2. Sample Collection
Maize Grain Sample Collection
โข Mature maize was collected at commercial maturity from a
commercial farm in the Amhara region, West Gojam zone in Adet
Wereda in Ethiopia
โข The sample size of the collected maize amount was 90 kg, and the
sample taken for each run was 5kg
3. Material Collection for Roaster
Collection of Equipment Construction Material
and Construction of Roasting Drum-like Machine
โข The construction materials used for making the roaster were
collected from the local market
โข The equipment and machines used were found in Bahir dar university
institute of Technology and these types of equipment were roller
machines which were used to roll the metal sheet into a cylindrical
form, a grinder that was used to cut different parts as designed
dimensions, a welding machine, cutting machine
4. Collection of Construction Materials
โข The collected material is categorized as food grade material, thermal
resistance material, good thermal insulating material, and strong and
capable the load and movement
โข The materials used for construction collected from the local market
were: stainless sheet metal, metal rods, framing square tube metals
used for the construction of base frame structure, bolts, electrodes
used for welding different parts together, grinding disks used to cut
different metal parts as the desired object, fiberglass used to
insulating the whole roaster cover additional teff straw were used the
burning chamber, painting grise used as anti-rust, two bearing used
for free movement of the cylinder and connect to the burning
chamber frame
5. Collection of Construction Materials
โข The materials used to construct the roaster were collected from the local
market, and these materials were categorized as food grade and resistant
to different conditions like high temperature, moisture, and strength for
heavy loads
Roasting Cylinder and Chamber Design
โข Inner Roasting Drum-like cylinder roaster design Factors taken
into consideration for the design of the roasting cylinder were
according to the edibility of the end product, volumetric capacity,
thermal properties of the drum materials, and also durability
โข Design requirement /assumption
6. Roasting Cylinder and Chamber Design
โข Drum Dimension calculation
โข Roaster Design Consideration and Sizing
Roaster Design Consideration and Sizing
โข Dimension
7. Cylindrical holder
โข The material used in the fabrication of the roasting machine was
stainless steel
โข The following constructional operations were carried out on the
components before the machine was finally built: The marking and
cutting of components, drilling of components, machining of shafts,
welding of components, filling and smoothing, assembly of
components, and painting were done according to the procedures set
โข The workshop tools and machines used included a scriber, a steel
ruler, a compass, a center punch, a treadle-operated guillotine for
cutting, and a welding machine for joining
8. Frame design
โข The frame of this roaster is the skeleton of the whole machine since it
holds, carries, and connects all the cylinders, shells, and burning
chambers
โข The frame has the following dimensions: 66, 66, and 100 cm in width,
height, and length, respectively
โข 4 the frame dimension and structure system of the roaster
9. Heating /burning chamber design
โข The internal body of the cylinder consists of length, radius, and width
with dimensions x1, x2, x3, and the two ends of the cylinder
โข The heat generated from burning wood is transferred through
conducting corrugated metal sheet by conduction and hot air
convection means of the heat transfer and the conducted heat is
transferred to the roasting cylinder in both conventional and
conduction heat transfer means
โข The burning chamber is designed to hold the wooden material and
distribute heat to the upper layer, or external surface, of the cylinder
under the jacketed, insulated shell
10. Components of the Machine Burning
Chamber
โข The air heater
โข The Air Inlet
โข The firing Chamberโs
Components of the Machine Burning Chamber
Air Vents/chimney /smoke exhaust
11. Design and Fabrication of the upper shell
cover of the Roaster
โข The upper cover of the roaster has dimensions of 33, and 100 cm in
radius and length, respectively, and this cover can be easily opened
and disassembled
โข The shell cover was bent with a roller machine and welded by a
welding machine using electrodes
โข The cover is designed according to the cylindrical roaster size, and the
size of this shell shown in Figure 3.4 has a 5 cm clearance from the
normal grain holding cylinder
12. Equipment Sizing and Capacity
โข The amount of heat transferred to the roast grain/maize will be
calculated according to the formula bellow where Qu = energy
absorbed by grain/ maize, m = mass of maize kernels, c = specific heat
capacity of the maize, โT = change in temperature of maize, and t =
roasting time The capacity of roasting capacity test aims to find out
how many machines the actual capacity and level of fitness roaster
are listed in the user manual
โข The roasting capacity can be formulated as in the Equation below:
Determination of power required to roast maize grain
โข The thermal conductivity of a material, in general, varies with
temperature
13. Maize Grain Preparation
โข The collected sample was dried by the sun until the moisture content
reached 13% or below
โข Only healthy kernels that are uniform in size have been used for
roasting
โข In this section, some details about the method, methodology,
equipment design, and other related activities discussed according to
the corresponding assigned procedures are written below
14. Maize Grain Preparation and Roasting
Roasting Experiment
Two methods of roasting and three levels of roasting time were selected
Each experiment was conducted with the same input or feed materials, and there
were trial experiments to adjust the roasting time that was used for systematic
random design
Conveyance Efficiency CE is also used to calculate the relationship, similar to the
formula used by Atere et al., to calculate the conveyance efficiency of water
removal for continuous roasting practice, but the roasting techniques may not be
used for "asharo kolo" since the process needs an intense roasting method for a
long time with a higher temperature
15. Roasting Experiment
โข Two methods of roasting and three levels of roasting time were
selected
โข Each experiment was conducted with the same input or feed
materials, and there were trial experiments to adjust the roasting
time that was used for systematic random design
โข Conveyance Efficiency CE is also used to calculate the relationship,
similar to the formula used by Atere et al., to calculate the
conveyance efficiency of water removal for continuous roasting
practice, but the roasting techniques may not be used for "asharo
kolo" since the process needs an intense roasting method for a long
time with a higher temperature
16. Roasting Experiment
โข The purpose of many roasting studies is to determine the optimal
temperature, rotation speed, and roasting time that produce a good
quality of roasted cereal and legumes and produces the taste and
color of peanuts favored to meet consumersโ expectations
17. 3.3.2 Sample Preparations for Roasting
โข The raw maize grain was purchased from a local market from farmers
at Adet, which is known for maize production, and the place is around
Bahir Dar city
โข The reason why the grain was purchased there was due to quality and
fresh samples because from the market merchants mixed weevil and
insect-damaged grain; hence, by eye inspection, we selected and
bought 80 kg of maize grain
โข The clean and screened maize samples were first soaked in water for
up to four days to gain the optimum amount of moisture that
facilitates germination and weakens the kernel hardness and then
used as a medium to transfer heat throughout the kernels
18. Roasting
โข About 6-10kg of Clean, soaked, and germinated maize was prepared
for each treatment and roasted according to the experimental design
setup
โข The maize was roasted for 30 min,40min, and 50min, in both newly
designed jacketed manual rotate-able cylindrical drum-like roasters
and open pan/ roasters with equivalent power supply and roaster
thickness
โข The power consumption is considered equivalent to one another
since the input mass is equal for each treatment
19. Sample Preparation for Analysis
Experimental Analysis and Activities cite
โข The construction of the equipment will be done in Bahir Dar City or
Bahir Dar University Different quality attributes of rotary roasted corn
will be analyzed at Bahir Dar University Institute of Technology
โข The roasted samples of grain under different experimental conditions
will collect and the following quality parameters will analyze in the
labs of BIT and others according to standard procedures
โข The experiments will be replicated to reduce the experimental and
reliability of results
20. Experimental Design
โข Maize kernels/barley will be subjected to pilot scale roasting
treatment for different time and temperature combinations using a
full factorial design with optimal time at 25min at 190oC ,but some
study shows barley roasted at 225oC according to the above base and
other past literature this study estimates the wooden fire burning
ranged between 100 and 250oC, but according to preliminary check,
the temperature has been determined
โข The factorial experiment was conducted as a randomized design with
three replicates and the experimental design and method for this
study was two-way ANOVA with three levels of time as a factor and
others considered as constant with three replications
21. Experimental Design
โข A complete randomized selection of the first level of time and the rest
systematic selection of interval approaches the level of roasting time
was selected after three trials of preliminary tests according to the
color and moisture content of roasted maize grain
22. Method of Analysis
Physicochemical Analysis
โข After the roasting process was done except for the moisture content,
the protein, fiber, fat, ash, and CHO were analyzed by taking the
samples from well-packed roasted samples, whereas the moisture
was immediately done after cooling roasted maize grain
โข Each proximate composition was done according to the methods
available and listed below details
23. Moisture Content
โข The moisture content of the raw corn grain, roasted samples was
determined according to the Association of Official Analytical
Chemists 2000โ ; using the official method No. 925.10 by oven drying
method
โข The 5g well-homogenized samples were weighed in a dry moisture
dish that dried in a hot air oven at 1050 for three hours and the
drying proceeded until a constant mass was obtained
โข The moisture content of the sample was calculated from the
equation: Where, %MC = Percentage of moisture in the sample, Mi =
Weight of fresh sample and Mf = Weight of dry sample
24. Crude Protein Content
โข The crude protein content of raw maize grain and roasted maize grain
samples were determined by the Kjeldahl method ; using the official
method No. 920
โข Around 0.5g of the samples were weighed and put in a digestion flask
and then 1gm of catalyst mixture was added
โข The flask has then been placed on a digestion burner for 4 hrs
25. Crude Fat Content
โข The Crude fat of the raw corn, control roasted, and machine-roasted
samples was determined based on the Soxhlet extraction method ;
using the official method No. 920
โข 250 ml quick-fit round bottom flasks were washed and dried in an
oven at 105หC for 25 minutes and allowed to cool to room
temperature before it was weighed
โข The fat obtained was expressed as a percentage of the initial weight
of the sample using the equation: Where: M1 = weight of the
extraction flask , M2 = weight of the extraction flask plus the dried
crude fat , and M = weight of the initial sample
26. Crude Fiber
โข The crude fiber content of the corn and roasted corn was determined
by AOAC, ; using the official method No. 962
โข About 200 ml of a 1.25% sulfuric acid solution was added to each
beaker and allowed to boil on a hot plate for 30 minutes by rotating
and stirring periodically
โข The crude fiber was calculated from the equation: Where: M = the
initial weight of samples, M1 = the weight of the crucible with dried
residue , and M2 = the weight of the crucible with ash
27. Total Ash Content
โข The ash content of the samples was determined by AOAC using the
official method 923
โข Porcelain crucibles were treated in a muffle furnace for 30 minutes at
550 ยฐC
โข The crucible was cooled in desiccators for about 30 minutes at room
temperature and weighed
28. 6 Carbohydrate Content
โข The total percentage of carbohydrates was determined by using the
difference method according to Onyeike
โข This method involves adding the total values of crude protein content
, crude fat content , crude fiber content , moisture content , and ash
content of the sample and subtracting them from
โข Total carbohydrates, including fiber, calculated from the equation are
Total CHO = 100 - โฆโฆโฆ
29. Gross Energy
โข The total energy content of the roasted samples was determined
according to AOAC by multiplying the mean values of crude fat , total
carbohydrate , and crude protein by the Atwater factors 9, 4, and 4,
respectively, taking the sum of the products
โข The total energy was calculated from the equation
30. Color Analysis
โข The color values of the maize grains were expressed as โLโ , โaโ , โbโ ,
and ฮE A handhold chroma meter calibrated by a standard
whiteboard was used to measure the color
โข The whiteness index values that combine lightness and yellow-blue
into a single term calculated as described by Hsu, Chen, Weng, and
Tseng as follows: calibrated by a standard whiteboard was used to
measure the color
โข Yellowness is represented by a positive b* value and blueness by a
negative b* value
31. Total Phenolic Content
โข The total phenolic content of samples was determined according to
the adapted Folin-Ciocalteu methods
โข Other beverage product phenol also determined by Folin-Ciocalteu
methods
โข The sample of roasted flour was homogenized with 10 mL of 60%
methanol containing 0.1% HCl and placed in a water bath for 2 hours
at 850 ยฐC to eliminate vitamin C, as described by
โข Folin Ciocalteuโs phenol reagent was stored at room temperature, and
the reagent was diluted with distilled water as required
32. Functional Properties
Bulk Density
โข The bulk density of the sample was determined according to the
methods described by The raw and roasted maize samples were
transferred to a pre-weigh measuring cylinder and the new weight
was recorded
โข The volume occupied by the flour in the measuring cylinder was also
recorded
โข The bulk density was calculated from the equations
33. Water Absorption Index and Capacity
โข The water absorption index of the raw and roasted maize samples
was determined according to the methods described by
โข The sample was suspended in 30 ml of distilled water, cooked for 15
minutes in 90 ยฐC water baths, then put in a tarred 50 ml centrifuge
tube and shaken for 30 minutes
โข The sample was centrifuged for 10 minutes at 3000 rpm, and the
clear supernatant of the centrifugation was transferred into a pre-
dried and weighed glass beaker for estimation of the water solubility
index
34. Determination of Water absorption capacity
โข Water absorption capacity is an indication of the amount of water
available for gelatinization
โข It was determined according to the method used by Edema et al.
โข Exactly 2.5 g of each roasted maize flour sample was added into 30 ml
distilled water in a weighed 50 ml centrifuge tube
35. Water Solubility Index
โข The water solubility index determines the number of polysaccharides
released from the granule with the addition of excess water
โข The water solubility index was determined by taking the sample and
filling a 100ml graduated cylinder up to the 10ml mark and adding up
to 50ml was attained and inverted for 2min and mixed well for 8
minutes after that the supernatant preserved from WAI
measurement, which was evaporated at 960C temperature overnight
โข The WSI was calculated from the equation
36. Performance Test
โข Before undertaking a performance test of the developed prototype, a
preliminary test was made to check whether the roaster is
functioning properly for the intended purpose
โข The roaster had good functionality except for a few minor defects,
which were easily corrected since we were making trials after making
and assembling its components especially the power source and
rotating mechanisms and related parts
โข the conducted roasting practice determines its performance in
different aspects the overall functionality of the roaster performance
and procedure of roasting the determination of moisture content was
done by taking samples at a random time interval
37. Statistical Analyses
โข The analysis of variance and the descriptive statistics were done using
Minitab software, and statistical analyses were carried out using this
software on a two-way ANOVA general linear model was used to
perform a meaningful comparison and to determine whether
significant differences existed between the treatments
โข An ANOVA with Schiffโs test was used to determine the source of the
significant differences in roasting time and roasting method
โข This study is supposed to conduct two roasting methods with three
levels of time and three replications of the responses