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www.ogsl.com
Sampling and Analysis
www.ogsl.com
Oil & Gas Systems Limited (OGS) supplies packaged fiscal analysis and pipeline integrity measurement
equipment including, but not limited to, process analyser system integration, flare metering and
analysis, manual spot sample and automated sampling, CV, H2
S moisture and total sulphur analysis
and water quality analysis (including oil in water).
A representative sample of a hydrocarbon product is necessary to ensure proper accounting for
transactions and efficient product processing. The amount of hydrocarbon product that is transported
between producer, processor, distributor and end-user is significant.
To be able to verify the exact composition of the product is important from an economic and
product treatment standpoint. A small percentage saving made by correctly determining
composition will quickly recoup the investment made in the purchase of a system designed to
obtain an optimum sample. In addition, if the best sampling procedures are followed, the potential for
disputes between supplier and customer will be greatly reduced.
Some of the standards that must be adhered to ensure representative samples include ISO 10715
and API 14.1. These standards are the most common and current ones referenced on gas sampling
procedures. This figure is a critical component of the flow formula from which we derive the product
quantity. An error in sampling affects both quality and quantity, and ultimately profitability.
Sampling Systems
A crucial factor in petroleum measurement is quality
analysis. For this reason liquid metering systems usually
have an associated sampling system.
There are generally two types of sampling - either
in-line sampling or bypass sampling and OGS has the
expertise and experience to provide such systems to
cover all operators requirements.
Sampling System
The automatic sampling of refined hydrocarbon liquids
for quality measurement is regulated by the following
international standards:
•	 API MPMS Chapter 8.2: Standard Practice for
Automatic Sampling of Petroleum and Petroleum
Products.
•	 ASTM D4177: Standard Practice for Automatic
Sampling of Petroleum and Petroleum Products.
•	 EN ISO 3171: Petroleum Liquids – Automatic pipeline sampling.
www.ogsl.com
For years, end users and their engineering contractors have striven to install flow metering systems for
which manufacturers offer a very precise uncertainty level.
SmartMix®
for Automatic Sampling with Exceptional Efficiency
Once installed, the performance of the
flow metering system must be corrected
using a sampling system, which in turn must
comply with international quality measurement
standards. While there is significant focus to
lower the flow metering uncertainty, the
maximum error that is admissible in the quality
measurement, particularly as a measure of
the mixing efficiency, remains comparatively
crude and inaccurate. Therefore, sampling
is still the “elephant in the room” that requires
immediate attention to reduce the significant
loss in revenue that is caused while using
current systems. To circumvent these problems,
our sister company, Oil & Gas Measurement
Limited (OGM) has developed the SmartMix®
technology, which has many unparalleled
efficiencies compared to current systems in
the market.
OGS designs and supplies manual, fast loop or isokinetic
homogeneous mixing systems to ensure compliance with
ISO 3171 using either clients nominated suppliers or our own
range of Maurer™ samplers and accessories as appropriate.
Generally for newer installations, the equipment proposed is
based on the understanding that no additional process mixing
is required in the sampling systems and that the process
lines are already well mixed to acceptable C1/C2 ratios. This
however, has not been verified by OGS and it may be
necessary to undertake further calculations to determine
if static mixing or the use of a jet mix system would be
required to ensure true representative sampling for each of the
product/fluid lines.
Sampling System
Typical SmartMix®
Sampling & Analysis Cabinet
www.ogsl.com
Typical SmartMix®
Skid
The SmartMix®
Technology and its Benefits
In general, assuming all other steps are done with extreme accuracy, the chain of uncertainty in
sampling or quality measurement is mainly dependent on how the representative sample is taken,
which is wholly dependent on the efficiency and accuracy of the mixing device employed. Any
inaccuracy in quality measurement results in significant financial exposure. Therefore, accurate and
homogeneous mixing is essential.
Mixing is the Key Step for Accurate Quality Measurement of Petroleum Liquids
“Sampling is not just ‘another’ function of measurement; it is the heart and soul of the profit figure... It
must start correctly if it is to end well!” (D.J. Fish, 1992)
Oil & Gas Measurement Limited’s (OGM’s) SmartMix®
technology brings a paradigm shift in efficient
and accurate mixing for the oil and gas and allied industries.
The SmartMix®
technology has the highest mixing efficiency
and accuracy thereby delivering the best investment for quality
measurement with rapid payback of investment. The technology
is engineered to avoid repeated recirculation of samples, thereby
ensuring a single pass and accurate sampling within the fast
loop by splitting the flow from the discharge side of the pump.
This twin stream design entering the jet-mix nozzle, along with the
SmartMix®
control system, provides superior and efficient mixing,
which in turn delivers practically infinite turndown in flowrates while
also ensuring zero pressure drop.
Key Benefits
•	 Greater than 97% mixing efficiency, saving millions of dollars in lost revenue.
•	 Efficient horizontal mixing even at very low velocities – without resorting to vertical installations
hence avoiding significant pressure drop due to bends while also eliminating significant cost of
pipeline rework.
•	 Efficient mixing even at the worst flow conditions (low velocities, low densities and/or low viscosities).
•	 Up to 80% shorter nozzle-scoop distance (compared to current systems in the market), allowing
very compact design where space is at a premium, particularly offshore.
•	 No pressure drop in the pipeline due to the presence of the nozzle and scoop assemblies.
•	 No emulsification of product due to efficient control of droplet size distribution.
•	 Significantly (up to 50%) lower pump power requirement compared to other system suppliers.
www.ogsl.com
The sampling system is optimised for low maintenance requirements and sustainability. An integral
component of the system is the cell sampler which ensures a consistent and repeatable sample is
taken. The cell sampler uses a three-step technique to ensure its performance stays unaffected by
possible variations in the process.
This sampler is essentially a power driven metering pump. The sampling mechanism is a tubular stem
with an inner concentric capture tube and a piston. Each cycle first captures a precise volume of
sample and then pumps it through a back pressure valve to a sample collection receiver.
The in-line sampler installed in a correctly designed system will take representative grabs of line
fluid at a predetermined rate normally relative to the pipeline flowrate. The composite of these grabs
(typically 1,000 to 10,000 collected during a pipeline transfer) provides a representative sample of the
oil batch for laboratory analysis and reference. The rate of sampling is normally controlled by a flow
computer which measures flow in the main export pipeline.
OGS will supply systems incorporating clients preferred/approved supplier of samplers as required. If
a customer has no preference we would use the most appropriate sampler or by choice, Maurer™
Instruments products which have the following sample rates:
• Electrically operated sampler - up to a maximum
15 grabs/min
• Pneumatically operated sampler - up to a maximum
30 grabs/min
Samplers
Water Cut and Density Measurement
It is common as part of the liquid sampling system to install densitometers and oil in water monitors for
online quality management.
OGS designs and manufactures such systems using industry recognised analyser manufacturers and
packages them with all necessary pressure let down equipment and controls.
Electric Insertion Sampler & Interface Box
Instruments products which have the following sample rates:
Sample Receiver & Weigh
Scales
Pneumatic Cell
Sampler
www.ogsl.com
Gas Analysis Packages
OGS can provide full analysis packages suitable for use in fiscal gas measurement. Typical gas
analysis packages would include:
•	 Gas chromatograph
(C1 – C12 as applicable)
•	 CO2
•	 H2
S
•	 Oxygen
•	 Dew point
•	 Wobbe index
•	 Other parameters to meet the clients
specific requirements
We utilise industry standard analysers which are then integrated within an enclosure complete with the
required pressure let-down equipment.
These enclosures are available in stainless steel or other suitable materials complete with full HVAC or
natural ventilation and fire and gas detection and alarm facilities.
OGS can provide complete design, manufacture, assembly and test of the following types of
metering systems for the following applications:
•	 Offshore platforms and FPSOs
•	 Onshore installations including terminals
and refineries
•	 Pipelines
•	 Petrochemical facilities
•	 Power stations
OGS can supply systems for hydrocarbon applications such as crude oil, conventional or
unconventional natural gas and condensate as well as refined products including LPG, lubricants, fuel
oil, kerosene and naphtha.
www.ogsl.com
OGS undertakes the complete design and supply of skid mounted or packaged equipment and our
scope of supply typically covers all stages of project execution including:
Scope of Supply
•	 Detailed design and engineering
•	 Project management
•	 Start-up and commissioning supervision
•	 Training and support
•	 Manufacture
•	 Shipping and packing
•	 Calibration, integrated testing and
certification
Gas Analyser House
Approvals
Since the company was established in 1989, we
have continously developed our approach to design,
procurement, project management, assembly, testing
and supply of packaged equipment.
OGS was one of the first systems integrators to achieve
ISO 9001 approval. Now, our approvals include:
•	 ISO 9001:2008 - Quality Management System
Registration
•	 ISO/TS 29001:2010 - Petroleum, petrochemical 		
and natural gas industries - Sector Specific Quality
Management System
•	 OHSAS 18001:2007- Health & Safety Management
System
We are approved by a wide range of operating
companies worldwide which include BP
, Shell, Chevron,
BG, Saudi Aramco, PDO and ADNOC Group
Companies, KOC and KNPC. We are also registered on
the FPAL and Achilles databases for the UK and Norway
and are a GE Global Source approved supplier.
Fast Loop System
Denmark House, St. Thomas Place, Ely, Cambridgeshire, CB7 4EX, UK
Email: info@oghl.co.uk | Tel: +44 1353 666640
www.ogsl.com
Revision 07/2018

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All you Need to Know About Sampling and Analysis - OGSI

  • 2. www.ogsl.com Oil & Gas Systems Limited (OGS) supplies packaged fiscal analysis and pipeline integrity measurement equipment including, but not limited to, process analyser system integration, flare metering and analysis, manual spot sample and automated sampling, CV, H2 S moisture and total sulphur analysis and water quality analysis (including oil in water). A representative sample of a hydrocarbon product is necessary to ensure proper accounting for transactions and efficient product processing. The amount of hydrocarbon product that is transported between producer, processor, distributor and end-user is significant. To be able to verify the exact composition of the product is important from an economic and product treatment standpoint. A small percentage saving made by correctly determining composition will quickly recoup the investment made in the purchase of a system designed to obtain an optimum sample. In addition, if the best sampling procedures are followed, the potential for disputes between supplier and customer will be greatly reduced. Some of the standards that must be adhered to ensure representative samples include ISO 10715 and API 14.1. These standards are the most common and current ones referenced on gas sampling procedures. This figure is a critical component of the flow formula from which we derive the product quantity. An error in sampling affects both quality and quantity, and ultimately profitability. Sampling Systems A crucial factor in petroleum measurement is quality analysis. For this reason liquid metering systems usually have an associated sampling system. There are generally two types of sampling - either in-line sampling or bypass sampling and OGS has the expertise and experience to provide such systems to cover all operators requirements. Sampling System The automatic sampling of refined hydrocarbon liquids for quality measurement is regulated by the following international standards: • API MPMS Chapter 8.2: Standard Practice for Automatic Sampling of Petroleum and Petroleum Products. • ASTM D4177: Standard Practice for Automatic Sampling of Petroleum and Petroleum Products. • EN ISO 3171: Petroleum Liquids – Automatic pipeline sampling.
  • 3. www.ogsl.com For years, end users and their engineering contractors have striven to install flow metering systems for which manufacturers offer a very precise uncertainty level. SmartMix® for Automatic Sampling with Exceptional Efficiency Once installed, the performance of the flow metering system must be corrected using a sampling system, which in turn must comply with international quality measurement standards. While there is significant focus to lower the flow metering uncertainty, the maximum error that is admissible in the quality measurement, particularly as a measure of the mixing efficiency, remains comparatively crude and inaccurate. Therefore, sampling is still the “elephant in the room” that requires immediate attention to reduce the significant loss in revenue that is caused while using current systems. To circumvent these problems, our sister company, Oil & Gas Measurement Limited (OGM) has developed the SmartMix® technology, which has many unparalleled efficiencies compared to current systems in the market. OGS designs and supplies manual, fast loop or isokinetic homogeneous mixing systems to ensure compliance with ISO 3171 using either clients nominated suppliers or our own range of Maurer™ samplers and accessories as appropriate. Generally for newer installations, the equipment proposed is based on the understanding that no additional process mixing is required in the sampling systems and that the process lines are already well mixed to acceptable C1/C2 ratios. This however, has not been verified by OGS and it may be necessary to undertake further calculations to determine if static mixing or the use of a jet mix system would be required to ensure true representative sampling for each of the product/fluid lines. Sampling System Typical SmartMix® Sampling & Analysis Cabinet
  • 4. www.ogsl.com Typical SmartMix® Skid The SmartMix® Technology and its Benefits In general, assuming all other steps are done with extreme accuracy, the chain of uncertainty in sampling or quality measurement is mainly dependent on how the representative sample is taken, which is wholly dependent on the efficiency and accuracy of the mixing device employed. Any inaccuracy in quality measurement results in significant financial exposure. Therefore, accurate and homogeneous mixing is essential. Mixing is the Key Step for Accurate Quality Measurement of Petroleum Liquids “Sampling is not just ‘another’ function of measurement; it is the heart and soul of the profit figure... It must start correctly if it is to end well!” (D.J. Fish, 1992) Oil & Gas Measurement Limited’s (OGM’s) SmartMix® technology brings a paradigm shift in efficient and accurate mixing for the oil and gas and allied industries. The SmartMix® technology has the highest mixing efficiency and accuracy thereby delivering the best investment for quality measurement with rapid payback of investment. The technology is engineered to avoid repeated recirculation of samples, thereby ensuring a single pass and accurate sampling within the fast loop by splitting the flow from the discharge side of the pump. This twin stream design entering the jet-mix nozzle, along with the SmartMix® control system, provides superior and efficient mixing, which in turn delivers practically infinite turndown in flowrates while also ensuring zero pressure drop. Key Benefits • Greater than 97% mixing efficiency, saving millions of dollars in lost revenue. • Efficient horizontal mixing even at very low velocities – without resorting to vertical installations hence avoiding significant pressure drop due to bends while also eliminating significant cost of pipeline rework. • Efficient mixing even at the worst flow conditions (low velocities, low densities and/or low viscosities). • Up to 80% shorter nozzle-scoop distance (compared to current systems in the market), allowing very compact design where space is at a premium, particularly offshore. • No pressure drop in the pipeline due to the presence of the nozzle and scoop assemblies. • No emulsification of product due to efficient control of droplet size distribution. • Significantly (up to 50%) lower pump power requirement compared to other system suppliers.
  • 5. www.ogsl.com The sampling system is optimised for low maintenance requirements and sustainability. An integral component of the system is the cell sampler which ensures a consistent and repeatable sample is taken. The cell sampler uses a three-step technique to ensure its performance stays unaffected by possible variations in the process. This sampler is essentially a power driven metering pump. The sampling mechanism is a tubular stem with an inner concentric capture tube and a piston. Each cycle first captures a precise volume of sample and then pumps it through a back pressure valve to a sample collection receiver. The in-line sampler installed in a correctly designed system will take representative grabs of line fluid at a predetermined rate normally relative to the pipeline flowrate. The composite of these grabs (typically 1,000 to 10,000 collected during a pipeline transfer) provides a representative sample of the oil batch for laboratory analysis and reference. The rate of sampling is normally controlled by a flow computer which measures flow in the main export pipeline. OGS will supply systems incorporating clients preferred/approved supplier of samplers as required. If a customer has no preference we would use the most appropriate sampler or by choice, Maurer™ Instruments products which have the following sample rates: • Electrically operated sampler - up to a maximum 15 grabs/min • Pneumatically operated sampler - up to a maximum 30 grabs/min Samplers Water Cut and Density Measurement It is common as part of the liquid sampling system to install densitometers and oil in water monitors for online quality management. OGS designs and manufactures such systems using industry recognised analyser manufacturers and packages them with all necessary pressure let down equipment and controls. Electric Insertion Sampler & Interface Box Instruments products which have the following sample rates: Sample Receiver & Weigh Scales Pneumatic Cell Sampler
  • 6. www.ogsl.com Gas Analysis Packages OGS can provide full analysis packages suitable for use in fiscal gas measurement. Typical gas analysis packages would include: • Gas chromatograph (C1 – C12 as applicable) • CO2 • H2 S • Oxygen • Dew point • Wobbe index • Other parameters to meet the clients specific requirements We utilise industry standard analysers which are then integrated within an enclosure complete with the required pressure let-down equipment. These enclosures are available in stainless steel or other suitable materials complete with full HVAC or natural ventilation and fire and gas detection and alarm facilities. OGS can provide complete design, manufacture, assembly and test of the following types of metering systems for the following applications: • Offshore platforms and FPSOs • Onshore installations including terminals and refineries • Pipelines • Petrochemical facilities • Power stations OGS can supply systems for hydrocarbon applications such as crude oil, conventional or unconventional natural gas and condensate as well as refined products including LPG, lubricants, fuel oil, kerosene and naphtha.
  • 7. www.ogsl.com OGS undertakes the complete design and supply of skid mounted or packaged equipment and our scope of supply typically covers all stages of project execution including: Scope of Supply • Detailed design and engineering • Project management • Start-up and commissioning supervision • Training and support • Manufacture • Shipping and packing • Calibration, integrated testing and certification Gas Analyser House Approvals Since the company was established in 1989, we have continously developed our approach to design, procurement, project management, assembly, testing and supply of packaged equipment. OGS was one of the first systems integrators to achieve ISO 9001 approval. Now, our approvals include: • ISO 9001:2008 - Quality Management System Registration • ISO/TS 29001:2010 - Petroleum, petrochemical and natural gas industries - Sector Specific Quality Management System • OHSAS 18001:2007- Health & Safety Management System We are approved by a wide range of operating companies worldwide which include BP , Shell, Chevron, BG, Saudi Aramco, PDO and ADNOC Group Companies, KOC and KNPC. We are also registered on the FPAL and Achilles databases for the UK and Norway and are a GE Global Source approved supplier. Fast Loop System
  • 8. Denmark House, St. Thomas Place, Ely, Cambridgeshire, CB7 4EX, UK Email: info@oghl.co.uk | Tel: +44 1353 666640 www.ogsl.com Revision 07/2018