2009
Date
3
Peter Grocutt
R&D Manager
applicable
Important Notice
Please check that your Linkam equipment has not been damaged during transport.
Ifthere is any evidence ofexternal damage to electrical items:
DO NOT CONNECT THE POWER CORD OR SWITCH THE ITEM ON
Contact Linkam Scientific or their appointed distributor immediately. Your warranty may be
impaired if Linkam is not informed ofany transport damage within 7 working days ofdelivery.
Safety Precautions
I)
2)
3)
4)
5)
6)
7)
8)
Read all ofthis guide before using the equipment. Save these instructions for later use.
Follow all warnings and instructions, marked on any of your Linkam equipment, or
contained within the manuals.
If for any reason the mains fuse needs to be replaced then it must be replaced by one of the same
type and rating as shown in the equipment ratings.
To prevent electric shock, do not remove the cover ofthe equipment.
Never use the equipment if the power cord has been damaged. Do not allow any heavy objects to
rest on the power cord. Never lay the power cord on the floor.
Do not obstruct any ventilation holes. Do not attempt to insert anything into these
openings. Provide adequate ventilation ofat least 75mm all around the equipment.
Do not expose the equipment to water. If for any reason it gets wet then remove the power cord
from the mains outlet and contact Linkam Scientific Technical Support.
The equipment is not intended to be used outdoors.
Each product is equipped with a 3-wire grounded (earth) power plug or a free-end 3 wire power
cord. The plug only fits into a grounded-type outlet. The free-end power cord should be con-
nected to a correctly grounded 3-wire power outlet. Do not defeat the purpose of the grolli,ld~
(earth) type plug.
Free - end power cords are colour coded as follows:
Colour
Brown
Blue
GreenlYellow
Function
Live
Neutral
Earth (Ground)
9) The power cord must be an appropriately rated and approved cord-set for the country it is being
used in.
10) If any problems occur then remove the power cord from the mains outlet and contact Linkam
Scientific Technical Support.
11) No attempt should be made to repair or ~odify the equipment in any way, as there are no user
replaceable parts. Any servicing should be carried out by qualified service personnel. Do not
remove the cover from the equipment unless the power cord has been removed from the mains
outlet.
4
Symbol Reference
This safety symbol is seen on the back panel ofthe equipment and warns the user:
Not to make or remove any connections while the unit is powered on.
Not to remove the cover.
Servicing should only be done by qualified service personnel.
It can also be seen on the Dewar for liquid nitrogen and warns the user:
Of the potential dangers in handling liquid nitrogen, especially the exposure to skin and of
asphyxiation in an enclosed space.
Please refer to your safety supervisor for special handling instructions.
This safety symbol is seen on the back panel ofthe equipment and warns the user:
That to avoid electric shock the power cord protective grounding conductor must be con-
nected to ground.
.'
5
Equipment Ratings
A.c. Mains Supply:
A.C. Frequency:
Maxcurrent:
Fuse:
100-240-
47-63Hz
1.7A
Current rating
Characteristic
Voltage rating
Breaking capacity
TechniCal Specification
Dimensions:
Weight:
376Lx 243W x 87H (mm)
3.6Kg (excluding cables)
2A
T
250V-
H
Operating environment: 5- 40°C, 80% relative humidity at 31°C decreasing linearly to 50% at
40°C (without condensation)
Tubing: Silicon rubber
Warranty
This equipment has a warranty against defects in material and workmanship for a period of 12 months.
Linkam will either repair or replace products that prove to be defective. For warranty service or repair, this
product must be returned to Linkam or a designated service facility.
The warranty shall not apply to defects resulting from interfacing, unauthorized modification or misuse,
operation o~tside of the environmental specifications for the product, or improper site preparation or main-
tenance.
Technical Support
Any technical questions or queries should be addressed.to the Technical Support Department at the ad-
dress shown on the back ofthis manual.
Equipment Maintenance
The LNP95 does not require any regular maintenance. Contact Linkam should you require any mainte-
nance.
Before cleaning the case or front panel of the LNP95, remove the mains cord from the mains
outlet. Use a small quantity of isopropyl alcohol on a soft cloth and gently wipe the surface.
. Product Registration
Register your Linkam instrument and software; please go to www.linkam.co.uk to fill in the Product
software Registration form. After registration, you can login to our website to download manuals and
access 'How To Videos'. .
Feedback
Your feedback will be greatly appreciated, please go to www.linkam.co.uk to fill in the Feedback form.
6
i
1
Introduction
Thank you for purchasing a Linkam instrument.
Please take the time to read through the manual
as it will help you to make the most out of the
equipment.
L.NP95 Liquid Nitrogen Pump
Cooling System
P.I,e)iSe check;that all of the following parts have
been supplied with the LNP95 System.
1.. LNP95
2. 2L Dewar with siphon assembly
(7L and 25L is available)
3. Instrument bus cable
4~ fPo~t:r cord
Remove Transit Screws
~Before using the LNP95 Liquid Nitrogen Pump
System, remove the 4 transit screws marked by
small yellow labels (5), from the base of the
LNP95. Transit screws shown by arrows in the
adjacent image. These screws hold the pumps in
plaCe for shipping.
Keep the screws safe by screwing them into the
holes on the back panel as shown by the arrows.
The screws must be replaced back into the transit
hples on the ~ase, when shipping back to Linkam
for service or repair.
7
Front Panel Tubing Connections
Refer to your hotstage manual for the connection
oftubing.
1. Window purge tube
2. Stage purge tube and connector
Back Panel Cable Connections
3. Main power socket
4. .Fuse box housing
5. Instrument bus (CAN) Sockets
6. USB socket. Do not use
7. Transit screws storage
Connect the Instrument Bus Cable (9) between
the LNP95 and T95 as shown.
Note: either of the purple coloured Instrument
Bus Sockets (5) on the LNP95 can be used.
Plug the power cord into the power socket and
push power switch (8).on the front of the LNP95
to tum it on or off.
LNP95 MUST BE SWITCHED ON BE~
FORE T95SY~TEM CONTROLLER.
8
Filling the Dewar with liquid
nitrogen
Please follow your health and safety manual for
directions on how to handle liquid nitrogen and
ensure that you have the correct safety equipment
including gloves and safety goggles.
Fill'i.tlte;Dewar approximately 2/3 full and replace
tj;I~,lid~th siphon attached.
~ ft;;6;';:,'~·;~ : '; ,:,' ~
DO NOT FASTEN THE CATCHES
Wait for the nitrogen to stop bubbling before
fastening the catches.
Take care when placing lid on a table to always
have the black capillary pointing upwards. It is
~asily damaged which will impair N2f1ow,
Operation
The LNP95 is controlled by the T95 temperature
System Controller that it is connected with. The
T95 temperature programmer is either controlled
by LinkPadtouch screen display, or by the Link-
sys32 computer software, details of how to con-
-trol the LNP95 can be found in the manuals for
these products.
LinkPad touch screen display
Linksys32 computersoftware
9
Appendix
Spares and Accessories
0994 DF Standard 2L Dewar
9588 DF2 Standard 2L Dewar (inc!. Lid and Siphon Assembly) Specify Stage Model
9590 SSDF2 2L Stainless Steel Dewar (Inc!. Lid and Siphon Assembly) Specify Stage Model
9592 D2L
Dewar Siphon Assembly 39cm (no Dewar lid and need to specify Stage Model) -
achieves a stage temperature of-196°C on THMS600IFTIR6001LTS350
9524 02L
Dewar Siphon Assembly 80cm (no Dewar lid and need to specify Stage Model)-
achieves a stage temperature of-120°C on THMS600tFTIR600
9808 02L
Dewar Siphon Assembly 100cm (no Dewar lid and need to specify Stage Model)-
achieves a stage temperature of-50°C on THMS600IFTIR600
9598 DS2 Extra Long Dewar Siphon Assembly for 25L Taylor Wharton "Classic" Dewar
· 5647 TWC25 25L Dewar Flask - Taylor Wharton Classic (without siphon)
This page is intentionally blank
9599 LNPTU Silicon Tubing & Connectors between LNP & Stage
7018 SILTUl Silicon Purge Tube LNP to Stage (2mm ID x 4mm OD)
19075 CANC Instrument Bus (CAN) Cable to connect LNP95 and T95
9850 DF7 Standard 7L Dewar (inc!. Lid and Siphon Assembly) Specify Stage Model
9851 DF7 7L Dewar (inc!. Lid but no Siphon Assembly)
9852 D7L Siphon Assembly for 7L Dewar need to specify Stage Model
10 11

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Liquid Nitrogen Pump Cooling System

  • 1. Linkam Scientific Instruments Ltd Tel: +44 (O) 1737 363 476 Fax: +44 (O) 1737363480 support@linkam.co.uk Unit 8, Epsom Downs Metro Centre Tadworth,Surrey, KT20 5lR, UK f-/ww.iinkam.co.uk V1.0.2.1609 LNP95 Liquid Nitrogen Pump Cooling System USER GUIDE I
  • 2. Contents LNP95 Liquid Nitrogen Pump Cooling System...............................................................................7 Remove Transit Screws.....................................................................................................7 Front Panel Tubing Connections........................................................................................8 Back Panel Cable Connections..........................................................................................8 Filling the Dewar with Liquid Nitrogen............................................................................................9 ~§i1~:'.~~"o~~;j~ 2 IUDltiiiil Declaration of Conformity Manufacturers Name: Manufacturers Address: Linkam Scientific Instruments Ltd 8 Epsom Downs Metro Centre Waterfield Tadworth Surrey KT205LR UK Declares that the product as originally delivered: Product Name: Product Number: Liquid Nitrogen Pump LNP95 has been independently tested and found to comply w,ith the following European Directives, and carries the CE marking accordingly: EMC Directive 2004/108IEC using product standard EN 61326-1:2006 Low Voltage Directive 2006/95IEC using product stai;idard EN 61010-1:2001 and also carries the additional certification: EMC Safety FCC CFR47 Part 15 CB IEC 61010-11 EN 61010-1 MET UL 61010-11 CSA C22.2 No.61010-1 under listing EI12928 28th August 2009 Date 3 Peter Grocutt R&D Manager applicable
  • 3. Important Notice Please check that your Linkam equipment has not been damaged during transport. Ifthere is any evidence ofexternal damage to electrical items: DO NOT CONNECT THE POWER CORD OR SWITCH THE ITEM ON Contact Linkam Scientific or their appointed distributor immediately. Your warranty may be impaired if Linkam is not informed ofany transport damage within 7 working days ofdelivery. Safety Precautions I) 2) 3) 4) 5) 6) 7) 8) Read all ofthis guide before using the equipment. Save these instructions for later use. Follow all warnings and instructions, marked on any of your Linkam equipment, or contained within the manuals. If for any reason the mains fuse needs to be replaced then it must be replaced by one of the same type and rating as shown in the equipment ratings. To prevent electric shock, do not remove the cover ofthe equipment. Never use the equipment if the power cord has been damaged. Do not allow any heavy objects to rest on the power cord. Never lay the power cord on the floor. Do not obstruct any ventilation holes. Do not attempt to insert anything into these openings. Provide adequate ventilation ofat least 75mm all around the equipment. Do not expose the equipment to water. If for any reason it gets wet then remove the power cord from the mains outlet and contact Linkam Scientific Technical Support. The equipment is not intended to be used outdoors. Each product is equipped with a 3-wire grounded (earth) power plug or a free-end 3 wire power cord. The plug only fits into a grounded-type outlet. The free-end power cord should be con- nected to a correctly grounded 3-wire power outlet. Do not defeat the purpose of the grolli,ld~ (earth) type plug. Free - end power cords are colour coded as follows: Colour Brown Blue GreenlYellow Function Live Neutral Earth (Ground) 9) The power cord must be an appropriately rated and approved cord-set for the country it is being used in. 10) If any problems occur then remove the power cord from the mains outlet and contact Linkam Scientific Technical Support. 11) No attempt should be made to repair or ~odify the equipment in any way, as there are no user replaceable parts. Any servicing should be carried out by qualified service personnel. Do not remove the cover from the equipment unless the power cord has been removed from the mains outlet. 4 Symbol Reference This safety symbol is seen on the back panel ofthe equipment and warns the user: Not to make or remove any connections while the unit is powered on. Not to remove the cover. Servicing should only be done by qualified service personnel. It can also be seen on the Dewar for liquid nitrogen and warns the user: Of the potential dangers in handling liquid nitrogen, especially the exposure to skin and of asphyxiation in an enclosed space. Please refer to your safety supervisor for special handling instructions. This safety symbol is seen on the back panel ofthe equipment and warns the user: That to avoid electric shock the power cord protective grounding conductor must be con- nected to ground. .' 5
  • 4. Equipment Ratings A.c. Mains Supply: A.C. Frequency: Maxcurrent: Fuse: 100-240- 47-63Hz 1.7A Current rating Characteristic Voltage rating Breaking capacity TechniCal Specification Dimensions: Weight: 376Lx 243W x 87H (mm) 3.6Kg (excluding cables) 2A T 250V- H Operating environment: 5- 40°C, 80% relative humidity at 31°C decreasing linearly to 50% at 40°C (without condensation) Tubing: Silicon rubber Warranty This equipment has a warranty against defects in material and workmanship for a period of 12 months. Linkam will either repair or replace products that prove to be defective. For warranty service or repair, this product must be returned to Linkam or a designated service facility. The warranty shall not apply to defects resulting from interfacing, unauthorized modification or misuse, operation o~tside of the environmental specifications for the product, or improper site preparation or main- tenance. Technical Support Any technical questions or queries should be addressed.to the Technical Support Department at the ad- dress shown on the back ofthis manual. Equipment Maintenance The LNP95 does not require any regular maintenance. Contact Linkam should you require any mainte- nance. Before cleaning the case or front panel of the LNP95, remove the mains cord from the mains outlet. Use a small quantity of isopropyl alcohol on a soft cloth and gently wipe the surface. . Product Registration Register your Linkam instrument and software; please go to www.linkam.co.uk to fill in the Product software Registration form. After registration, you can login to our website to download manuals and access 'How To Videos'. . Feedback Your feedback will be greatly appreciated, please go to www.linkam.co.uk to fill in the Feedback form. 6 i 1 Introduction Thank you for purchasing a Linkam instrument. Please take the time to read through the manual as it will help you to make the most out of the equipment. L.NP95 Liquid Nitrogen Pump Cooling System P.I,e)iSe check;that all of the following parts have been supplied with the LNP95 System. 1.. LNP95 2. 2L Dewar with siphon assembly (7L and 25L is available) 3. Instrument bus cable 4~ fPo~t:r cord Remove Transit Screws ~Before using the LNP95 Liquid Nitrogen Pump System, remove the 4 transit screws marked by small yellow labels (5), from the base of the LNP95. Transit screws shown by arrows in the adjacent image. These screws hold the pumps in plaCe for shipping. Keep the screws safe by screwing them into the holes on the back panel as shown by the arrows. The screws must be replaced back into the transit hples on the ~ase, when shipping back to Linkam for service or repair. 7
  • 5. Front Panel Tubing Connections Refer to your hotstage manual for the connection oftubing. 1. Window purge tube 2. Stage purge tube and connector Back Panel Cable Connections 3. Main power socket 4. .Fuse box housing 5. Instrument bus (CAN) Sockets 6. USB socket. Do not use 7. Transit screws storage Connect the Instrument Bus Cable (9) between the LNP95 and T95 as shown. Note: either of the purple coloured Instrument Bus Sockets (5) on the LNP95 can be used. Plug the power cord into the power socket and push power switch (8).on the front of the LNP95 to tum it on or off. LNP95 MUST BE SWITCHED ON BE~ FORE T95SY~TEM CONTROLLER. 8 Filling the Dewar with liquid nitrogen Please follow your health and safety manual for directions on how to handle liquid nitrogen and ensure that you have the correct safety equipment including gloves and safety goggles. Fill'i.tlte;Dewar approximately 2/3 full and replace tj;I~,lid~th siphon attached. ~ ft;;6;';:,'~·;~ : '; ,:,' ~ DO NOT FASTEN THE CATCHES Wait for the nitrogen to stop bubbling before fastening the catches. Take care when placing lid on a table to always have the black capillary pointing upwards. It is ~asily damaged which will impair N2f1ow, Operation The LNP95 is controlled by the T95 temperature System Controller that it is connected with. The T95 temperature programmer is either controlled by LinkPadtouch screen display, or by the Link- sys32 computer software, details of how to con- -trol the LNP95 can be found in the manuals for these products. LinkPad touch screen display Linksys32 computersoftware 9
  • 6. Appendix Spares and Accessories 0994 DF Standard 2L Dewar 9588 DF2 Standard 2L Dewar (inc!. Lid and Siphon Assembly) Specify Stage Model 9590 SSDF2 2L Stainless Steel Dewar (Inc!. Lid and Siphon Assembly) Specify Stage Model 9592 D2L Dewar Siphon Assembly 39cm (no Dewar lid and need to specify Stage Model) - achieves a stage temperature of-196°C on THMS600IFTIR6001LTS350 9524 02L Dewar Siphon Assembly 80cm (no Dewar lid and need to specify Stage Model)- achieves a stage temperature of-120°C on THMS600tFTIR600 9808 02L Dewar Siphon Assembly 100cm (no Dewar lid and need to specify Stage Model)- achieves a stage temperature of-50°C on THMS600IFTIR600 9598 DS2 Extra Long Dewar Siphon Assembly for 25L Taylor Wharton "Classic" Dewar · 5647 TWC25 25L Dewar Flask - Taylor Wharton Classic (without siphon) This page is intentionally blank 9599 LNPTU Silicon Tubing & Connectors between LNP & Stage 7018 SILTUl Silicon Purge Tube LNP to Stage (2mm ID x 4mm OD) 19075 CANC Instrument Bus (CAN) Cable to connect LNP95 and T95 9850 DF7 Standard 7L Dewar (inc!. Lid and Siphon Assembly) Specify Stage Model 9851 DF7 7L Dewar (inc!. Lid but no Siphon Assembly) 9852 D7L Siphon Assembly for 7L Dewar need to specify Stage Model 10 11