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Laboratory work – November 19 - 2008
Course for Cement Applications
 Holcim Cone TM tool concept
 Cement / Superplasticizer compatibility
 Self-Compacting concrete
Moussa Baalbaki / Michael Romer / Anatol Zingg
HGRS/PID
2
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Tasks & groups - Wednesday, November 19, 2008
Topic – AM session Water demand with Holcim Cone TM
Responsible M. Baalbaki M. Romer / A. Zingg
11:30 – 12:50 Group 1 (EN Room) Group 2 (Rheology Room)
12:50 – 13:50 Lunch
Topics – PM session
Cement/admixture
compatibility
Self-compacting concrete
Responsible M. Romer / A. Zingg M. Baalbaki
14:00 – 15:20 Group 1 (EN Room) Group 2 (Concrete Room)
15:20 – 16:00 Coffee break - Betonlabor
16:00 – 17:20 Group 2 (EN Room) Group 1 (Concrete Room)
3
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Objectives of the laboratory work
 Cement/superplasticer compatibility
 Introduce the new Holcim cone TM application based test
method to assess
- The water demand for a given cement according to its intrinsic
characteristics
- the cement/admixture compatibility
 Self-compacting concrete
 Produce self-compacting concrete according to the powder
and to the admixture (viscosity enhancer admixture)
approaches
 Present different test methods to assess the self-
compactability properties (self-flowing, resistance to
blocking and deformability)
Holcim Cone TM
Cement / superplasticer compatibility
5
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Holcim cone tool concept
A two-step test
 Step 1 – intrinsic characteristic of the cement in terms of
water demand and strength are determined
 Results depend only on the physical and chemical
characteristics of the cement
 Done without water reducers or superplasicizers
 Can be used in normal cement production
 Step 2 – from cement quality to concrete performance
requirements
 Determination of water reduction to meet requirements for
workability and design strength
 Assessment of best economical & available admixtures
that meet concrete performance
6
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
How concrete is specified
EN 206-1
C25/30
Classes of
compressive
strength
XC4
XF1
Classes of
exposure
Dmax = 32
Maximum
size of
Aggregates
Cl 0,20
Classes of
chloride
content
C3
Classes of
workability
7
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Application example – Civil Engineering
Reinforced
foundation
non-reinf. concrete carriage way Bkl. SV. I - III
hutch base
underwater concrete
Cap
non-reinf. concrete carriage way
Superstructure
Cap
parapet wall
Bore
pile
Hydraulically bounded gravel base
parapet wall
XF4
XF4
XO
XC
XD
XF
XA
8
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Classes of Workability
 According to the methods used in Switzerland to
measure workability
Class value [mm] Class value [mm] Class value [mm]
F1** ≤ 340 C0** ≥ 1,46 S1 10 - 40
F2 350 - 410 C1 1,45 - 1,26 S2 50 - 90
F3 420 - 480 C2 1,25 - 1,11 S3 100 - 150
F4 490 - 550 C3 1,10 - 1,04 S4 160 - 210
F5 560 - 620 S5** ≥ 220
F6** ≥ 630
Slump flow Walz Index Slump
** classes not recommended for this method due to the lack of accuracy in the measurement
9
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
HC TM vs EN 206 class of consistency
S class
Slump
F class
DIN
flow
HC TM
flow
Mortar of concrete < 5 mm
No compaction
With compaction
No compaction
10
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
S3
F3
S4
F4
S5
F5
S2
F2
ASTM slump VS DIN flow – EN 206 class of consistency
 Good correlation between ASTM and DIN concrete slump
y = 0.8725x + 341.45
R2
= 0.9058
360
400
440
480
520
560
600
0 20 40 60 80 100 120 140 160 180 200 220 240 260
ASTM slump (mm) - S
DIN
slump
flow
(mm)
-
F
11
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Class F consistency vs Holcim cone - Normo 4
y = 0.8676x - 241.71
R2
= 0.9582
100
125
150
175
200
225
250
275
400 420 440 460 480 500 520 540 560 580 600
Concrete flow - DIN (mm)
Holcim
flow
(mm)
F2 F3 F4 F5
12
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Concrete mix design – Precast element (Example)
kg/m3 Density Volume (L/m3) Mortar volume
Sand/mortar ratio
(%)
w/c 0.35 -- --
1000-407 =
593
326/593 = 55%
Cement 400 3.14 127
Water 140 1 140
Sand [< 5
mm]
865 2.65 326
Coarse
aggregates
[>5 m]
1100 2.7 407
Total 1000L
Total 2505 kg/m3
13
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Step 1 - Water demand - from 11:30 until 13:00
Mix 1 2 3
W/C 0.50 0.55 0.60
Cement
type
Group 1 Normo 4 – CEM I 42.5
Group 2 White cement Albaro – CEM I 52.5
14
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Water demand – 10 & 45 min
0.55
0.56
0.57
0.58
0.59
0.6
0.61
0.62
0.63
0.64
0.65
10 min 45 min
W/C
Water
demand
(w/c)
CEM I 42.5
CEM I 52.5
15
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Step 2 – Cement/admixture performance - PM session
Group 1 2
Cement type White cement Albaro – CEM I 52.
W/C 0.35
Superplastcizer
type
Sika 210 Glenium 51
Dosage (%) 1.2 1.5 2 0.4 0.45 0.5
16
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Admixture compatibility with White cement – CEM I 52.5
W/C = 0.35 - Target flow: 200 mm
0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
10 min 45 min
Superplasticizer
dosage
(%)
Sika 210
Glenium 51
Self-compacting concrete
18
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Self-compacting concrete mix design – PM session
Mix design approach Robust Admixture
W/C 0.43 0.50
W/B 0.29 0.50
Water [kg/m3] 175 195
Cement – Normo 4 Siggenthal [kg/m3] 400 390
Fly ash – Hydrolent [kg/m3] 200 --
Superplasticizer – sika 210 [kg/m3] 8 13
VEA – welan gum [g/m3] -- 100
Sand [kg/m3]
0.2 – 0.5 mm 256 311
0.5 – 1 mm 304 370
1 – 2 mm 48 58
2 – 4 mm 192 235
Aggregate [kg/m3]
4 – 8 mm 295 320
8 – 16 mm 545 600
19
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Mixing procedure
Admixture Robust
Step 1
Mix 1 min.
Coarse aggr.
+ sand
+ water
Coarse aggr.
+ sand
+ water
Step 2
Mix 3 min.
Add Cement Add Cement + fly ash
Break 1 min.
Step 3
Mix 5 min.
Add Sikament 210 (SP) Add Sikament 210 (SP)
Testing Measure Flow, U-box, V-funnel Measure Flow, U-box, V-funnel
Step 4
Mix 2 min.
Add Velan Gum (VEA)
Testing Measure Flow, U-box, V-funnel
20
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Testing on fresh concrete
 Slump flow
 V-funnel
 U-box
21
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Fresh concrete properties – Group 1
Mix design approach Robust Admixture Target
W/C 0.43 0.50
W/B 0.29 0.50
(+ 60 g Sika
210)
Without VEA With VEA
Slump flow (cm) 60 -- 67 60 -70 cm
V – funnel (sec) 14 -- 4.1 6 – 15 sec
U-box (cm)
>30 cm
(Rank 1)
--
>30 cm
(Rank 3)
> 30 cm
22
(optional) 04.09.2022/SN/SN
(optional) Filename.ppt
Holcim Group Support CCA 2008
Fresh concrete properties – Group 2
Mix design approach Robust Admixture Target
W/C 0.43 0.50
W/B 0.29 0.50
(+ 78 g Sika
210)
Without VEA
With VEA +
2g
Slump flow (cm) 65 -- 66 60 -70 cm
V – funnel (sec) 10 -- 5 6 – 15 sec
U-box (cm)
>30 cm
(Rank 1)
--
>30 cm
(Rank 3)
> 30 cm

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081200baalbakiresults.ppt

  • 1. Laboratory work – November 19 - 2008 Course for Cement Applications  Holcim Cone TM tool concept  Cement / Superplasticizer compatibility  Self-Compacting concrete Moussa Baalbaki / Michael Romer / Anatol Zingg HGRS/PID
  • 2. 2 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Tasks & groups - Wednesday, November 19, 2008 Topic – AM session Water demand with Holcim Cone TM Responsible M. Baalbaki M. Romer / A. Zingg 11:30 – 12:50 Group 1 (EN Room) Group 2 (Rheology Room) 12:50 – 13:50 Lunch Topics – PM session Cement/admixture compatibility Self-compacting concrete Responsible M. Romer / A. Zingg M. Baalbaki 14:00 – 15:20 Group 1 (EN Room) Group 2 (Concrete Room) 15:20 – 16:00 Coffee break - Betonlabor 16:00 – 17:20 Group 2 (EN Room) Group 1 (Concrete Room)
  • 3. 3 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Objectives of the laboratory work  Cement/superplasticer compatibility  Introduce the new Holcim cone TM application based test method to assess - The water demand for a given cement according to its intrinsic characteristics - the cement/admixture compatibility  Self-compacting concrete  Produce self-compacting concrete according to the powder and to the admixture (viscosity enhancer admixture) approaches  Present different test methods to assess the self- compactability properties (self-flowing, resistance to blocking and deformability)
  • 4. Holcim Cone TM Cement / superplasticer compatibility
  • 5. 5 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Holcim cone tool concept A two-step test  Step 1 – intrinsic characteristic of the cement in terms of water demand and strength are determined  Results depend only on the physical and chemical characteristics of the cement  Done without water reducers or superplasicizers  Can be used in normal cement production  Step 2 – from cement quality to concrete performance requirements  Determination of water reduction to meet requirements for workability and design strength  Assessment of best economical & available admixtures that meet concrete performance
  • 6. 6 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 How concrete is specified EN 206-1 C25/30 Classes of compressive strength XC4 XF1 Classes of exposure Dmax = 32 Maximum size of Aggregates Cl 0,20 Classes of chloride content C3 Classes of workability
  • 7. 7 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Application example – Civil Engineering Reinforced foundation non-reinf. concrete carriage way Bkl. SV. I - III hutch base underwater concrete Cap non-reinf. concrete carriage way Superstructure Cap parapet wall Bore pile Hydraulically bounded gravel base parapet wall XF4 XF4 XO XC XD XF XA
  • 8. 8 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Classes of Workability  According to the methods used in Switzerland to measure workability Class value [mm] Class value [mm] Class value [mm] F1** ≤ 340 C0** ≥ 1,46 S1 10 - 40 F2 350 - 410 C1 1,45 - 1,26 S2 50 - 90 F3 420 - 480 C2 1,25 - 1,11 S3 100 - 150 F4 490 - 550 C3 1,10 - 1,04 S4 160 - 210 F5 560 - 620 S5** ≥ 220 F6** ≥ 630 Slump flow Walz Index Slump ** classes not recommended for this method due to the lack of accuracy in the measurement
  • 9. 9 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 HC TM vs EN 206 class of consistency S class Slump F class DIN flow HC TM flow Mortar of concrete < 5 mm No compaction With compaction No compaction
  • 10. 10 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 S3 F3 S4 F4 S5 F5 S2 F2 ASTM slump VS DIN flow – EN 206 class of consistency  Good correlation between ASTM and DIN concrete slump y = 0.8725x + 341.45 R2 = 0.9058 360 400 440 480 520 560 600 0 20 40 60 80 100 120 140 160 180 200 220 240 260 ASTM slump (mm) - S DIN slump flow (mm) - F
  • 11. 11 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Class F consistency vs Holcim cone - Normo 4 y = 0.8676x - 241.71 R2 = 0.9582 100 125 150 175 200 225 250 275 400 420 440 460 480 500 520 540 560 580 600 Concrete flow - DIN (mm) Holcim flow (mm) F2 F3 F4 F5
  • 12. 12 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Concrete mix design – Precast element (Example) kg/m3 Density Volume (L/m3) Mortar volume Sand/mortar ratio (%) w/c 0.35 -- -- 1000-407 = 593 326/593 = 55% Cement 400 3.14 127 Water 140 1 140 Sand [< 5 mm] 865 2.65 326 Coarse aggregates [>5 m] 1100 2.7 407 Total 1000L Total 2505 kg/m3
  • 13. 13 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Step 1 - Water demand - from 11:30 until 13:00 Mix 1 2 3 W/C 0.50 0.55 0.60 Cement type Group 1 Normo 4 – CEM I 42.5 Group 2 White cement Albaro – CEM I 52.5
  • 14. 14 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Water demand – 10 & 45 min 0.55 0.56 0.57 0.58 0.59 0.6 0.61 0.62 0.63 0.64 0.65 10 min 45 min W/C Water demand (w/c) CEM I 42.5 CEM I 52.5
  • 15. 15 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Step 2 – Cement/admixture performance - PM session Group 1 2 Cement type White cement Albaro – CEM I 52. W/C 0.35 Superplastcizer type Sika 210 Glenium 51 Dosage (%) 1.2 1.5 2 0.4 0.45 0.5
  • 16. 16 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Admixture compatibility with White cement – CEM I 52.5 W/C = 0.35 - Target flow: 200 mm 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 10 min 45 min Superplasticizer dosage (%) Sika 210 Glenium 51
  • 18. 18 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Self-compacting concrete mix design – PM session Mix design approach Robust Admixture W/C 0.43 0.50 W/B 0.29 0.50 Water [kg/m3] 175 195 Cement – Normo 4 Siggenthal [kg/m3] 400 390 Fly ash – Hydrolent [kg/m3] 200 -- Superplasticizer – sika 210 [kg/m3] 8 13 VEA – welan gum [g/m3] -- 100 Sand [kg/m3] 0.2 – 0.5 mm 256 311 0.5 – 1 mm 304 370 1 – 2 mm 48 58 2 – 4 mm 192 235 Aggregate [kg/m3] 4 – 8 mm 295 320 8 – 16 mm 545 600
  • 19. 19 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Mixing procedure Admixture Robust Step 1 Mix 1 min. Coarse aggr. + sand + water Coarse aggr. + sand + water Step 2 Mix 3 min. Add Cement Add Cement + fly ash Break 1 min. Step 3 Mix 5 min. Add Sikament 210 (SP) Add Sikament 210 (SP) Testing Measure Flow, U-box, V-funnel Measure Flow, U-box, V-funnel Step 4 Mix 2 min. Add Velan Gum (VEA) Testing Measure Flow, U-box, V-funnel
  • 20. 20 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Testing on fresh concrete  Slump flow  V-funnel  U-box
  • 21. 21 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Fresh concrete properties – Group 1 Mix design approach Robust Admixture Target W/C 0.43 0.50 W/B 0.29 0.50 (+ 60 g Sika 210) Without VEA With VEA Slump flow (cm) 60 -- 67 60 -70 cm V – funnel (sec) 14 -- 4.1 6 – 15 sec U-box (cm) >30 cm (Rank 1) -- >30 cm (Rank 3) > 30 cm
  • 22. 22 (optional) 04.09.2022/SN/SN (optional) Filename.ppt Holcim Group Support CCA 2008 Fresh concrete properties – Group 2 Mix design approach Robust Admixture Target W/C 0.43 0.50 W/B 0.29 0.50 (+ 78 g Sika 210) Without VEA With VEA + 2g Slump flow (cm) 65 -- 66 60 -70 cm V – funnel (sec) 10 -- 5 6 – 15 sec U-box (cm) >30 cm (Rank 1) -- >30 cm (Rank 3) > 30 cm