SlideShare a Scribd company logo
1 of 8
Download to read offline
Jixi Zhang
Yanyao Jiang
e-mail: yjiang@unr.edu
Department of Mechanical Engineering (312),
University of Nevada, Reno, NV 89557
A Study of Inhomogeneous Plastic
Deformation of 1045 Steel
An experimental study was conducted on the inhomogeneous plastic deformation of 1045
steel subjected to monotonic tension and cyclic tension-compression. Small strain gages
were used to characterize the local deformation and transmission electron microscopy
(TEM) was used to study the microstructures associated with the observed deformation
phenomenon. Under monotonic tension, the strain of the Lu¨ders front was lower than the
full Lu¨ders strain. The local strains were inhomogeneous even at the work-hardening
stage. Under stress-controlled cyclic loading with stress amplitudes below the lower yield
stress, cyclic deformation consisted of an incubation stage, a significantly inhomogeneous
cyclic softening stage, and a saturation stage. Inhomogeneous cyclic plasticity persisted
at the saturation stage. A monotonic tension preload can eliminate the incubation stage in
the subsequent cyclic loading. Under asymmetric cyclic loading with a mean stress, the
cyclic plastic deformation was accompanied by noticeable inhomogeneous ratcheting
deformation. TEM was used to analyze the distribution and evolution of the dislocation
structures at different locations of the specimen. With increasing loading cycles, the dis-
location substructures evolved in a sequence of loose tangles, thick veins, long walls,
elongated cells, and equiaxial cells. Based upon the mechanical experiments and obser-
vations of dislocation arrangements, the mechanisms governing inhomogeneous cyclic
plastic deformation were discussed. ͓DOI: 10.1115/1.1647125͔
Keywords: Dislocation arrangement, inhomogeneous cyclic plastic deformation, Lu¨ders
band, SAE 1045 steel
1 Introduction
Inhomogeneous deformation associated with Lu¨ders band
propagation has been extensively investigated ͓1͔. During the
monotonic tension of an annealed mild steel, plastic deformation
is initiated in a local region indicated by a negative slope in the
stress-strain curve and propagates at a decreased stress level
known as the lower yield stress. A distinct plateau appears in the
stress-strain curve and the local deformation within the gage sec-
tion of the specimen is inhomogeneous, characterized with the
propagation of the Lu¨ders bands. In the plastically deformed re-
gions, the strain has a constant value ͑Lu¨ders strain͒ while the
deformation is elastic in the remaining area of the gage section.
After the Lu¨ders bands cover the whole gage section, deformation
is essentially homogeneous before necking develops ͓1͔.
For the materials exhibiting Lu¨ders band phenomenon under
monotonic tension, some interesting mechanical behaviors may
occur under cyclic loading. It is generally found that a carbon
steel subjected to strain-controlled cyclic loading experiences a
sudden drop in the stress amplitude response after a certain num-
ber of loading cycles ͓2͔. After an incubation phase of almost
purely elastic deformation, significant cyclic softening is observed
for carbon steels under fully reversed stress-controlled cyclic
loading with a stress amplitude lower than the lower yield stress
͓3–14͔. The larger the stress amplitude, the shorter the incubation
stage and the larger the saturated plastic strain amplitude ͓3͔. A
similar phenomenon was observed in normalized as well as
quenched and tempered low alloyed steels ͓15͔.
Inhomogeneous cyclic plastic deformation of carbon and al-
loyed steels has been investigated using photoelasticity ͓4,15͔,
microhardness ͓15͔, and strain gages ͓3,15͔. By using three small
strain gages glued on the gage section of a solid specimen, Eifler
and Macherauch ͓15͔ reported that an SAE 4140 steel experienced
inhomogeneous cyclic softening when subjected to a fully re-
versed stress-controlled loading. Uniform deformation was re-
ported to occur after a finite number of loading cycles. By using
ten small strain gages distributed along the specimen of a normal-
ized 1045 steel, quantitative measurement of the distribution of
plastic deformation during cyclic tension-compression loading
was investigated by Jiang ͓3͔. It was observed that the cyclic
plastic deformation was initiated in local areas of the specimen
and propagated through the gage section of the specimen with
increasing number of cycles. Inhomogeneous plastic strain devel-
oped during the cyclic softening and persisted at the saturation
stage. The inhomogeneous cyclic deformation was dependent on
the loading magnitude and evolved with continued cyclic loading.
Different local mean strains developed even though the stress-
controlled cyclic loading was symmetric. Under asymmetric
stress-controlled cyclic loading with a mean stress, inhomoge-
neous ratcheting deformation occurred in the direction of mean
stress after a period of incubation and the inhomogeneity persisted
at the saturation stage ͓3͔.
For mild carbon steels, the dislocation structures in ferrite
grains after cyclic loading have been studied ͓9,12,16–19͔. Most
researchers have focused on the observation of dislocation struc-
tures at the saturation state, usually, between 30% to 100% of the
total fatigue life of the material. At room temperature, the dislo-
cation arrangement in the surface layer differs considerably from
that of the interior of the specimen. On the surface, persistent slip
bands are usually observed independent of stress amplitude. In the
interior of the specimen, dislocations arrange themselves into cell
structures when the stress amplitude is high, or into bands when
the stress amplitude is low ͓9,12,16,17͔. Within the temperature
range of dynamic strain aging, dislocation bundles and broad
walls prevail even though the stress amplitude is high; while both
below and above the temperature range, the dislocations arrange
themselves into cells ͓18,19͔.
The current work was a continued effort to explore the inhomo-
geneous plastic deformation by adopting the experimental meth-
ods used earlier ͓3͔. The localized plastic deformation of 1045
steel subjected to monotonic tension and cyclic tension-
compression with and without a mean stress was further investi-
Contributed by the Materials Division for publication in the JOURNAL OF ENGI-
NEERING MATERIALS AND TECHNOLOGY. Manuscript received by the Materials
Division December 2, 2002; revision received November 5, 2003. Associate Editor:
W. Soboyejo.
164 Õ Vol. 126, APRIL 2004 Copyright © 2004 by ASME Transactions of the ASME
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
gated. The influence of monotonic tension preload on cyclic plas-
tic deformation and the persistence of inhomogeneous plastic
deformation during multiple-step cyclic loading were studied. At-
tempts were made to study the dislocation structures and the evo-
lution of dislocations during inhomogeneous deformation by us-
ing transmission electron microscopy ͑TEM͒. The mechanisms
involved in the initiation and propagation of inhomogeneous cy-
clic plastic deformation were discussed.
2 Experiments
The as-received SAE 1045 steel was in a hot rolled state with
the following chemical compositions: 0.46 wt.% C, 0.27 wt.% Si,
0.70 wt.% Mn, 0.019 wt.% P, 0.027 wt.% S, with balance of Fe.
Cylindrical specimens were machined after normalizing the mate-
rial at 815°C for 8 hours. The specimens were identical in material
and heat treatment to those used in a previous study ͓3͔. A typical
microstructure after normalization is shown in Fig. 1. The volume
fraction of pearlite was approximately 55% and the mean ferrite
grain size was 10 ␮m. The uniform gage section of the specimen
had a diameter of 12 mm and a gage length of 25.4 mm. The
gauge length surface was machined followed by polishing with
fine sand papers with grit size 600.
To measure local strains, a Micro-Measurements Group EA-06-
062MD-120 10-element strip gage was bonded on the surface
within the gage section of the specimen. The strip strain gage
length was 20 mm. Each gage element had a resistance of 120 ⍀
and the gage factor was 2.01. Each strain gage had an area of
1.57ϫ1.57 mm, with a spacing between strain gages in the strip of
2.1 mm. The row of strain gages was aligned with the specimen
axis identical to that used in a previous study ͓3͔. A 25.4 mm gage
length extensometer was attached to the specimen in the gage
section to measure the average deformation.
Experiments were conducted at room temperature in air. Cyclic
testing was conducted at a frequency of 0.25 Hz. During an ex-
periment, the load, extensometer displacement, and the outputs of
all the 10 strain gages were recorded simultaneously. Two hundred
data points were recorded for each variable during a loading
cycle. To distinguish the deformation measured by the extensom-
eter and the strain gages, the strain obtained from the extensom-
eter is referred to as ‘‘extensometer strain’’ while the strain gage
measurements are denoted as ‘‘local strains’’.
Thin foil TEM samples were prepared with the material cut
from the designated areas in the testing specimen using a low
speed diamond saw. The normal direction of the thin foils was
parallel to the specimen axis. The thin foils were mechanically
ground on both sides with fine sand papers down to a thickness of
100 ␮m. Discs of 3 mm diameter were punched from these foils.
The discs were then electropolished using a twin jet technique in
a solution of 10 vol.% perchloric acid mixed with 90 vol.% eth-
anol at Ϫ30 °C until perforation. The samples were examined
with a JEOL 200CX TEM operated at 200 KV.
3 Experimental Results
3.1 Lu¨ders Bands Under Monotonic Loading. Monotonic
tension was conducted under stroke ͑displacement͒-controlled
loading mode. The extension rate was 0.002 mm/s that corre-
sponded to an approximately 5ϫ10Ϫ5
/s strain rate. The results
are shown in Fig. 2. The upper yield stress is 420 MPa and the
lower yield stress is 400 MPa. The distinct plateau in the stress-
extensometer strain curve corresponds to the formation and propa-
gation of Lu¨ders bands. The full Lu¨ders strain ͑the length of the
plateau͒ is 0.98%. The dots and numbers in the stress-
extensometer strain curve ͑Fig. 2͑a͒͒ denote the moment that the
corresponding strain gage on the specimen showed the onset of
plastic deformation. In other words, a dot represents the specific
value of the extensometer strain at which the Lu¨ders front reached
the area covered by the numbered strain gage. The onset of plastic
deformation of each strain gage is indicated by an abrupt increase
in local strain, as shown in Fig. 2͑b͒. The area under Gage 10 was
the last area that experienced plastic deformation. The particular
moment did not correspond to the end of the plateau in the stress-
strain curve ͑Fig. 2͑a͒͒. Two factors are responsible for this dis-
crepancy. The extensometer gage length ͑25.4 mm͒ was longer
than the strip strain gage length ͑20 mm͒. More importantly, the
strain at the Lu¨ders front was significantly smaller than the full
Lu¨ders strain.
Detailed local strains shown in Fig. 2͑b͒ can provide a better
insight of the Lu¨ders band propagation. Both local strains and
extensometer strain are shown with respect to time. A number
shown on the side of each curve denotes a specific strain gage.
The strain gages in the strip were numbered starting from the top
of the gage section. After the extensometer strain reached 0.002,
which corresponded to the upper yield stress, the area covered by
Gage 2 and Gage 3 started to deform plastically. The process
continued with the plastic deformation occurring in the areas cov-
ered by Gages 4, 5, 6, 7, 8, 9, and 10. Except Gage 1, all the other
gages displayed a certain pattern. Among the ten strain gages,
eight gages ͑Gage 3ϳ10͒ experienced the abrupt deformation in
Fig. 1 Microstructure of SAE 1045 steel after normalization
Fig. 2 Monotonic tension behavior of 1045 steel: „a… mono-
tonic stress-extensometer strain curve; and „b… variations of
local strains
Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 165
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
such a way that the end of the strain burst was followed by the
start of the strain burst of the neighboring strain gage ͑Fig. 2͑b͒͒.
Considering the finite length of the strain gage, this observation
indicates that the value of the burst strain is approximately 0.66%.
Since the strain burst was followed by strain hardening in the
subsequent loading for a given location, a simple mathematic
speculation can lead to the conclusion that the ‘‘real’’ strain at the
Lu¨ders front should be a little smaller in value than that measured
using a small but finite length strain gage.
A vertical line in Fig. 2͑b͒ denotes the end of the plateau in the
stress-extensometer strain curve. A common conclusion from
early research is that the end of the plateau is the starting point of
homogeneous deformation in the gage section ͓1͔. However, the
results shown in Fig. 2͑b͒ clearly indicate that at the end of the
plateau, the local deformation was still inhomogeneous. The inho-
mogeneous deformation persisted in the work-hardening zone.
3.2 Localized Cyclic Plastic Deformation. A fully re-
versed stress-controlled tension-compression experiment was con-
ducted for 1550 cycles and the results are summarized in Fig. 3.
The stress amplitude was 320 MPa which was less than the lower
yield stress ͑400 MPa͒ of the material. The variations of local
strain amplitudes and mean strains with the number of loading
cycles were used to characterize the cyclic strain history. The
cyclic deformation process consisted of three stages: an incuba-
tion stage between 1ϳ230 cycles, a propagation stage between
230ϳ750 cycles, and a saturation stage after 750 cycles. During
the incubation stage, the material displayed almost purely elastic
deformation. After about 230 cycles, cyclic plastic deformation
was initiated in the area covered by Gage 2 ͑upper part of the gage
section͒ and propagated gradually into the two opposite directions
with increasing number of loading cycles. The shaded bars in-
serted in Fig. 3͑a͒ illustrate the propagation of the local plastic
deformation. The length of a bar represents the gage length cov-
ered by the strain gage strip ͑20 mm͒ and the shaded area denotes
the plastically deformed region. A threshold of 0.02% plastic
strain amplitude was used to define the onset of cyclic plastic
deformation. The local deformation was significantly inhomoge-
neous during the propagation stage. Inhomogeneous and nonzero
local mean strains developed simultaneously although symmetric
cyclic stress was applied.
After approximately 750 loading cycles, the strain amplitude
and mean strains became stabilized and the whole gage section
experienced cyclic plastic deformation. However, the stabilized
strain amplitudes and mean strains within the gage section were
not uniform ͑Fig. 3͑b͒͒. At Gage 2, where cyclic plastic deforma-
tion occurred first, the strain amplitude was the largest while the
mean strain was negative. At Gage 10, where cyclic plastic defor-
mation occurred last, the strain amplitude was the smallest while
the mean strain was positive. The non-uniform strains persisted
during subsequent cycling.
The influence of stress amplitude and mean stress on incuba-
tion, propagation, and saturation strain amplitude is listed in Table
1. A larger stress amplitude leads to a shorter incubation stage, a
shorter propagation stage, and a larger saturation strain amplitude.
A tensile mean stress slightly shortens the incubation period but
has no significant influence on the saturation strain amplitude.
However, a tensile mean stress reduces the propagation period
greatly. These results are consistent with those reported previously
͓3–8͔.
A two-step experiment was designed to examine the influence
of the monotonic tension preload on cyclic plastic deformation.
Monotonic tension was terminated when the extensometer strain
reached 0.5%. After the monotonic loading, the Lu¨ders bands had
propagated over a half of the gage section covering Gage 1 to
Gage 6 ͑Fig. 4͑a͒͒. The rest of the area covering Gage 7 to Gage
10 remained plastically undeformed.
Following the monotonic preload, a fully reversed stress-
controlled cyclic loading with a stress amplitude of 320 MPa was
applied. The magnitudes of local strains in the cyclic loading are
shown in Figs. 4͑b͒ and ͑c͒. One noticeable observation is the
elimination of the incubation period due to the monotonic preload.
In the area that had been plastically deformed in the monotonic
preload, the strain amplitude decreased slightly to the saturation
values. In the area that had not been plastically deformed in the
monotonic loading, incubation stage disappeared. The propagation
of cyclic plastic deformation occurred immediately upon the ap-
plication of the cyclic loading and the strain amplitudes of Gages
7, 8, and 9 increased gradually to the saturation values. The propa-
gation stage was noticeably shortened. The saturation strain am-
plitudes were nearly identical to those shown in Fig. 3, knowing
that the cyclic load magnitudes for the two cases were identical.
Results shown in Fig. 4͑c͒ reveal that the local mean strains were
scattered and distributed irregularly.
A three-step stress-controlled cyclic tension-compression ex-
periment was used to examine the influence of prior cyclic plas-
ticity history on further cyclic deformation at a different mean
stress. The stress amplitude was 300 MPa for all the three loading
steps and the mean stresses were 100 MPa, 0, and Ϫ100 MPa in
Step 1, Step 2, and Step 3, respectively. The numbers of loading
cycles performed in Step 1, Step 2, and Step 3 were 920, 1250,
and 1250, respectively. The results are summarized in Fig. 5 and
Table 2.
Cyclic plasticity in Step 1 eliminated the incubation and propa-
gation stages in Step 2 and Step 3. In each loading step, the strain
amplitudes do not change significantly, but the mean strain in-
Fig. 3 Cyclic deformation of 1045 steel under fully reversed
stress-controlled uniaxial loading: „a… variations of local strain
amplitudes and propagation of plastic zone; and „b… variations
of local mean strains
Table 1 Influence of stress amplitude and mean stress on cy-
clic plastic deformation
⌬␴/2 ͑MPa͒ ␴m ͑MPa) Ni ͑Cycles) Np ͑Cycles) ⌬␧/2 ͑%͒
350 0 12 48 0.35
320 0 230 470 0.25
270 0 6000 8000 0.15
320 80 160 ϳ5 0.25
300 100 240 5 0.23
166 Õ Vol. 126, APRIL 2004 Transactions of the ASME
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
creased gradually in the direction of mean stress ͑ratcheting͒. The
local mean strains were non-uniform. The heterogeneity persisted
and increased with the loading steps. It was reported ͓7,20͔ that
under multiple-step loading, materials exhibited a strong memory
of the previous loading history, and such memory had a great
influence on the subsequent ratcheting.
Also shown in Figs. 3 and 4 are the average local strains and
the extensometer strains. The average local strain was the average
of the strain values taken from the 10 strain gages. One purpose to
compare the two values was to monitor the possible breakage or
debonding of strain gages during an experiment. The small differ-
ence between the average local strain value and the extensometer
measurement was mainly due to the difference between the exten-
someter gage length ͑25.4 mm͒ and the length of the strain strip
͑20 mm͒, knowing that the deformation within the gage section
was non-uniform.
3.3 Dislocation Substructures. Under fully reversed stress-
controlled tension-compression loading with a stress amplitude of
320 MPa, four companion specimens were tested. The experi-
ments were terminated at different cycles and dislocation sub-
structures at different strain gage sites were examined. The loca-
tions where the TEM samples were taken and the number of
loading cycles tested are indicated in Fig. 3͑a͒. The loading cycles
corresponded to the incubation, propagation, and saturation
stages.
During the incubation stage, the dislocation substructure had no
obvious change as compared to that of the annealed condition. A
typical dislocation arrangement is shown in Fig. 6 for a sample
taken from the specimen that has been loaded for 200 loading
cycles. The dislocation density in ferrite was low. Individual dis-
locations could be identified clearly. There was no detectable in-
dication of plastic deformation in the ferrite grains.
Fig. 4 Influence of monotonic tension preload on cyclic defor-
mation: „a… local tensile strains under monotonic tension pre-
load; „b… variations of local strain amplitudes with loading
cycles in subsequent cyclic loading; and „c… variations of local
mean strains with loading cycles in subsequent cyclic loading
Fig. 5 Cyclic deformation of 1045 steel under three-step
stress-controlled cyclic loading: „a… variations of strain ampli-
tudes; and „b… variations of mean strains
Table 2 Influence of mean stress and strain history on ratch-
eting deformation
Step ␴m ͑M Pa) Ni ͑Cycles) Np ͑Cycles) ⌬␧/2 ͑%͒ ␧m (%)
1 100 240 5 0.23 1.4ϳ1.6
2 0 0 0 0.23 0.5ϳ0.85
3 Ϫ100 0 0 0.2 Ϫ0.58ϳϪ1.2
Fig. 6 Typical dislocation arrangement during the incubation
stage
Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 167
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
Figure 7 shows the typical dislocation arrangements during the
propagation stage. The experiment was terminated after 420
cycles, which was within the stage of cyclic plastic propagation
͑Fig. 3͑a͒͒. The local strains were significantly inhomogeneous
and different dislocation substructures were observed at different
strain gage sites ͑see Fig. 3͑a͒ and Fig. 7͒. Since ferrite grains in
the material were randomly oriented, the resolved shear stress
amplitudes acting on the primary slip systems of individual ferrite
grains were different. In addition, dislocation arrangements in in-
dividual ferrite grains differed even at the same strain gage site.
Here, the representative dislocation arrangements in the most se-
riously deformed ferrite grains are presented. On the area covered
by Gage 10 where the plastic deformation was the smallest as
compared to the rest of the area of the gage section, only a few
ferrite grains were plastically deformed. Shown in Fig. 7͑a͒ is a
typical dislocation configuration in plastically deformed ferrite
grains. Loose dislocation tangles indicated the initiation of plastic
deformation. These dislocation tangles were distributed randomly
within the ferrite grains, indicating that the locations for the ini-
tiation of plastic deformation were randomly distributed within
the ferrite grains. Figure 7͑b͒ shows the dislocation configuration
on the area covered by Gage 6 where the strain amplitude was
medium. Dislocation density increased sharply by dislocation
multiplication and thick dislocation multipole veins distributed
randomly within the ferrite grains.
At Gage 2, plastic deformation was the largest over the gage
section. Most ferrite grains were plastically deformed. A typical
dislocation arrangement in the ferrite grains is shown in Fig. 7͑c͒.
Further plastic deformation resulted in an increase in the diameter
and dislocation density of the veins. The process reached a point
where local instabilities in the veins occurred due to dislocation
interaction and annihilation. This was followed by the evolution
of dislocation substructures into thinner yet denser dislocation
walls. The dislocation density between the walls was very low.
Although the build-up of macroscopic strain was complete at
the end of the propagation stage, continued cyclic loading led to a
further development of dislocation structures. The dislocation
configuration at the saturation state at a cycle number of 1550 is
shown in Fig. 8. In general, long and dense walls, elongated cells,
and equiaxial cells were observed. There were no obvious quali-
tative differences among dislocation arrangements for the material
within the gage length.
At the stage of cyclic plastic deformation propagation, the de-
formation process can be accomplished by single slips and the
influence of the grain/phase boundaries is not significant. How-
ever, in the subsequent transition to the cell structures, multiple
slip process is a necessity. At this point, the grain/phase bound-
aries play an important role. The plastic deformation in grain/
phase boundaries requires more activated slip systems due to the
constraints introduced. TEM observations confirmed that the mul-
tiple slip systems were always activated at first at the grain/phase
boundaries that resulted in the formation of the cell structures. A
typical TEM micrograph at the saturation stage is shown in Fig. 9.
Arrow A points to a grain boundary and Arrows B and C indicate
phase boundaries. With continued cyclic loading, the dislocation
cells were developed further into the central zone of the ferrite
grains.
4 Discussions
Strain gages provide a practical and accurate method to mea-
sure the local deformation. The results shown in Fig. 2͑b͒ are
different from those of previous research on Lu¨ders bands in sev-
Fig. 7 Typical dislocation arrangements during the propaga-
tion stage „at cycle 420…: „a… at Gage 10 „low local strain ampli-
tude: 0.165%…; „b… at Gage 6 „medium local strain amplitude:
0.2%…; and „c… at Gage 2 „high local strain amplitude: 0.23%…
Fig. 8 Typical dislocation arrangement at the saturation stage
168 Õ Vol. 126, APRIL 2004 Transactions of the ASME
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
eral aspects. It is generally asserted that during propagation of
Lu¨ders bands, plastic strain in the plastically deformed zone is
equal to the full Lu¨ders strain. Upon the start of work-hardening,
the deformation is uniform. The current work reveals that inho-
mogeneous deformation persists into the work-hardening stage.
The Lu¨ders bands results reported in the current investigation
are inconsistent with those of the previous studies. The testing
material, the specimen geometry, and the techniques used to mea-
sure the local strains may have contributed to the discrepancy. A
thin and flat specimen was often used in the investigation of Lu¨d-
ers bands ͓21–32͔. In the current investigation, specimens of a
normalized 1045 steel with a circular cross section were tested.
An obvious advantage in using a specimen with a flat surface is
the convenience and suitability for surface observations. The pos-
sible influence of the testing specimen geometry on the Lu¨ders
band observations may require further investigation. Usually, sur-
face scratches ͓21–23,33͔, surface grid ͓24,25͔, contrast interfer-
ometer ͓22,23,26͔, stresscoat ͓34͔, electroplating of the specimen
prior to testing ͓27͔, optical ‘‘To¨pler Schlieren’’ method ͓21,33͔,
critical macro-illumination ͓28͔, gridreflection ͓26͔, clip-
extensometer ͓29,35͔, high speed camera ͓30͔, and infrared cam-
era ͓31͔ were used to observe the Lu¨ders bands and to identify the
local strains. These methods do not provide an accurate quantita-
tive measurement of the local strain. It is noted that by using four
small strain gages bonded on the specimen, a similar phenomenon
to that shown in Fig. 2͑b͒ was observed in an annealed aluminum
alloy under monotonic tension ͓32͔.
The formation and propagation of Lu¨ders bands in irons and
carbon steels under monotonic tension are generally attributed to
the strong interaction of interstitial atoms with dislocations,
known as Cottrell atmospheres ͓1͔. In the Cottrell atmospheres,
interstitial atoms segregate to dislocations and pin them in posi-
tions to lower the lattice distortion energy. In a normalized 1045
steel, the yield stress of pearlite is much higher than that of ferrite
͓36–38͔. In the current investigation, the strain amplitude was low
and plastic deformation took place mainly in the ferrite grains.
The ferrite grains contain small amount of carbon and nitrogen
atoms in solid solution and the Cottrell atmospheres play an im-
portant role in plastic deformation. In monotonic tension, the
abrupt increase of strain at the Lu¨ders front can be ascribed to the
dislocations unpinned from the Cottrell atmospheres. Their mo-
tion leads to an abrupt multiplication of new dislocations. Subse-
quently, dislocations multiply further but slowly.
Previous studies have confirmed that cyclic plasticity of low
carbon steels can eliminate Lu¨ders bands phenomenon in a sub-
sequent monotonic tension ͓10–14,39–41͔. This elimination oc-
curs in the first half cycle for stress amplitude higher than the
yield point. For stress amplitude below the yield point, the Lu¨ders
strain decreases continuously with increasing number of cycles.
The current investigation reveals that a monotonic tension preload
eliminates the incubation stage and either shortens or completely
eliminates the propagation stage of the cyclic plastic deformation
in the subsequent cyclic loading. It is reasonable to infer from the
observations that the formation and propagation of Lu¨ders bands
under monotonic tension and the inhomogeneous cyclic plastic
deformation phenomenon should be closely related in terms of
mechanism.
Klesnil and Luka´sˇ ͓10,11͔ used the Cottrell atmospheres to in-
terpret successfully the mechanism of the cyclic softening of low
carbon steels under stress-controlled cyclic loading with the stress
amplitude being below the yield stress. A low carbon steel ͑0.07%
C, 0.48% Mn, 0.3% Si, 0.018% P, 0.019% S͒ with a mean grain
size of ferrite of 40 ␮m was used. The yield stress of the material
was 278 MPa. Stress was cycled between 228 MPa and 250 MPa.
It was noted that cyclic plasticity was initiated at the first loading
cycle for the cases under consideration ͓10,11͔. There exist a few
ferrite grains in the material where certain dislocations are less
effectively pinned by interstitials and can move at a stress level
below the yield stress. In the first half cycle, a small number of
such dislocations in some isolated grains are unpinned. This pro-
cess is repeated in each loading cycle followed. As a result, the
number of grains with free dislocations and bulk plastic strain
amplitude increase with increasing loading cycles. On the other
hand, fatigue hardening process, namely the increase of disloca-
tion density, and formation of dislocation structure occur in these
grains that lead to a decrease in plastic strain amplitude. The su-
perposition and interaction of these two processes result in the
observed cyclic softening and hardening phenomenon.
It is noticed that the microstructure and cyclic deformation be-
havior of the 1045 steel used in the current investigation are dif-
ferent from those of the low-carbon steel. In the current study, the
size of the ferrite grains is much smaller and they are separated
and constrained by the pearlite grains. The yield stress of the
ferrite grains is much higher than that in the low carbon steel. For
the 1045 steel under stress-controlled cyclic loading with stress
amplitude much lower than the lower yield stress, the incubation
stage is long and cannot be ignored. During the cyclic softening
stage, the distribution of local strains is significantly inhomoge-
neous. The local deformation depends not only on the number of
the ferrite grains with free dislocations but also on the extent of
plastic deformation of these ferrite grains. Therefore, the mecha-
nism of cyclic plasticity of the 1045 steel should be different from
that of the low-carbon steel.
For the 1045 steel under stress-controlled cyclic loading with a
stress amplitude much lower than the lower yield stress, deforma-
tion is almost purely elastic during the incubation stage. The dis-
location configuration is identical to that in the original normal-
ized condition with no observable change in the dislocation
density. Traditionally, phase/grain boundaries are viewed as the
most possible sites of stress concentration where pre-yield micros-
train may occur ͓42͔. However, during the incubation stage, the
concentration and pile-up of dislocations at the phase/grain
boundaries were rarely observed. As shown in Fig. 7, the loose
dislocation tangles, indicators of the initiation of plastic deforma-
tion, distribute randomly within the ferrite grains. Significant
changes in dislocation density and configuration can be observed
only during the propagation phase. During the saturation stage,
dislocation cells are found to form at first at phase/grain bound-
aries. The formation of the cells gradually propagates into the
interior of the grains.
The microscopic mechanism involved in the inhomogeneous
cyclic plastic deformation can be discussed based on the experi-
mental observations. In the incubation stage, the dislocations
pinned by the Cottrell atmospheres relax gradually under cyclic
stressing and become free and mobile dislocations. At the propa-
gation stage, the movement of free dislocations leads to the mul-
tiplication, interaction, and annihilation of dislocations. The dis-
Fig. 9 Dislocation cells are formed at first at the grainÕphase
boundary „at 1550th cycle in a saturation stage…
Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 169
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
location configurations evolve into dislocation tangles, veins, and
dense walls. In the later phase of propagation and the early phase
of saturation, multiple slip systems are activated at first near the
phase/grain boundaries and then propagate into the interior of the
ferrite grains. The dislocation arrangements eventually evolve into
cell structures.
The viewpoint is supported by the experimental results from the
two-step loading experiment shown in Fig. 4. In the plastically
deformed zone, the dislocations in the ferrite grains had been
unpinned and multiplied sufficiently. As a result, the incubation
and propagation stages were eliminated in the subsequent cyclic
loading. In the area where deformation remained macroscopically
elastic after the tension preload, the incubation stage disappeared
in the second loading step. This suggests that during the propaga-
tion process of Lu¨ders bands under the monotonic tension, the
dislocations in the plastically undeformed zone have been un-
pinned from the Cottrell atmospheres. However, these dislocations
do not move or only make local short-ranged movement, and
immediate generation of new dislocations has not yet taken place.
The aforementioned discussion was concentrated on the inho-
mogeneous cyclic plasticity, the associated dislocation substruc-
tures, and possible mechanisms. However, the underlying mecha-
nism for localized cyclic plasticity has not been fully explained.
The mechanism governing the propagation of cyclic plastic defor-
mation from one area to another in the specimen remains unclear.
The mechanism operative in the localized monotonic plasticity
associated with the formation of Lu¨ders bands in irons and carbon
steels probably can provide some enlightenment.
During monotonic tension of irons and carbon steels, Lu¨ders
bands are believed to nucleate at points of high local stresses, such
as fillets, precipitates, and grain boundaries ͓1͔. The propagation
of Lu¨ders bands depends on factors such as crystal structure, grain
size, shape of the sample, composition, and microstructure ͓43͔.
The propagation of Lu¨ders bands in single crystals probably is
engendered by the local constraints and stress concentrations set
up between the deformed and undeformed regions. In a fine-
grained mild steel, the edge of Lu¨ders bands appears sharp. It is a
reasonable speculation that deformation is spreading grain by
grain through the specimen. Dislocations in the yielding grain run
up to the grain boundary, and form pile-up arrays of dislocations,
whose presence increases the stress in the neighboring grain until
a dislocation source there becomes unpinned and the grain yields.
As the grain size increases, the edge of Lu¨ders band becomes
diffuse. As pointed by Hall ͓1͔, ‘‘This effect arises approximately
at the point where Hutchison’s curve ͓44͔ for the upper yield
stress with respect to grain size intersects the lower yield stress. In
other words, the stress differences are here so low that any small
inhomogeneity in grain size will cause part of the band front to
progress far in advance of the remainder.’’
The inhomogeneous cyclic plastic deformation has a similarity
to the propagation of the Lu¨ders band. However, whether or not
similar or identical mechanisms exist for the two phenomena re-
quires further investigation. In addition, the effect of the stress
state on the inhomogeneous cyclic plasticity is also a subject of
future research.
5 Conclusions
From the experimental observations on the inhomogeneous
plastic deformation of 1045 steel, the following conclusions can
be drawn:
1. Under monotonic tension, the burst strain of Lu¨ders front is
much lower than the full Lu¨ders strain. The local deformation
remains inhomogeneous even at the work-hardening stage after
the termination of the Lu¨ders band propagation.
2. For stress-controlled tension-compression cyclic loading
with the maximum stress lower than the lower yield stress of the
material, cyclic plastic deformation is characterized by three
stages: incubation, propagation, and saturation. The local strains
are significantly inhomogeneous during the propagation stage and
the inhomogeneity persists at the saturation stage.
3. The monotonic tension preload can eliminate or shorten the
incubation and propagation stages of the cyclic plasticity in the
subsequent cyclic loading.
4. Inhomogeneous cyclic plasticity persists under multiple-step
loading. The inhomogeneity is evidenced mainly by the persistent
difference in local mean strains.
5. During the incubation stage, the dislocation structures do not
change significantly. With increasing loading cycles, the disloca-
tion structures evolve in a sequence of loose tangles, thick veins,
long walls, elongated cells, and equiaxial cells.
6. Under cyclic stressing, the dislocations pinned by the Cot-
trell atmospheres in the ferrite grains are unpinned gradually and
become free and mobile dislocations. The movement of free dis-
locations leads to the multiplication, interaction, and annihilation
of dislocations. Dislocation cells are formed at first at the grain
boundaries with the activation of multiple slip systems followed
by the cells propagation into the interior of the ferrite grains.
Acknowledgment
Financial support was provided by the National Science Foun-
dation ͑CMS-9984857͒. TEM experiments were conducted at the
National Center for Electron Microscopy at Lawrence Berkeley
National Laboratory. The assistance of Drs. Eric Stach, Tamara
Radetic, and Chengyu Song is greatly appreciated.
Nomenclature
⌬␴/2ϭ stress amplitude
␴m ϭ mean stress
R ϭ stress ratio ͑minimum stress over maximum stress͒
Ni ϭ number of loading cycle of the incubation stage
Np ϭ number of loading cycle of the propagation stage
␧ ϭ extensometer strain
⌬␧/2 ϭ stabilized strain amplitude
␧m ϭ mean strain
␧L1 ϭ strain at the Lu¨ders front
␧L ϭ full Lu¨ders strain
References
͓1͔ Hall, E. O., 1970, Yield Point Phenomena in Metals and Alloys, Plenum Press,
New York.
͓2͔ Fatemi, A., and Stephens, R. I., 1989, ‘‘Cyclic Deformation of 1045 Steel
Under In-Phase and 90° Out-of-Phase Axial-Torsional Loading Conditions,’’ in
Multiaxial Fatigue, Analysis and Experiments, AE-14, G. E. Leese and D.
Socie, eds., SAE International, pp. 139–147, Chap. 10.
͓3͔ Jiang, Y., 2001, ‘‘An Experimental Study of Inhomogeneous Cyclic Plastic
Deformation,’’ ASME J. Eng. Mater. Technol., 123, pp. 274–280.
͓4͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1977, ‘‘Inhomogeneous
Deformation Processes in the Incipient Crack-Free Fatigue Stage of Unalloyed
Steels,’’ Arch. Eisenhuettenwes., 48, pp. 575–578.
͓5͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1978, ‘‘On the Influence of
Mean Stress on the Fatigue Behavior of Unalloyed Steels,’’ Arch. Eisen-
huettenwes., 49, pp. 31–36.
͓6͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1979, ‘‘Cyclic Induced Creep
of a Plain Carbon Steel at Room Temperature,’’ Fatigue Eng. Mater. Struct., 1,
pp. 287–295.
͓7͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1979, ‘‘Macroscopic
Changes of Length as a Consequence of Changes of Mean Stress During
Cyclic Tension-Compression Tests on CK45,’’ Arch. Eisenhuettenwes., 50, pp.
439–442.
͓8͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1980, ‘‘Macroscopic
Changes of Length Under Cyclic Load for Steel CK45 in Normalized and in
Strained Condition,’’ Arch. Eisenhuettenwes., 51, pp. 155–157.
͓9͔ Pohl, K., Mayr, P., and Macherauch, E., 1981, ‘‘Cyclic Deformation Behavior
of a Low Carbon Steel in the Temperature Range Between Room Temperature
and 850 K,’’ Int. J. Fract., 17, pp. 221–233.
͓10͔ Klesnil, M., and Luka´sˇ, P., 1992, Fatigue of Metallic Materials, Elsevier,
Amsterdam-Oxford-New York-Tokyo.
͓11͔ Klesnil, M., and Luka´sˇ, P., 1967, ‘‘Fatigue Softening and Hardening of An-
nealed Low-Carbon Steel,’’ J. Iron Steel Inst., London, 205, pp. 746–749.
͓12͔ Klesnil, M., Holzmann, M., Luka´sˇ, P., and Rysˇ, P., 1965, ‘‘Some Aspects of
Fatigue Process in Low-Carbon Steel,’’ J. Iron Steel Inst., London, 203, pp.
47–53.
170 Õ Vol. 126, APRIL 2004 Transactions of the ASME
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
͓13͔ Abel, A., and Muir, H., 1975, ‘‘Fatigue Softening on Low-Carbon Steel,’’
Philos. Mag., 32, pp. 553–563.
͓14͔ Abel, A., and Muir, H., 1973, ‘‘The Nature of Microyielding,’’ Acta Metall.,
21, pp. 99–105.
͓15͔ Eifler, D., and Macherauch, E., 1983, ‘‘Inhomogeneous Work-Softening Dur-
ing Cyclic Loading of SAE 4140 in Different Heat Treated States,’’ Proc. 2nd
Int. Sym. Defects, Fract. & Fat., G. C. Sih and J. W. Provan, eds., Can Mar-
tinus Nijhoff Publ The Hague, Neth, pp. 171–182.
͓16͔ Klesnil, M., and Luka´sˇ, P., 1965, ‘‘Dislocation Arrangement in the Surface
Layer of ␣-Iron Grains during Cyclic Loading,’’ J. Iron Steel Inst., London,
203, pp. 1043–1048.
͓17͔ Pohl, K., Mayr, P., and Macherauch, E., 1980, ‘‘Persistent Slip Band in the
Interior of a Fatigued Low Carbon Steel,’’ Scr. Metall., 14, pp. 1167–1169.
͓18͔ Christ, H.-J., Wamukwamba, C. K., and Mughrabi, H., 1997, ‘‘The Effect of
Mean Stress on the High-Temperature Fatigue Behavior of SAE 1045 Steel,’’
Mater. Sci. Eng., A, 234–236, pp. 382–385.
͓19͔ Weisse, M., Wamukwamba, C. K., Christ, H.-J., and Mughrabi, H., 1993, ‘‘The
Cyclic Deformation and Fatigue Behavior of the Low Carbon Steel SAE 1045
in the Temperature Regime of Dynamic Strain Ageing,’’ Acta Metall. Mater.,
41, pp. 2227–2233.
͓20͔ Jiang, Y., and Sehitoglu, H., 1994, ‘‘Multiaxial Cyclic Ratchetting Under Mul-
tiple Step Loading,’’ Int. J. Plast., 10, pp. 849–870.
͓21͔ Hall, E. O., 1951, ‘‘The Deformation and Aging of Mild Steel: II. Character-
istics of the Lu¨ders Deformation. III. Discussion of Results,’’ Proc. Phys. Soc.
London, Sect. B, 64, pp. 742–753.
͓22͔ Iricibar, R., Mazza, J., and Cabo, A., 1975, ‘‘The Microscopic Strain Profile of
a Propagating Lu¨ders Band Front in Mild Steel,’’ Scr. Metall., 9, pp. 1051–
1058.
͓23͔ Iricibar, R., Mazza, J., and Cabo, A., 1977, ‘‘On the Lu¨ders Band in Mild
Steel-I,’’ Acta Metall., 25, pp. 1163–1168.
͓24͔ Prewo, K., Li, J. C. M., and Gensamer, M., 1972, ‘‘Lu¨ders Band Motion in
Iron,’’ Metall. Trans., 3, pp. 2261–2269.
͓25͔ Lloyd, D. J., and Morris, L. R., 1977, ‘‘Lu¨ders Band Deformation in a Fine
Grained Aluminum Alloy,’’ Acta Metall., 25, pp. 857–861.
͓26͔ Verel, D. J., and Sleeswyk, A. W., 1973, ‘‘Lu¨ders Band Propagation at Low
Velocities,’’ Acta Metall., 21, pp. 1087–1098.
͓27͔ Liss, R. B., 1957, ‘‘Lu¨ders Bands,’’ Acta Metall., 5, pp. 341–342.
͓28͔ Boxall, T. D., and Hundy, B. B., 1955, ‘‘Photographing Stretcher-Strain Mark-
ings With the Vickers Projection Microscope,’’ Metall. Trans., 51, pp. 52–54.
͓29͔ Iricibar, R., and Mazza, J., 1975, ‘‘Meaning of the Strain Profile of a Propa-
gating Lu¨ders Band Front,’’ Scr. Metall., 9, pp. 1045–1050.
͓30͔ Miyazaki, S., and Fujita, H., 1979, ‘‘Dynamic Observation of the Process of
Lu¨ders Band Formation in Polycrystalline Iron,’’ Trans. Jpn. Inst. Met., 20, pp.
603–608.
͓31͔ Louche, H., and Chrysochoos, A., 2001, ‘‘Thermal and Dissipative Effects
Accompanying Lu¨ders Band Propagation,’’ Mater. Sci. Eng., A, 307, pp. 15–
22.
͓32͔ Onodera, R., Nonomura, M., and Aramaki, M., 2000, ‘‘Stress Drop, Lu¨ders
Strain and Strain Rate During Serrated Flow,’’ J. Jpn. Inst. Met., 64, pp. 1162–
1171.
͓33͔ Sylwestrowicz, W., and Hall, E. O., 1951, ‘‘The Deformation and Aging of
Mild Steel,’’ Proc. Phys. Soc. London, Sect. B, 64, pp. 495–502.
͓34͔ Fisher, J. C., and Rogers, H. C., 1956, ‘‘Propagation of Lu¨ders Bands in Steel
Wires,’’ Acta Metall., 4, pp. 180–185.
͓35͔ Moon, D. W., 1971, ‘‘Strain Distribution Through a Propagating Lu¨ders Band
Front,’’ Scr. Metall., 5, pp. 213–216.
͓36͔ Karlsson, B., and Linde´n, G., 1975, ‘‘Plastic Deformation of Ferrite-Pearlite
Structures in Steel,’’ Mater. Sci. Eng., 17, pp. 209–219.
͓37͔ Karlsson, B., and Linde´n, G., 1975, ‘‘Plastic Deformation of Eutectoid Steel
With Different Cementite Morphologies,’’ Mater. Sci. Eng., 17, pp. 153–164.
͓38͔ Karlsson, B., and Sundstrom, B. O., 1974, ‘‘Inhomogeneity in Plastic Defor-
mation of Two-Phase Steels,’’ Mater. Sci. Eng., 16, pp. 161–168.
͓39͔ Ivanova, V. S., Terent’yev, V. F., and Poyda, V. G., 1970, ‘‘Features of the
Built-up of Strain in Low-Carbon Steel Subjected to Cycles of Stress,’’ Phys.
Met. Metallogr., 30, pp. 165–171.
͓40͔ Oates, G., and Wilson, D. V., 1964, ‘‘The Effects of Dislocation Locking and
Strain Aging on the Fatigue Limit of Low-Carbon Steel,’’Acta Metall., 12, pp.
21–33.
͓41͔ Abel, A., and Muir, H., 1973, ‘‘The Effect of Cyclic Loading on Subsequent
Yielding,’’ Acta Metall., 21, pp. 93–97.
͓42͔ Carrington, W. E., and McLean, D., 1965, ‘‘Slip Nuclei in Silicon-Iron,’’ Acta
Metall., 13, pp. 493–499.
͓43͔ Ananathan, V. S., and Hall, E. O., 1991, ‘‘Macroscopic Aspects of Lu¨ders
Band Deformation in Mild Steel,’’ Acta Metall. Mater., 39, pp. 3153–3160.
͓44͔ Hutchison, M. M., 1963, ‘‘The Temperature Dependence of the Yield Stress of
Polycrystalline Iron,’’ Philos. Mag., 8, pp. 121–127.
Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 171
Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use

More Related Content

What's hot

Mechanical testing of materials
Mechanical testing of materialsMechanical testing of materials
Mechanical testing of materialsAli Elgazzar
 
Dislocations and strengthening mechanisms
Dislocations and strengthening mechanismsDislocations and strengthening mechanisms
Dislocations and strengthening mechanismsADEGBUJI QUDUS ABAYOMI
 
Physical properties of dental material [autosaved]
Physical properties of dental material [autosaved]Physical properties of dental material [autosaved]
Physical properties of dental material [autosaved]shailjakatiyar2
 
Metallurgy P R O P E R T I E S And Definitions
Metallurgy   P R O P E R T I E S And DefinitionsMetallurgy   P R O P E R T I E S And Definitions
Metallurgy P R O P E R T I E S And DefinitionsMoiz Barry
 
Stress-Strain Curves for Metals, Ceramics and Polymers
Stress-Strain Curves for Metals, Ceramics and PolymersStress-Strain Curves for Metals, Ceramics and Polymers
Stress-Strain Curves for Metals, Ceramics and PolymersLuís Rita
 
Aircraft materials lecture 2
Aircraft materials lecture 2Aircraft materials lecture 2
Aircraft materials lecture 2Kanupriya jhanji
 
Mechanical properties of Materials
Mechanical properties of MaterialsMechanical properties of Materials
Mechanical properties of MaterialsMuthukumar V
 
IMPACT TEST REPORT ...
IMPACT TEST REPORT                                                           ...IMPACT TEST REPORT                                                           ...
IMPACT TEST REPORT ...musadoto
 
Materials testing
Materials testingMaterials testing
Materials testingrishal619
 
Influence of intrinsic solidification behavior on solidification of AISI3XX
Influence of intrinsic solidification behavior on solidification of AISI3XXInfluence of intrinsic solidification behavior on solidification of AISI3XX
Influence of intrinsic solidification behavior on solidification of AISI3XXMainak Saha(मैनक साहा)
 

What's hot (18)

Mechanical tests
Mechanical testsMechanical tests
Mechanical tests
 
impact test 10-4
impact test 10-4impact test 10-4
impact test 10-4
 
Mechanical testing of materials
Mechanical testing of materialsMechanical testing of materials
Mechanical testing of materials
 
Mechanical Testing of Materials
Mechanical Testing of Materials Mechanical Testing of Materials
Mechanical Testing of Materials
 
Dislocations and strengthening mechanisms
Dislocations and strengthening mechanismsDislocations and strengthening mechanisms
Dislocations and strengthening mechanisms
 
Physical properties of dental material [autosaved]
Physical properties of dental material [autosaved]Physical properties of dental material [autosaved]
Physical properties of dental material [autosaved]
 
Materials testing
Materials testingMaterials testing
Materials testing
 
Metallurgy P R O P E R T I E S And Definitions
Metallurgy   P R O P E R T I E S And DefinitionsMetallurgy   P R O P E R T I E S And Definitions
Metallurgy P R O P E R T I E S And Definitions
 
Stress-Strain Curves for Metals, Ceramics and Polymers
Stress-Strain Curves for Metals, Ceramics and PolymersStress-Strain Curves for Metals, Ceramics and Polymers
Stress-Strain Curves for Metals, Ceramics and Polymers
 
Aircraft materials lecture 2
Aircraft materials lecture 2Aircraft materials lecture 2
Aircraft materials lecture 2
 
Mechanical properties of Materials
Mechanical properties of MaterialsMechanical properties of Materials
Mechanical properties of Materials
 
IMPACT TEST REPORT ...
IMPACT TEST REPORT                                                           ...IMPACT TEST REPORT                                                           ...
IMPACT TEST REPORT ...
 
Hardness test
Hardness testHardness test
Hardness test
 
Materials testing
Materials testingMaterials testing
Materials testing
 
Mechanical Tests
Mechanical TestsMechanical Tests
Mechanical Tests
 
Chapter 4 (JF302)
Chapter 4 (JF302)Chapter 4 (JF302)
Chapter 4 (JF302)
 
Influence of intrinsic solidification behavior on solidification of AISI3XX
Influence of intrinsic solidification behavior on solidification of AISI3XXInfluence of intrinsic solidification behavior on solidification of AISI3XX
Influence of intrinsic solidification behavior on solidification of AISI3XX
 
Creep & fatigue
Creep & fatigueCreep & fatigue
Creep & fatigue
 

Viewers also liked (17)

Boletim (6)
Boletim (6)Boletim (6)
Boletim (6)
 
Comment third ed
Comment third edComment third ed
Comment third ed
 
Boletim (8)
Boletim (8)Boletim (8)
Boletim (8)
 
01 fhwa choques y vuelcos por despistes vehículo solo
01 fhwa choques y vuelcos por despistes vehículo solo01 fhwa choques y vuelcos por despistes vehículo solo
01 fhwa choques y vuelcos por despistes vehículo solo
 
17 ohio 2016 manual completo fr si
17 ohio 2016 manual completo fr si17 ohio 2016 manual completo fr si
17 ohio 2016 manual completo fr si
 
5 brief asv dreznes bfos-bfos-unlp-gosi
5 brief asv dreznes bfos-bfos-unlp-gosi5 brief asv dreznes bfos-bfos-unlp-gosi
5 brief asv dreznes bfos-bfos-unlp-gosi
 
Boletim (9)
Boletim (9)Boletim (9)
Boletim (9)
 
Herramientas educativas web_21
Herramientas educativas web_21Herramientas educativas web_21
Herramientas educativas web_21
 
6 fjs o 41211 vs. tcr nicaragua
6 fjs o 41211 vs. tcr nicaragua6 fjs o 41211 vs. tcr nicaragua
6 fjs o 41211 vs. tcr nicaragua
 
Herramientas manuales y_motorizadas (1)
Herramientas manuales y_motorizadas (1)Herramientas manuales y_motorizadas (1)
Herramientas manuales y_motorizadas (1)
 
El futbol (3)
El futbol (3)El futbol (3)
El futbol (3)
 
3 egic dnv cihnº10 alcantarillas
3 egic dnv cihnº10 alcantarillas3 egic dnv cihnº10 alcantarillas
3 egic dnv cihnº10 alcantarillas
 
Gira estudio asv fhwa trentacoste
Gira estudio asv fhwa trentacosteGira estudio asv fhwa trentacoste
Gira estudio asv fhwa trentacoste
 
10 chicananivel crucedobleniveldesnivel
10 chicananivel crucedobleniveldesnivel10 chicananivel crucedobleniveldesnivel
10 chicananivel crucedobleniveldesnivel
 
Boletim (11)
Boletim (11)Boletim (11)
Boletim (11)
 
Boletim novembro 2016
Boletim novembro 2016Boletim novembro 2016
Boletim novembro 2016
 
Boletim novembro 2016 tm
Boletim novembro 2016   tmBoletim novembro 2016   tm
Boletim novembro 2016 tm
 

Similar to 164 1 (1)

Welcome to International Journal of Engineering Research and Development (IJERD)
Welcome to International Journal of Engineering Research and Development (IJERD)Welcome to International Journal of Engineering Research and Development (IJERD)
Welcome to International Journal of Engineering Research and Development (IJERD)IJERD Editor
 
physical and mechcanical properties of dental materials..ppt
physical and mechcanical properties of dental materials..pptphysical and mechcanical properties of dental materials..ppt
physical and mechcanical properties of dental materials..pptmanjulikatyagi
 
Strain life approach
Strain life approachStrain life approach
Strain life approachRudresh M
 
Test Rig of Free End Torsion Effect on Linear Strain
Test Rig of Free End Torsion Effect on Linear StrainTest Rig of Free End Torsion Effect on Linear Strain
Test Rig of Free End Torsion Effect on Linear Straintheijes
 
12-2-Publication-Experimental Analysis of Explosive Forming
12-2-Publication-Experimental Analysis of Explosive Forming12-2-Publication-Experimental Analysis of Explosive Forming
12-2-Publication-Experimental Analysis of Explosive FormingSaeed Jabalamelian
 
Failure Mechanism In Ductile & Brittle Material
Failure Mechanism In Ductile & Brittle MaterialFailure Mechanism In Ductile & Brittle Material
Failure Mechanism In Ductile & Brittle Materialshaikhsaif
 
Material (Failure Diagnosis)
Material (Failure Diagnosis)Material (Failure Diagnosis)
Material (Failure Diagnosis)Ahmed Ehab
 
Lec 2 stress strain diagram (lec 2)
Lec 2 stress strain diagram (lec 2)Lec 2 stress strain diagram (lec 2)
Lec 2 stress strain diagram (lec 2)Abdul Rehman Memon
 
BASIC MECHANICAL WORKING PROCESSES /METAL FORMING
BASIC MECHANICAL WORKING PROCESSES /METAL FORMINGBASIC MECHANICAL WORKING PROCESSES /METAL FORMING
BASIC MECHANICAL WORKING PROCESSES /METAL FORMINGMukuldev Khunte
 
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...IRJET Journal
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...ijeljournal
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...ijeljournal
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...ijeljournal
 

Similar to 164 1 (1) (20)

L1303059097
L1303059097L1303059097
L1303059097
 
Welcome to International Journal of Engineering Research and Development (IJERD)
Welcome to International Journal of Engineering Research and Development (IJERD)Welcome to International Journal of Engineering Research and Development (IJERD)
Welcome to International Journal of Engineering Research and Development (IJERD)
 
Engg mat
Engg mat Engg mat
Engg mat
 
Research Paper on Nacre
Research Paper on NacreResearch Paper on Nacre
Research Paper on Nacre
 
MATERIALS-ENGG-UNIT- 3.pdf
MATERIALS-ENGG-UNIT- 3.pdfMATERIALS-ENGG-UNIT- 3.pdf
MATERIALS-ENGG-UNIT- 3.pdf
 
physical and mechcanical properties of dental materials..ppt
physical and mechcanical properties of dental materials..pptphysical and mechcanical properties of dental materials..ppt
physical and mechcanical properties of dental materials..ppt
 
Structures and Materials- Section 4 Behaviour of Materials
Structures and Materials- Section 4 Behaviour of MaterialsStructures and Materials- Section 4 Behaviour of Materials
Structures and Materials- Section 4 Behaviour of Materials
 
Strain life approach
Strain life approachStrain life approach
Strain life approach
 
Test Rig of Free End Torsion Effect on Linear Strain
Test Rig of Free End Torsion Effect on Linear StrainTest Rig of Free End Torsion Effect on Linear Strain
Test Rig of Free End Torsion Effect on Linear Strain
 
12-2-Publication-Experimental Analysis of Explosive Forming
12-2-Publication-Experimental Analysis of Explosive Forming12-2-Publication-Experimental Analysis of Explosive Forming
12-2-Publication-Experimental Analysis of Explosive Forming
 
Failure Mechanism In Ductile & Brittle Material
Failure Mechanism In Ductile & Brittle MaterialFailure Mechanism In Ductile & Brittle Material
Failure Mechanism In Ductile & Brittle Material
 
Material (Failure Diagnosis)
Material (Failure Diagnosis)Material (Failure Diagnosis)
Material (Failure Diagnosis)
 
Lec 2 stress strain diagram (lec 2)
Lec 2 stress strain diagram (lec 2)Lec 2 stress strain diagram (lec 2)
Lec 2 stress strain diagram (lec 2)
 
Ch7_mechanical_properties_1.ppt
Ch7_mechanical_properties_1.pptCh7_mechanical_properties_1.ppt
Ch7_mechanical_properties_1.ppt
 
BASIC MECHANICAL WORKING PROCESSES /METAL FORMING
BASIC MECHANICAL WORKING PROCESSES /METAL FORMINGBASIC MECHANICAL WORKING PROCESSES /METAL FORMING
BASIC MECHANICAL WORKING PROCESSES /METAL FORMING
 
F012213639
F012213639F012213639
F012213639
 
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...
IRJET- Study of Cold-Formed Steel Flexural Member Under Monotonic and Reverse...
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
 
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
Anisotropy of Coercive Force of Single Crystals and Sheets of Silicon Iron wi...
 

Recently uploaded

Study on Air-Water & Water-Water Heat Exchange in a Finned Tube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned Tube ExchangerStudy on Air-Water & Water-Water Heat Exchange in a Finned Tube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned Tube ExchangerAnamika Sarkar
 
Application of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptxApplication of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptx959SahilShah
 
Introduction to Machine Learning Unit-3 for II MECH
Introduction to Machine Learning Unit-3 for II MECHIntroduction to Machine Learning Unit-3 for II MECH
Introduction to Machine Learning Unit-3 for II MECHC Sai Kiran
 
Call Girls Delhi {Jodhpur} 9711199012 high profile service
Call Girls Delhi {Jodhpur} 9711199012 high profile serviceCall Girls Delhi {Jodhpur} 9711199012 high profile service
Call Girls Delhi {Jodhpur} 9711199012 high profile servicerehmti665
 
What are the advantages and disadvantages of membrane structures.pptx
What are the advantages and disadvantages of membrane structures.pptxWhat are the advantages and disadvantages of membrane structures.pptx
What are the advantages and disadvantages of membrane structures.pptxwendy cai
 
Effects of rheological properties on mixing
Effects of rheological properties on mixingEffects of rheological properties on mixing
Effects of rheological properties on mixingviprabot1
 
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxDecoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxJoão Esperancinha
 
Sachpazis Costas: Geotechnical Engineering: A student's Perspective Introduction
Sachpazis Costas: Geotechnical Engineering: A student's Perspective IntroductionSachpazis Costas: Geotechnical Engineering: A student's Perspective Introduction
Sachpazis Costas: Geotechnical Engineering: A student's Perspective IntroductionDr.Costas Sachpazis
 
Past, Present and Future of Generative AI
Past, Present and Future of Generative AIPast, Present and Future of Generative AI
Past, Present and Future of Generative AIabhishek36461
 
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfCCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfAsst.prof M.Gokilavani
 
main PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidmain PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidNikhilNagaraju
 
Concrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxConcrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxKartikeyaDwivedi3
 
Risk Assessment For Installation of Drainage Pipes.pdf
Risk Assessment For Installation of Drainage Pipes.pdfRisk Assessment For Installation of Drainage Pipes.pdf
Risk Assessment For Installation of Drainage Pipes.pdfROCENODodongVILLACER
 
Arduino_CSE ece ppt for working and principal of arduino.ppt
Arduino_CSE ece ppt for working and principal of arduino.pptArduino_CSE ece ppt for working and principal of arduino.ppt
Arduino_CSE ece ppt for working and principal of arduino.pptSAURABHKUMAR892774
 
Oxy acetylene welding presentation note.
Oxy acetylene welding presentation note.Oxy acetylene welding presentation note.
Oxy acetylene welding presentation note.eptoze12
 

Recently uploaded (20)

Study on Air-Water & Water-Water Heat Exchange in a Finned Tube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned Tube ExchangerStudy on Air-Water & Water-Water Heat Exchange in a Finned Tube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned Tube Exchanger
 
Application of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptxApplication of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptx
 
Introduction to Machine Learning Unit-3 for II MECH
Introduction to Machine Learning Unit-3 for II MECHIntroduction to Machine Learning Unit-3 for II MECH
Introduction to Machine Learning Unit-3 for II MECH
 
POWER SYSTEMS-1 Complete notes examples
POWER SYSTEMS-1 Complete notes  examplesPOWER SYSTEMS-1 Complete notes  examples
POWER SYSTEMS-1 Complete notes examples
 
Design and analysis of solar grass cutter.pdf
Design and analysis of solar grass cutter.pdfDesign and analysis of solar grass cutter.pdf
Design and analysis of solar grass cutter.pdf
 
Call Us -/9953056974- Call Girls In Vikaspuri-/- Delhi NCR
Call Us -/9953056974- Call Girls In Vikaspuri-/- Delhi NCRCall Us -/9953056974- Call Girls In Vikaspuri-/- Delhi NCR
Call Us -/9953056974- Call Girls In Vikaspuri-/- Delhi NCR
 
Call Girls Delhi {Jodhpur} 9711199012 high profile service
Call Girls Delhi {Jodhpur} 9711199012 high profile serviceCall Girls Delhi {Jodhpur} 9711199012 high profile service
Call Girls Delhi {Jodhpur} 9711199012 high profile service
 
What are the advantages and disadvantages of membrane structures.pptx
What are the advantages and disadvantages of membrane structures.pptxWhat are the advantages and disadvantages of membrane structures.pptx
What are the advantages and disadvantages of membrane structures.pptx
 
Effects of rheological properties on mixing
Effects of rheological properties on mixingEffects of rheological properties on mixing
Effects of rheological properties on mixing
 
young call girls in Green Park🔝 9953056974 🔝 escort Service
young call girls in Green Park🔝 9953056974 🔝 escort Serviceyoung call girls in Green Park🔝 9953056974 🔝 escort Service
young call girls in Green Park🔝 9953056974 🔝 escort Service
 
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxDecoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
 
Sachpazis Costas: Geotechnical Engineering: A student's Perspective Introduction
Sachpazis Costas: Geotechnical Engineering: A student's Perspective IntroductionSachpazis Costas: Geotechnical Engineering: A student's Perspective Introduction
Sachpazis Costas: Geotechnical Engineering: A student's Perspective Introduction
 
Past, Present and Future of Generative AI
Past, Present and Future of Generative AIPast, Present and Future of Generative AI
Past, Present and Future of Generative AI
 
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfCCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
 
main PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidmain PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfid
 
Concrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxConcrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptx
 
Risk Assessment For Installation of Drainage Pipes.pdf
Risk Assessment For Installation of Drainage Pipes.pdfRisk Assessment For Installation of Drainage Pipes.pdf
Risk Assessment For Installation of Drainage Pipes.pdf
 
Arduino_CSE ece ppt for working and principal of arduino.ppt
Arduino_CSE ece ppt for working and principal of arduino.pptArduino_CSE ece ppt for working and principal of arduino.ppt
Arduino_CSE ece ppt for working and principal of arduino.ppt
 
Oxy acetylene welding presentation note.
Oxy acetylene welding presentation note.Oxy acetylene welding presentation note.
Oxy acetylene welding presentation note.
 
young call girls in Rajiv Chowk🔝 9953056974 🔝 Delhi escort Service
young call girls in Rajiv Chowk🔝 9953056974 🔝 Delhi escort Serviceyoung call girls in Rajiv Chowk🔝 9953056974 🔝 Delhi escort Service
young call girls in Rajiv Chowk🔝 9953056974 🔝 Delhi escort Service
 

164 1 (1)

  • 1. Jixi Zhang Yanyao Jiang e-mail: yjiang@unr.edu Department of Mechanical Engineering (312), University of Nevada, Reno, NV 89557 A Study of Inhomogeneous Plastic Deformation of 1045 Steel An experimental study was conducted on the inhomogeneous plastic deformation of 1045 steel subjected to monotonic tension and cyclic tension-compression. Small strain gages were used to characterize the local deformation and transmission electron microscopy (TEM) was used to study the microstructures associated with the observed deformation phenomenon. Under monotonic tension, the strain of the Lu¨ders front was lower than the full Lu¨ders strain. The local strains were inhomogeneous even at the work-hardening stage. Under stress-controlled cyclic loading with stress amplitudes below the lower yield stress, cyclic deformation consisted of an incubation stage, a significantly inhomogeneous cyclic softening stage, and a saturation stage. Inhomogeneous cyclic plasticity persisted at the saturation stage. A monotonic tension preload can eliminate the incubation stage in the subsequent cyclic loading. Under asymmetric cyclic loading with a mean stress, the cyclic plastic deformation was accompanied by noticeable inhomogeneous ratcheting deformation. TEM was used to analyze the distribution and evolution of the dislocation structures at different locations of the specimen. With increasing loading cycles, the dis- location substructures evolved in a sequence of loose tangles, thick veins, long walls, elongated cells, and equiaxial cells. Based upon the mechanical experiments and obser- vations of dislocation arrangements, the mechanisms governing inhomogeneous cyclic plastic deformation were discussed. ͓DOI: 10.1115/1.1647125͔ Keywords: Dislocation arrangement, inhomogeneous cyclic plastic deformation, Lu¨ders band, SAE 1045 steel 1 Introduction Inhomogeneous deformation associated with Lu¨ders band propagation has been extensively investigated ͓1͔. During the monotonic tension of an annealed mild steel, plastic deformation is initiated in a local region indicated by a negative slope in the stress-strain curve and propagates at a decreased stress level known as the lower yield stress. A distinct plateau appears in the stress-strain curve and the local deformation within the gage sec- tion of the specimen is inhomogeneous, characterized with the propagation of the Lu¨ders bands. In the plastically deformed re- gions, the strain has a constant value ͑Lu¨ders strain͒ while the deformation is elastic in the remaining area of the gage section. After the Lu¨ders bands cover the whole gage section, deformation is essentially homogeneous before necking develops ͓1͔. For the materials exhibiting Lu¨ders band phenomenon under monotonic tension, some interesting mechanical behaviors may occur under cyclic loading. It is generally found that a carbon steel subjected to strain-controlled cyclic loading experiences a sudden drop in the stress amplitude response after a certain num- ber of loading cycles ͓2͔. After an incubation phase of almost purely elastic deformation, significant cyclic softening is observed for carbon steels under fully reversed stress-controlled cyclic loading with a stress amplitude lower than the lower yield stress ͓3–14͔. The larger the stress amplitude, the shorter the incubation stage and the larger the saturated plastic strain amplitude ͓3͔. A similar phenomenon was observed in normalized as well as quenched and tempered low alloyed steels ͓15͔. Inhomogeneous cyclic plastic deformation of carbon and al- loyed steels has been investigated using photoelasticity ͓4,15͔, microhardness ͓15͔, and strain gages ͓3,15͔. By using three small strain gages glued on the gage section of a solid specimen, Eifler and Macherauch ͓15͔ reported that an SAE 4140 steel experienced inhomogeneous cyclic softening when subjected to a fully re- versed stress-controlled loading. Uniform deformation was re- ported to occur after a finite number of loading cycles. By using ten small strain gages distributed along the specimen of a normal- ized 1045 steel, quantitative measurement of the distribution of plastic deformation during cyclic tension-compression loading was investigated by Jiang ͓3͔. It was observed that the cyclic plastic deformation was initiated in local areas of the specimen and propagated through the gage section of the specimen with increasing number of cycles. Inhomogeneous plastic strain devel- oped during the cyclic softening and persisted at the saturation stage. The inhomogeneous cyclic deformation was dependent on the loading magnitude and evolved with continued cyclic loading. Different local mean strains developed even though the stress- controlled cyclic loading was symmetric. Under asymmetric stress-controlled cyclic loading with a mean stress, inhomoge- neous ratcheting deformation occurred in the direction of mean stress after a period of incubation and the inhomogeneity persisted at the saturation stage ͓3͔. For mild carbon steels, the dislocation structures in ferrite grains after cyclic loading have been studied ͓9,12,16–19͔. Most researchers have focused on the observation of dislocation struc- tures at the saturation state, usually, between 30% to 100% of the total fatigue life of the material. At room temperature, the dislo- cation arrangement in the surface layer differs considerably from that of the interior of the specimen. On the surface, persistent slip bands are usually observed independent of stress amplitude. In the interior of the specimen, dislocations arrange themselves into cell structures when the stress amplitude is high, or into bands when the stress amplitude is low ͓9,12,16,17͔. Within the temperature range of dynamic strain aging, dislocation bundles and broad walls prevail even though the stress amplitude is high; while both below and above the temperature range, the dislocations arrange themselves into cells ͓18,19͔. The current work was a continued effort to explore the inhomo- geneous plastic deformation by adopting the experimental meth- ods used earlier ͓3͔. The localized plastic deformation of 1045 steel subjected to monotonic tension and cyclic tension- compression with and without a mean stress was further investi- Contributed by the Materials Division for publication in the JOURNAL OF ENGI- NEERING MATERIALS AND TECHNOLOGY. Manuscript received by the Materials Division December 2, 2002; revision received November 5, 2003. Associate Editor: W. Soboyejo. 164 Õ Vol. 126, APRIL 2004 Copyright © 2004 by ASME Transactions of the ASME Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 2. gated. The influence of monotonic tension preload on cyclic plas- tic deformation and the persistence of inhomogeneous plastic deformation during multiple-step cyclic loading were studied. At- tempts were made to study the dislocation structures and the evo- lution of dislocations during inhomogeneous deformation by us- ing transmission electron microscopy ͑TEM͒. The mechanisms involved in the initiation and propagation of inhomogeneous cy- clic plastic deformation were discussed. 2 Experiments The as-received SAE 1045 steel was in a hot rolled state with the following chemical compositions: 0.46 wt.% C, 0.27 wt.% Si, 0.70 wt.% Mn, 0.019 wt.% P, 0.027 wt.% S, with balance of Fe. Cylindrical specimens were machined after normalizing the mate- rial at 815°C for 8 hours. The specimens were identical in material and heat treatment to those used in a previous study ͓3͔. A typical microstructure after normalization is shown in Fig. 1. The volume fraction of pearlite was approximately 55% and the mean ferrite grain size was 10 ␮m. The uniform gage section of the specimen had a diameter of 12 mm and a gage length of 25.4 mm. The gauge length surface was machined followed by polishing with fine sand papers with grit size 600. To measure local strains, a Micro-Measurements Group EA-06- 062MD-120 10-element strip gage was bonded on the surface within the gage section of the specimen. The strip strain gage length was 20 mm. Each gage element had a resistance of 120 ⍀ and the gage factor was 2.01. Each strain gage had an area of 1.57ϫ1.57 mm, with a spacing between strain gages in the strip of 2.1 mm. The row of strain gages was aligned with the specimen axis identical to that used in a previous study ͓3͔. A 25.4 mm gage length extensometer was attached to the specimen in the gage section to measure the average deformation. Experiments were conducted at room temperature in air. Cyclic testing was conducted at a frequency of 0.25 Hz. During an ex- periment, the load, extensometer displacement, and the outputs of all the 10 strain gages were recorded simultaneously. Two hundred data points were recorded for each variable during a loading cycle. To distinguish the deformation measured by the extensom- eter and the strain gages, the strain obtained from the extensom- eter is referred to as ‘‘extensometer strain’’ while the strain gage measurements are denoted as ‘‘local strains’’. Thin foil TEM samples were prepared with the material cut from the designated areas in the testing specimen using a low speed diamond saw. The normal direction of the thin foils was parallel to the specimen axis. The thin foils were mechanically ground on both sides with fine sand papers down to a thickness of 100 ␮m. Discs of 3 mm diameter were punched from these foils. The discs were then electropolished using a twin jet technique in a solution of 10 vol.% perchloric acid mixed with 90 vol.% eth- anol at Ϫ30 °C until perforation. The samples were examined with a JEOL 200CX TEM operated at 200 KV. 3 Experimental Results 3.1 Lu¨ders Bands Under Monotonic Loading. Monotonic tension was conducted under stroke ͑displacement͒-controlled loading mode. The extension rate was 0.002 mm/s that corre- sponded to an approximately 5ϫ10Ϫ5 /s strain rate. The results are shown in Fig. 2. The upper yield stress is 420 MPa and the lower yield stress is 400 MPa. The distinct plateau in the stress- extensometer strain curve corresponds to the formation and propa- gation of Lu¨ders bands. The full Lu¨ders strain ͑the length of the plateau͒ is 0.98%. The dots and numbers in the stress- extensometer strain curve ͑Fig. 2͑a͒͒ denote the moment that the corresponding strain gage on the specimen showed the onset of plastic deformation. In other words, a dot represents the specific value of the extensometer strain at which the Lu¨ders front reached the area covered by the numbered strain gage. The onset of plastic deformation of each strain gage is indicated by an abrupt increase in local strain, as shown in Fig. 2͑b͒. The area under Gage 10 was the last area that experienced plastic deformation. The particular moment did not correspond to the end of the plateau in the stress- strain curve ͑Fig. 2͑a͒͒. Two factors are responsible for this dis- crepancy. The extensometer gage length ͑25.4 mm͒ was longer than the strip strain gage length ͑20 mm͒. More importantly, the strain at the Lu¨ders front was significantly smaller than the full Lu¨ders strain. Detailed local strains shown in Fig. 2͑b͒ can provide a better insight of the Lu¨ders band propagation. Both local strains and extensometer strain are shown with respect to time. A number shown on the side of each curve denotes a specific strain gage. The strain gages in the strip were numbered starting from the top of the gage section. After the extensometer strain reached 0.002, which corresponded to the upper yield stress, the area covered by Gage 2 and Gage 3 started to deform plastically. The process continued with the plastic deformation occurring in the areas cov- ered by Gages 4, 5, 6, 7, 8, 9, and 10. Except Gage 1, all the other gages displayed a certain pattern. Among the ten strain gages, eight gages ͑Gage 3ϳ10͒ experienced the abrupt deformation in Fig. 1 Microstructure of SAE 1045 steel after normalization Fig. 2 Monotonic tension behavior of 1045 steel: „a… mono- tonic stress-extensometer strain curve; and „b… variations of local strains Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 165 Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 3. such a way that the end of the strain burst was followed by the start of the strain burst of the neighboring strain gage ͑Fig. 2͑b͒͒. Considering the finite length of the strain gage, this observation indicates that the value of the burst strain is approximately 0.66%. Since the strain burst was followed by strain hardening in the subsequent loading for a given location, a simple mathematic speculation can lead to the conclusion that the ‘‘real’’ strain at the Lu¨ders front should be a little smaller in value than that measured using a small but finite length strain gage. A vertical line in Fig. 2͑b͒ denotes the end of the plateau in the stress-extensometer strain curve. A common conclusion from early research is that the end of the plateau is the starting point of homogeneous deformation in the gage section ͓1͔. However, the results shown in Fig. 2͑b͒ clearly indicate that at the end of the plateau, the local deformation was still inhomogeneous. The inho- mogeneous deformation persisted in the work-hardening zone. 3.2 Localized Cyclic Plastic Deformation. A fully re- versed stress-controlled tension-compression experiment was con- ducted for 1550 cycles and the results are summarized in Fig. 3. The stress amplitude was 320 MPa which was less than the lower yield stress ͑400 MPa͒ of the material. The variations of local strain amplitudes and mean strains with the number of loading cycles were used to characterize the cyclic strain history. The cyclic deformation process consisted of three stages: an incuba- tion stage between 1ϳ230 cycles, a propagation stage between 230ϳ750 cycles, and a saturation stage after 750 cycles. During the incubation stage, the material displayed almost purely elastic deformation. After about 230 cycles, cyclic plastic deformation was initiated in the area covered by Gage 2 ͑upper part of the gage section͒ and propagated gradually into the two opposite directions with increasing number of loading cycles. The shaded bars in- serted in Fig. 3͑a͒ illustrate the propagation of the local plastic deformation. The length of a bar represents the gage length cov- ered by the strain gage strip ͑20 mm͒ and the shaded area denotes the plastically deformed region. A threshold of 0.02% plastic strain amplitude was used to define the onset of cyclic plastic deformation. The local deformation was significantly inhomoge- neous during the propagation stage. Inhomogeneous and nonzero local mean strains developed simultaneously although symmetric cyclic stress was applied. After approximately 750 loading cycles, the strain amplitude and mean strains became stabilized and the whole gage section experienced cyclic plastic deformation. However, the stabilized strain amplitudes and mean strains within the gage section were not uniform ͑Fig. 3͑b͒͒. At Gage 2, where cyclic plastic deforma- tion occurred first, the strain amplitude was the largest while the mean strain was negative. At Gage 10, where cyclic plastic defor- mation occurred last, the strain amplitude was the smallest while the mean strain was positive. The non-uniform strains persisted during subsequent cycling. The influence of stress amplitude and mean stress on incuba- tion, propagation, and saturation strain amplitude is listed in Table 1. A larger stress amplitude leads to a shorter incubation stage, a shorter propagation stage, and a larger saturation strain amplitude. A tensile mean stress slightly shortens the incubation period but has no significant influence on the saturation strain amplitude. However, a tensile mean stress reduces the propagation period greatly. These results are consistent with those reported previously ͓3–8͔. A two-step experiment was designed to examine the influence of the monotonic tension preload on cyclic plastic deformation. Monotonic tension was terminated when the extensometer strain reached 0.5%. After the monotonic loading, the Lu¨ders bands had propagated over a half of the gage section covering Gage 1 to Gage 6 ͑Fig. 4͑a͒͒. The rest of the area covering Gage 7 to Gage 10 remained plastically undeformed. Following the monotonic preload, a fully reversed stress- controlled cyclic loading with a stress amplitude of 320 MPa was applied. The magnitudes of local strains in the cyclic loading are shown in Figs. 4͑b͒ and ͑c͒. One noticeable observation is the elimination of the incubation period due to the monotonic preload. In the area that had been plastically deformed in the monotonic preload, the strain amplitude decreased slightly to the saturation values. In the area that had not been plastically deformed in the monotonic loading, incubation stage disappeared. The propagation of cyclic plastic deformation occurred immediately upon the ap- plication of the cyclic loading and the strain amplitudes of Gages 7, 8, and 9 increased gradually to the saturation values. The propa- gation stage was noticeably shortened. The saturation strain am- plitudes were nearly identical to those shown in Fig. 3, knowing that the cyclic load magnitudes for the two cases were identical. Results shown in Fig. 4͑c͒ reveal that the local mean strains were scattered and distributed irregularly. A three-step stress-controlled cyclic tension-compression ex- periment was used to examine the influence of prior cyclic plas- ticity history on further cyclic deformation at a different mean stress. The stress amplitude was 300 MPa for all the three loading steps and the mean stresses were 100 MPa, 0, and Ϫ100 MPa in Step 1, Step 2, and Step 3, respectively. The numbers of loading cycles performed in Step 1, Step 2, and Step 3 were 920, 1250, and 1250, respectively. The results are summarized in Fig. 5 and Table 2. Cyclic plasticity in Step 1 eliminated the incubation and propa- gation stages in Step 2 and Step 3. In each loading step, the strain amplitudes do not change significantly, but the mean strain in- Fig. 3 Cyclic deformation of 1045 steel under fully reversed stress-controlled uniaxial loading: „a… variations of local strain amplitudes and propagation of plastic zone; and „b… variations of local mean strains Table 1 Influence of stress amplitude and mean stress on cy- clic plastic deformation ⌬␴/2 ͑MPa͒ ␴m ͑MPa) Ni ͑Cycles) Np ͑Cycles) ⌬␧/2 ͑%͒ 350 0 12 48 0.35 320 0 230 470 0.25 270 0 6000 8000 0.15 320 80 160 ϳ5 0.25 300 100 240 5 0.23 166 Õ Vol. 126, APRIL 2004 Transactions of the ASME Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 4. creased gradually in the direction of mean stress ͑ratcheting͒. The local mean strains were non-uniform. The heterogeneity persisted and increased with the loading steps. It was reported ͓7,20͔ that under multiple-step loading, materials exhibited a strong memory of the previous loading history, and such memory had a great influence on the subsequent ratcheting. Also shown in Figs. 3 and 4 are the average local strains and the extensometer strains. The average local strain was the average of the strain values taken from the 10 strain gages. One purpose to compare the two values was to monitor the possible breakage or debonding of strain gages during an experiment. The small differ- ence between the average local strain value and the extensometer measurement was mainly due to the difference between the exten- someter gage length ͑25.4 mm͒ and the length of the strain strip ͑20 mm͒, knowing that the deformation within the gage section was non-uniform. 3.3 Dislocation Substructures. Under fully reversed stress- controlled tension-compression loading with a stress amplitude of 320 MPa, four companion specimens were tested. The experi- ments were terminated at different cycles and dislocation sub- structures at different strain gage sites were examined. The loca- tions where the TEM samples were taken and the number of loading cycles tested are indicated in Fig. 3͑a͒. The loading cycles corresponded to the incubation, propagation, and saturation stages. During the incubation stage, the dislocation substructure had no obvious change as compared to that of the annealed condition. A typical dislocation arrangement is shown in Fig. 6 for a sample taken from the specimen that has been loaded for 200 loading cycles. The dislocation density in ferrite was low. Individual dis- locations could be identified clearly. There was no detectable in- dication of plastic deformation in the ferrite grains. Fig. 4 Influence of monotonic tension preload on cyclic defor- mation: „a… local tensile strains under monotonic tension pre- load; „b… variations of local strain amplitudes with loading cycles in subsequent cyclic loading; and „c… variations of local mean strains with loading cycles in subsequent cyclic loading Fig. 5 Cyclic deformation of 1045 steel under three-step stress-controlled cyclic loading: „a… variations of strain ampli- tudes; and „b… variations of mean strains Table 2 Influence of mean stress and strain history on ratch- eting deformation Step ␴m ͑M Pa) Ni ͑Cycles) Np ͑Cycles) ⌬␧/2 ͑%͒ ␧m (%) 1 100 240 5 0.23 1.4ϳ1.6 2 0 0 0 0.23 0.5ϳ0.85 3 Ϫ100 0 0 0.2 Ϫ0.58ϳϪ1.2 Fig. 6 Typical dislocation arrangement during the incubation stage Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 167 Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 5. Figure 7 shows the typical dislocation arrangements during the propagation stage. The experiment was terminated after 420 cycles, which was within the stage of cyclic plastic propagation ͑Fig. 3͑a͒͒. The local strains were significantly inhomogeneous and different dislocation substructures were observed at different strain gage sites ͑see Fig. 3͑a͒ and Fig. 7͒. Since ferrite grains in the material were randomly oriented, the resolved shear stress amplitudes acting on the primary slip systems of individual ferrite grains were different. In addition, dislocation arrangements in in- dividual ferrite grains differed even at the same strain gage site. Here, the representative dislocation arrangements in the most se- riously deformed ferrite grains are presented. On the area covered by Gage 10 where the plastic deformation was the smallest as compared to the rest of the area of the gage section, only a few ferrite grains were plastically deformed. Shown in Fig. 7͑a͒ is a typical dislocation configuration in plastically deformed ferrite grains. Loose dislocation tangles indicated the initiation of plastic deformation. These dislocation tangles were distributed randomly within the ferrite grains, indicating that the locations for the ini- tiation of plastic deformation were randomly distributed within the ferrite grains. Figure 7͑b͒ shows the dislocation configuration on the area covered by Gage 6 where the strain amplitude was medium. Dislocation density increased sharply by dislocation multiplication and thick dislocation multipole veins distributed randomly within the ferrite grains. At Gage 2, plastic deformation was the largest over the gage section. Most ferrite grains were plastically deformed. A typical dislocation arrangement in the ferrite grains is shown in Fig. 7͑c͒. Further plastic deformation resulted in an increase in the diameter and dislocation density of the veins. The process reached a point where local instabilities in the veins occurred due to dislocation interaction and annihilation. This was followed by the evolution of dislocation substructures into thinner yet denser dislocation walls. The dislocation density between the walls was very low. Although the build-up of macroscopic strain was complete at the end of the propagation stage, continued cyclic loading led to a further development of dislocation structures. The dislocation configuration at the saturation state at a cycle number of 1550 is shown in Fig. 8. In general, long and dense walls, elongated cells, and equiaxial cells were observed. There were no obvious quali- tative differences among dislocation arrangements for the material within the gage length. At the stage of cyclic plastic deformation propagation, the de- formation process can be accomplished by single slips and the influence of the grain/phase boundaries is not significant. How- ever, in the subsequent transition to the cell structures, multiple slip process is a necessity. At this point, the grain/phase bound- aries play an important role. The plastic deformation in grain/ phase boundaries requires more activated slip systems due to the constraints introduced. TEM observations confirmed that the mul- tiple slip systems were always activated at first at the grain/phase boundaries that resulted in the formation of the cell structures. A typical TEM micrograph at the saturation stage is shown in Fig. 9. Arrow A points to a grain boundary and Arrows B and C indicate phase boundaries. With continued cyclic loading, the dislocation cells were developed further into the central zone of the ferrite grains. 4 Discussions Strain gages provide a practical and accurate method to mea- sure the local deformation. The results shown in Fig. 2͑b͒ are different from those of previous research on Lu¨ders bands in sev- Fig. 7 Typical dislocation arrangements during the propaga- tion stage „at cycle 420…: „a… at Gage 10 „low local strain ampli- tude: 0.165%…; „b… at Gage 6 „medium local strain amplitude: 0.2%…; and „c… at Gage 2 „high local strain amplitude: 0.23%… Fig. 8 Typical dislocation arrangement at the saturation stage 168 Õ Vol. 126, APRIL 2004 Transactions of the ASME Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 6. eral aspects. It is generally asserted that during propagation of Lu¨ders bands, plastic strain in the plastically deformed zone is equal to the full Lu¨ders strain. Upon the start of work-hardening, the deformation is uniform. The current work reveals that inho- mogeneous deformation persists into the work-hardening stage. The Lu¨ders bands results reported in the current investigation are inconsistent with those of the previous studies. The testing material, the specimen geometry, and the techniques used to mea- sure the local strains may have contributed to the discrepancy. A thin and flat specimen was often used in the investigation of Lu¨d- ers bands ͓21–32͔. In the current investigation, specimens of a normalized 1045 steel with a circular cross section were tested. An obvious advantage in using a specimen with a flat surface is the convenience and suitability for surface observations. The pos- sible influence of the testing specimen geometry on the Lu¨ders band observations may require further investigation. Usually, sur- face scratches ͓21–23,33͔, surface grid ͓24,25͔, contrast interfer- ometer ͓22,23,26͔, stresscoat ͓34͔, electroplating of the specimen prior to testing ͓27͔, optical ‘‘To¨pler Schlieren’’ method ͓21,33͔, critical macro-illumination ͓28͔, gridreflection ͓26͔, clip- extensometer ͓29,35͔, high speed camera ͓30͔, and infrared cam- era ͓31͔ were used to observe the Lu¨ders bands and to identify the local strains. These methods do not provide an accurate quantita- tive measurement of the local strain. It is noted that by using four small strain gages bonded on the specimen, a similar phenomenon to that shown in Fig. 2͑b͒ was observed in an annealed aluminum alloy under monotonic tension ͓32͔. The formation and propagation of Lu¨ders bands in irons and carbon steels under monotonic tension are generally attributed to the strong interaction of interstitial atoms with dislocations, known as Cottrell atmospheres ͓1͔. In the Cottrell atmospheres, interstitial atoms segregate to dislocations and pin them in posi- tions to lower the lattice distortion energy. In a normalized 1045 steel, the yield stress of pearlite is much higher than that of ferrite ͓36–38͔. In the current investigation, the strain amplitude was low and plastic deformation took place mainly in the ferrite grains. The ferrite grains contain small amount of carbon and nitrogen atoms in solid solution and the Cottrell atmospheres play an im- portant role in plastic deformation. In monotonic tension, the abrupt increase of strain at the Lu¨ders front can be ascribed to the dislocations unpinned from the Cottrell atmospheres. Their mo- tion leads to an abrupt multiplication of new dislocations. Subse- quently, dislocations multiply further but slowly. Previous studies have confirmed that cyclic plasticity of low carbon steels can eliminate Lu¨ders bands phenomenon in a sub- sequent monotonic tension ͓10–14,39–41͔. This elimination oc- curs in the first half cycle for stress amplitude higher than the yield point. For stress amplitude below the yield point, the Lu¨ders strain decreases continuously with increasing number of cycles. The current investigation reveals that a monotonic tension preload eliminates the incubation stage and either shortens or completely eliminates the propagation stage of the cyclic plastic deformation in the subsequent cyclic loading. It is reasonable to infer from the observations that the formation and propagation of Lu¨ders bands under monotonic tension and the inhomogeneous cyclic plastic deformation phenomenon should be closely related in terms of mechanism. Klesnil and Luka´sˇ ͓10,11͔ used the Cottrell atmospheres to in- terpret successfully the mechanism of the cyclic softening of low carbon steels under stress-controlled cyclic loading with the stress amplitude being below the yield stress. A low carbon steel ͑0.07% C, 0.48% Mn, 0.3% Si, 0.018% P, 0.019% S͒ with a mean grain size of ferrite of 40 ␮m was used. The yield stress of the material was 278 MPa. Stress was cycled between 228 MPa and 250 MPa. It was noted that cyclic plasticity was initiated at the first loading cycle for the cases under consideration ͓10,11͔. There exist a few ferrite grains in the material where certain dislocations are less effectively pinned by interstitials and can move at a stress level below the yield stress. In the first half cycle, a small number of such dislocations in some isolated grains are unpinned. This pro- cess is repeated in each loading cycle followed. As a result, the number of grains with free dislocations and bulk plastic strain amplitude increase with increasing loading cycles. On the other hand, fatigue hardening process, namely the increase of disloca- tion density, and formation of dislocation structure occur in these grains that lead to a decrease in plastic strain amplitude. The su- perposition and interaction of these two processes result in the observed cyclic softening and hardening phenomenon. It is noticed that the microstructure and cyclic deformation be- havior of the 1045 steel used in the current investigation are dif- ferent from those of the low-carbon steel. In the current study, the size of the ferrite grains is much smaller and they are separated and constrained by the pearlite grains. The yield stress of the ferrite grains is much higher than that in the low carbon steel. For the 1045 steel under stress-controlled cyclic loading with stress amplitude much lower than the lower yield stress, the incubation stage is long and cannot be ignored. During the cyclic softening stage, the distribution of local strains is significantly inhomoge- neous. The local deformation depends not only on the number of the ferrite grains with free dislocations but also on the extent of plastic deformation of these ferrite grains. Therefore, the mecha- nism of cyclic plasticity of the 1045 steel should be different from that of the low-carbon steel. For the 1045 steel under stress-controlled cyclic loading with a stress amplitude much lower than the lower yield stress, deforma- tion is almost purely elastic during the incubation stage. The dis- location configuration is identical to that in the original normal- ized condition with no observable change in the dislocation density. Traditionally, phase/grain boundaries are viewed as the most possible sites of stress concentration where pre-yield micros- train may occur ͓42͔. However, during the incubation stage, the concentration and pile-up of dislocations at the phase/grain boundaries were rarely observed. As shown in Fig. 7, the loose dislocation tangles, indicators of the initiation of plastic deforma- tion, distribute randomly within the ferrite grains. Significant changes in dislocation density and configuration can be observed only during the propagation phase. During the saturation stage, dislocation cells are found to form at first at phase/grain bound- aries. The formation of the cells gradually propagates into the interior of the grains. The microscopic mechanism involved in the inhomogeneous cyclic plastic deformation can be discussed based on the experi- mental observations. In the incubation stage, the dislocations pinned by the Cottrell atmospheres relax gradually under cyclic stressing and become free and mobile dislocations. At the propa- gation stage, the movement of free dislocations leads to the mul- tiplication, interaction, and annihilation of dislocations. The dis- Fig. 9 Dislocation cells are formed at first at the grainÕphase boundary „at 1550th cycle in a saturation stage… Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 169 Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 7. location configurations evolve into dislocation tangles, veins, and dense walls. In the later phase of propagation and the early phase of saturation, multiple slip systems are activated at first near the phase/grain boundaries and then propagate into the interior of the ferrite grains. The dislocation arrangements eventually evolve into cell structures. The viewpoint is supported by the experimental results from the two-step loading experiment shown in Fig. 4. In the plastically deformed zone, the dislocations in the ferrite grains had been unpinned and multiplied sufficiently. As a result, the incubation and propagation stages were eliminated in the subsequent cyclic loading. In the area where deformation remained macroscopically elastic after the tension preload, the incubation stage disappeared in the second loading step. This suggests that during the propaga- tion process of Lu¨ders bands under the monotonic tension, the dislocations in the plastically undeformed zone have been un- pinned from the Cottrell atmospheres. However, these dislocations do not move or only make local short-ranged movement, and immediate generation of new dislocations has not yet taken place. The aforementioned discussion was concentrated on the inho- mogeneous cyclic plasticity, the associated dislocation substruc- tures, and possible mechanisms. However, the underlying mecha- nism for localized cyclic plasticity has not been fully explained. The mechanism governing the propagation of cyclic plastic defor- mation from one area to another in the specimen remains unclear. The mechanism operative in the localized monotonic plasticity associated with the formation of Lu¨ders bands in irons and carbon steels probably can provide some enlightenment. During monotonic tension of irons and carbon steels, Lu¨ders bands are believed to nucleate at points of high local stresses, such as fillets, precipitates, and grain boundaries ͓1͔. The propagation of Lu¨ders bands depends on factors such as crystal structure, grain size, shape of the sample, composition, and microstructure ͓43͔. The propagation of Lu¨ders bands in single crystals probably is engendered by the local constraints and stress concentrations set up between the deformed and undeformed regions. In a fine- grained mild steel, the edge of Lu¨ders bands appears sharp. It is a reasonable speculation that deformation is spreading grain by grain through the specimen. Dislocations in the yielding grain run up to the grain boundary, and form pile-up arrays of dislocations, whose presence increases the stress in the neighboring grain until a dislocation source there becomes unpinned and the grain yields. As the grain size increases, the edge of Lu¨ders band becomes diffuse. As pointed by Hall ͓1͔, ‘‘This effect arises approximately at the point where Hutchison’s curve ͓44͔ for the upper yield stress with respect to grain size intersects the lower yield stress. In other words, the stress differences are here so low that any small inhomogeneity in grain size will cause part of the band front to progress far in advance of the remainder.’’ The inhomogeneous cyclic plastic deformation has a similarity to the propagation of the Lu¨ders band. However, whether or not similar or identical mechanisms exist for the two phenomena re- quires further investigation. In addition, the effect of the stress state on the inhomogeneous cyclic plasticity is also a subject of future research. 5 Conclusions From the experimental observations on the inhomogeneous plastic deformation of 1045 steel, the following conclusions can be drawn: 1. Under monotonic tension, the burst strain of Lu¨ders front is much lower than the full Lu¨ders strain. The local deformation remains inhomogeneous even at the work-hardening stage after the termination of the Lu¨ders band propagation. 2. For stress-controlled tension-compression cyclic loading with the maximum stress lower than the lower yield stress of the material, cyclic plastic deformation is characterized by three stages: incubation, propagation, and saturation. The local strains are significantly inhomogeneous during the propagation stage and the inhomogeneity persists at the saturation stage. 3. The monotonic tension preload can eliminate or shorten the incubation and propagation stages of the cyclic plasticity in the subsequent cyclic loading. 4. Inhomogeneous cyclic plasticity persists under multiple-step loading. The inhomogeneity is evidenced mainly by the persistent difference in local mean strains. 5. During the incubation stage, the dislocation structures do not change significantly. With increasing loading cycles, the disloca- tion structures evolve in a sequence of loose tangles, thick veins, long walls, elongated cells, and equiaxial cells. 6. Under cyclic stressing, the dislocations pinned by the Cot- trell atmospheres in the ferrite grains are unpinned gradually and become free and mobile dislocations. The movement of free dis- locations leads to the multiplication, interaction, and annihilation of dislocations. Dislocation cells are formed at first at the grain boundaries with the activation of multiple slip systems followed by the cells propagation into the interior of the ferrite grains. Acknowledgment Financial support was provided by the National Science Foun- dation ͑CMS-9984857͒. TEM experiments were conducted at the National Center for Electron Microscopy at Lawrence Berkeley National Laboratory. The assistance of Drs. Eric Stach, Tamara Radetic, and Chengyu Song is greatly appreciated. Nomenclature ⌬␴/2ϭ stress amplitude ␴m ϭ mean stress R ϭ stress ratio ͑minimum stress over maximum stress͒ Ni ϭ number of loading cycle of the incubation stage Np ϭ number of loading cycle of the propagation stage ␧ ϭ extensometer strain ⌬␧/2 ϭ stabilized strain amplitude ␧m ϭ mean strain ␧L1 ϭ strain at the Lu¨ders front ␧L ϭ full Lu¨ders strain References ͓1͔ Hall, E. O., 1970, Yield Point Phenomena in Metals and Alloys, Plenum Press, New York. ͓2͔ Fatemi, A., and Stephens, R. I., 1989, ‘‘Cyclic Deformation of 1045 Steel Under In-Phase and 90° Out-of-Phase Axial-Torsional Loading Conditions,’’ in Multiaxial Fatigue, Analysis and Experiments, AE-14, G. E. Leese and D. Socie, eds., SAE International, pp. 139–147, Chap. 10. ͓3͔ Jiang, Y., 2001, ‘‘An Experimental Study of Inhomogeneous Cyclic Plastic Deformation,’’ ASME J. Eng. Mater. Technol., 123, pp. 274–280. ͓4͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1977, ‘‘Inhomogeneous Deformation Processes in the Incipient Crack-Free Fatigue Stage of Unalloyed Steels,’’ Arch. Eisenhuettenwes., 48, pp. 575–578. ͓5͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1978, ‘‘On the Influence of Mean Stress on the Fatigue Behavior of Unalloyed Steels,’’ Arch. Eisen- huettenwes., 49, pp. 31–36. ͓6͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1979, ‘‘Cyclic Induced Creep of a Plain Carbon Steel at Room Temperature,’’ Fatigue Eng. Mater. Struct., 1, pp. 287–295. ͓7͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1979, ‘‘Macroscopic Changes of Length as a Consequence of Changes of Mean Stress During Cyclic Tension-Compression Tests on CK45,’’ Arch. Eisenhuettenwes., 50, pp. 439–442. ͓8͔ Pilo, D., Reik, W., Mayr, P., and Macherauch, E., 1980, ‘‘Macroscopic Changes of Length Under Cyclic Load for Steel CK45 in Normalized and in Strained Condition,’’ Arch. Eisenhuettenwes., 51, pp. 155–157. ͓9͔ Pohl, K., Mayr, P., and Macherauch, E., 1981, ‘‘Cyclic Deformation Behavior of a Low Carbon Steel in the Temperature Range Between Room Temperature and 850 K,’’ Int. J. Fract., 17, pp. 221–233. ͓10͔ Klesnil, M., and Luka´sˇ, P., 1992, Fatigue of Metallic Materials, Elsevier, Amsterdam-Oxford-New York-Tokyo. ͓11͔ Klesnil, M., and Luka´sˇ, P., 1967, ‘‘Fatigue Softening and Hardening of An- nealed Low-Carbon Steel,’’ J. Iron Steel Inst., London, 205, pp. 746–749. ͓12͔ Klesnil, M., Holzmann, M., Luka´sˇ, P., and Rysˇ, P., 1965, ‘‘Some Aspects of Fatigue Process in Low-Carbon Steel,’’ J. Iron Steel Inst., London, 203, pp. 47–53. 170 Õ Vol. 126, APRIL 2004 Transactions of the ASME Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use
  • 8. ͓13͔ Abel, A., and Muir, H., 1975, ‘‘Fatigue Softening on Low-Carbon Steel,’’ Philos. Mag., 32, pp. 553–563. ͓14͔ Abel, A., and Muir, H., 1973, ‘‘The Nature of Microyielding,’’ Acta Metall., 21, pp. 99–105. ͓15͔ Eifler, D., and Macherauch, E., 1983, ‘‘Inhomogeneous Work-Softening Dur- ing Cyclic Loading of SAE 4140 in Different Heat Treated States,’’ Proc. 2nd Int. Sym. Defects, Fract. & Fat., G. C. Sih and J. W. Provan, eds., Can Mar- tinus Nijhoff Publ The Hague, Neth, pp. 171–182. ͓16͔ Klesnil, M., and Luka´sˇ, P., 1965, ‘‘Dislocation Arrangement in the Surface Layer of ␣-Iron Grains during Cyclic Loading,’’ J. Iron Steel Inst., London, 203, pp. 1043–1048. ͓17͔ Pohl, K., Mayr, P., and Macherauch, E., 1980, ‘‘Persistent Slip Band in the Interior of a Fatigued Low Carbon Steel,’’ Scr. Metall., 14, pp. 1167–1169. ͓18͔ Christ, H.-J., Wamukwamba, C. K., and Mughrabi, H., 1997, ‘‘The Effect of Mean Stress on the High-Temperature Fatigue Behavior of SAE 1045 Steel,’’ Mater. Sci. Eng., A, 234–236, pp. 382–385. ͓19͔ Weisse, M., Wamukwamba, C. K., Christ, H.-J., and Mughrabi, H., 1993, ‘‘The Cyclic Deformation and Fatigue Behavior of the Low Carbon Steel SAE 1045 in the Temperature Regime of Dynamic Strain Ageing,’’ Acta Metall. Mater., 41, pp. 2227–2233. ͓20͔ Jiang, Y., and Sehitoglu, H., 1994, ‘‘Multiaxial Cyclic Ratchetting Under Mul- tiple Step Loading,’’ Int. J. Plast., 10, pp. 849–870. ͓21͔ Hall, E. O., 1951, ‘‘The Deformation and Aging of Mild Steel: II. Character- istics of the Lu¨ders Deformation. III. Discussion of Results,’’ Proc. Phys. Soc. London, Sect. B, 64, pp. 742–753. ͓22͔ Iricibar, R., Mazza, J., and Cabo, A., 1975, ‘‘The Microscopic Strain Profile of a Propagating Lu¨ders Band Front in Mild Steel,’’ Scr. Metall., 9, pp. 1051– 1058. ͓23͔ Iricibar, R., Mazza, J., and Cabo, A., 1977, ‘‘On the Lu¨ders Band in Mild Steel-I,’’ Acta Metall., 25, pp. 1163–1168. ͓24͔ Prewo, K., Li, J. C. M., and Gensamer, M., 1972, ‘‘Lu¨ders Band Motion in Iron,’’ Metall. Trans., 3, pp. 2261–2269. ͓25͔ Lloyd, D. J., and Morris, L. R., 1977, ‘‘Lu¨ders Band Deformation in a Fine Grained Aluminum Alloy,’’ Acta Metall., 25, pp. 857–861. ͓26͔ Verel, D. J., and Sleeswyk, A. W., 1973, ‘‘Lu¨ders Band Propagation at Low Velocities,’’ Acta Metall., 21, pp. 1087–1098. ͓27͔ Liss, R. B., 1957, ‘‘Lu¨ders Bands,’’ Acta Metall., 5, pp. 341–342. ͓28͔ Boxall, T. D., and Hundy, B. B., 1955, ‘‘Photographing Stretcher-Strain Mark- ings With the Vickers Projection Microscope,’’ Metall. Trans., 51, pp. 52–54. ͓29͔ Iricibar, R., and Mazza, J., 1975, ‘‘Meaning of the Strain Profile of a Propa- gating Lu¨ders Band Front,’’ Scr. Metall., 9, pp. 1045–1050. ͓30͔ Miyazaki, S., and Fujita, H., 1979, ‘‘Dynamic Observation of the Process of Lu¨ders Band Formation in Polycrystalline Iron,’’ Trans. Jpn. Inst. Met., 20, pp. 603–608. ͓31͔ Louche, H., and Chrysochoos, A., 2001, ‘‘Thermal and Dissipative Effects Accompanying Lu¨ders Band Propagation,’’ Mater. Sci. Eng., A, 307, pp. 15– 22. ͓32͔ Onodera, R., Nonomura, M., and Aramaki, M., 2000, ‘‘Stress Drop, Lu¨ders Strain and Strain Rate During Serrated Flow,’’ J. Jpn. Inst. Met., 64, pp. 1162– 1171. ͓33͔ Sylwestrowicz, W., and Hall, E. O., 1951, ‘‘The Deformation and Aging of Mild Steel,’’ Proc. Phys. Soc. London, Sect. B, 64, pp. 495–502. ͓34͔ Fisher, J. C., and Rogers, H. C., 1956, ‘‘Propagation of Lu¨ders Bands in Steel Wires,’’ Acta Metall., 4, pp. 180–185. ͓35͔ Moon, D. W., 1971, ‘‘Strain Distribution Through a Propagating Lu¨ders Band Front,’’ Scr. Metall., 5, pp. 213–216. ͓36͔ Karlsson, B., and Linde´n, G., 1975, ‘‘Plastic Deformation of Ferrite-Pearlite Structures in Steel,’’ Mater. Sci. Eng., 17, pp. 209–219. ͓37͔ Karlsson, B., and Linde´n, G., 1975, ‘‘Plastic Deformation of Eutectoid Steel With Different Cementite Morphologies,’’ Mater. Sci. Eng., 17, pp. 153–164. ͓38͔ Karlsson, B., and Sundstrom, B. O., 1974, ‘‘Inhomogeneity in Plastic Defor- mation of Two-Phase Steels,’’ Mater. Sci. Eng., 16, pp. 161–168. ͓39͔ Ivanova, V. S., Terent’yev, V. F., and Poyda, V. G., 1970, ‘‘Features of the Built-up of Strain in Low-Carbon Steel Subjected to Cycles of Stress,’’ Phys. Met. Metallogr., 30, pp. 165–171. ͓40͔ Oates, G., and Wilson, D. V., 1964, ‘‘The Effects of Dislocation Locking and Strain Aging on the Fatigue Limit of Low-Carbon Steel,’’Acta Metall., 12, pp. 21–33. ͓41͔ Abel, A., and Muir, H., 1973, ‘‘The Effect of Cyclic Loading on Subsequent Yielding,’’ Acta Metall., 21, pp. 93–97. ͓42͔ Carrington, W. E., and McLean, D., 1965, ‘‘Slip Nuclei in Silicon-Iron,’’ Acta Metall., 13, pp. 493–499. ͓43͔ Ananathan, V. S., and Hall, E. O., 1991, ‘‘Macroscopic Aspects of Lu¨ders Band Deformation in Mild Steel,’’ Acta Metall. Mater., 39, pp. 3153–3160. ͓44͔ Hutchison, M. M., 1963, ‘‘The Temperature Dependence of the Yield Stress of Polycrystalline Iron,’’ Philos. Mag., 8, pp. 121–127. Journal of Engineering Materials and Technology APRIL 2004, Vol. 126 Õ 171 Downloaded From: http://materialstechnology.asmedigitalcollection.asme.org/ on 10/18/2016 Terms of Use: http://www.asme.org/about-asme/terms-of-use