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Research, Design and Manufacturing of a
small scale Roll to Roll Nanoimprint
Lithography (R2RNIL) Machine
Apostolos Veltsin, University of
Glasgow, February 2016
1APOSTOLOS VELTSIN - 1106086University of Glasgow, 2016
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 2
Nanoimprint lithography (NIL)
• Method for fabricating micro-, nano- patterns
• First devised by Prof. Stephen Chou, 1996
Roll to roll (R2R)
• Most demanding type of NIL
• High industrial scale application
• Rolls of flexible material used
• Combination on rollers
• Thermal embossing or UV curing
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 3
Aim
• Small scale R2R printer
• Provides nano- patterned PS films
• Using UV curing
• 27 mm width
• Bottom surface of test tube array plates
• Interchangeable molds
• Maximum of 170 μm thickness
• Full customisation needed
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 4
Approach
Research, development and
manufacturing
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 5
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 6
Used printers
• Similar idea with a R2R printer
• Retrieve components
• Provided by IT service
• Recycle the rest of the components
Structural components
• MakerBeam shafts used
• Allow full customisation
• Custom brackets produced on laser cutter
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 7
Unwinding unit
• Removable reel design
• 42 mm width
Guide
• Width of 42 mm
• Roller prevents scratches on the foil
Feeder
• Retrieved from a printer
• Two shafts with rollers, sufficient grip
• Mounted on a motor
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 8
Corona treatment unit
• BD-20AC by Nbond
• Removable design
• Raises the surface energy of the substrate
• Improves bonding capabilities
• Electrode provides 10,000-50,000 Volts
• Causes EM interference
• Pretreating substrate fixes problem
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 9
Coating unit
• Method chosen: slot die
• Custom made on our CNC
• Side 1: flat with 4 holes
• Side 2: 4 holes, groove cut, feed hole
• Gaskets control thickness and width
• Ideal width 30 mm
• Photocurable coating purchased
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 10
Imprint unit
• 2 guide rollers
• 1 custom imprint shaft
• Acrylic base controls demolding angle
• PDMS mold attached with zip ties
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 11
PDMS (Polydimethylsiloxane) mold
• Polymeric organosilicon
• Unusual rheological properties
• Flexible, good for R2R
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 12
UV unit
• Use of 1 ultraviolet LZ4 emitter
• Wavelength of 365 nm
• Viewing angle 110°
• EYE PROTECTION NEEDED
• On an aluminium heatsink
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 13
End feeder
• 2 shafts forced together with springs
• O-rings improve grip
• Servo runs the bottom shaft
• Bearings allow smooth movement
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 15
Electronics - PCB fabrication
• After breadboard and Veroboard
• Fabricated in Rankine building
• Shield design
• Includes power supply that provides 12V and 5V
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 16
Electronics box
• To fit everything together
• Safe enclosed design
• Allowing access to controls
• Firstly designed in CAD
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 17
Front side
1. Feeder control
2. End feeder control
3. Reverse mode
4. UV led switch
Back side
5. Power supply connector
Right side
6. Servo motors switch
Left side
7. USB for microcontroller
8. UV intensity control
Experiments
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 18
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 21
Surface tension
• Attension Optical Tensiometer
• Testing behavior of corona treatment
• 31 experiments took place
• Contact angles found
• Result 1: Untreated sample, 87.5°
• Result 2: Best case scenario with
corona not making interference, 58°
• Result 3: Pretreated sample at
maximum power, 9°
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 22
Microscope results for micro- patterns
Mold Sample
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 23
Results after 400 samples for nano- patterns
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 24
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 25
TX spectral analysis
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 26
Conclusion
• Successful project
• 40 runs
• 460 samples
• Speed of 3 samples/min
• 160 μm thickness
• Can be further optimised
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 27
Further work
• Faraday cage for EM interference
• Pump for photocurable coating
• Two UV LEDs
• Improved lacquer with less UV
absorbers
University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 28
Any questions?

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1106086v_Veltsin_ENG5041P_Presentation_15-16

  • 1. Research, Design and Manufacturing of a small scale Roll to Roll Nanoimprint Lithography (R2RNIL) Machine Apostolos Veltsin, University of Glasgow, February 2016 1APOSTOLOS VELTSIN - 1106086University of Glasgow, 2016
  • 2. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 2 Nanoimprint lithography (NIL) • Method for fabricating micro-, nano- patterns • First devised by Prof. Stephen Chou, 1996 Roll to roll (R2R) • Most demanding type of NIL • High industrial scale application • Rolls of flexible material used • Combination on rollers • Thermal embossing or UV curing
  • 3. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 3 Aim • Small scale R2R printer • Provides nano- patterned PS films • Using UV curing • 27 mm width • Bottom surface of test tube array plates • Interchangeable molds • Maximum of 170 μm thickness • Full customisation needed
  • 4. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 4 Approach
  • 5. Research, development and manufacturing University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 5
  • 6. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 6 Used printers • Similar idea with a R2R printer • Retrieve components • Provided by IT service • Recycle the rest of the components Structural components • MakerBeam shafts used • Allow full customisation • Custom brackets produced on laser cutter
  • 7. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 7 Unwinding unit • Removable reel design • 42 mm width Guide • Width of 42 mm • Roller prevents scratches on the foil Feeder • Retrieved from a printer • Two shafts with rollers, sufficient grip • Mounted on a motor
  • 8. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 8 Corona treatment unit • BD-20AC by Nbond • Removable design • Raises the surface energy of the substrate • Improves bonding capabilities • Electrode provides 10,000-50,000 Volts • Causes EM interference • Pretreating substrate fixes problem
  • 9. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 9 Coating unit • Method chosen: slot die • Custom made on our CNC • Side 1: flat with 4 holes • Side 2: 4 holes, groove cut, feed hole • Gaskets control thickness and width • Ideal width 30 mm • Photocurable coating purchased
  • 10. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 10 Imprint unit • 2 guide rollers • 1 custom imprint shaft • Acrylic base controls demolding angle • PDMS mold attached with zip ties
  • 11. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 11 PDMS (Polydimethylsiloxane) mold • Polymeric organosilicon • Unusual rheological properties • Flexible, good for R2R
  • 12. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 12 UV unit • Use of 1 ultraviolet LZ4 emitter • Wavelength of 365 nm • Viewing angle 110° • EYE PROTECTION NEEDED • On an aluminium heatsink
  • 13. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 13 End feeder • 2 shafts forced together with springs • O-rings improve grip • Servo runs the bottom shaft • Bearings allow smooth movement
  • 14. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 15 Electronics - PCB fabrication • After breadboard and Veroboard • Fabricated in Rankine building • Shield design • Includes power supply that provides 12V and 5V
  • 15. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 16 Electronics box • To fit everything together • Safe enclosed design • Allowing access to controls • Firstly designed in CAD
  • 16. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 17 Front side 1. Feeder control 2. End feeder control 3. Reverse mode 4. UV led switch Back side 5. Power supply connector Right side 6. Servo motors switch Left side 7. USB for microcontroller 8. UV intensity control
  • 17. Experiments University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 18
  • 18. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 21 Surface tension • Attension Optical Tensiometer • Testing behavior of corona treatment • 31 experiments took place • Contact angles found • Result 1: Untreated sample, 87.5° • Result 2: Best case scenario with corona not making interference, 58° • Result 3: Pretreated sample at maximum power, 9°
  • 19. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 22 Microscope results for micro- patterns Mold Sample
  • 20. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 23 Results after 400 samples for nano- patterns
  • 21. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 24
  • 22. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 25 TX spectral analysis
  • 23. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 26 Conclusion • Successful project • 40 runs • 460 samples • Speed of 3 samples/min • 160 μm thickness • Can be further optimised
  • 24. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 27 Further work • Faraday cage for EM interference • Pump for photocurable coating • Two UV LEDs • Improved lacquer with less UV absorbers
  • 25. University of Glasgow, 2016 APOSTOLOS VELTSIN - 1106086 28 Any questions?

Editor's Notes

  1. Prof. sub-100nm patterns by deforming thermoplastic, controlled pressure and temp Rolls of flexible foil or plastic passed through a combination of rollers and get patterned with one of the two methods
  2. Allows full customisation, something not available on similar design out there
  3. Unscrew pieces and give it to them