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University:
SAGAR ALI
16 CH 56
Chemical Engineering
Mehran University Of
EngineeringandTechnology,Jamshoro
(MUET)
Industry: Colgate Palmolive PakistanLtd.
Department: Colgate Dental Cream(CDC)
pg. 2
Name:
Class Roll No:
Technology:
Background of Colgate Palmolive Pakistan
Acknowledgement
BeingastudentofChemicalEngineeringMehranUET,I’mgratefulto
ColgateStaffandEngineerswhogavemeawarmwelcomeandadetailed
orientation regarding Colgate-Palmolive Pakistan Limited. They have
beenverycooperativeandmotivatedinternstolearnhereasmuchas
they want.
I’malsowhole-heartedlybeholdentotheManagement,Supervisorsand
Workers,andspecialthankstoMr.SALEEM,whoencouraged,guidedand
supported us (the internes) throughout this internship program. We have
hadveryhonorabletimeworkinghere,inspectingtheirwaysofworking
things out. Me along with my fellows learnt very much incompetitive
environment of theindustry.
Ialso express my gratitude to Mr. FURQAN AHMED, Mr. SHEERAZ JUNEJO
and Mr.MUHAMMADUZAIRwhohavebeenverysupportiveatevery
step.Theyhavegiventheirprecioustimefromtheirdailytoughroutine
and guided me throughout this whole period of Internship.
• In 1984 started as a license manufacturer of Colgate-Palmolive
products in Pakistan
• In 1990 Colgate-Palmolive Inc. (USA) joined as a 30% equity partner
• Market leaders in Oral Care, Surface Care & Fabric Care categories
• 450 Distributors acrossPakistan
• ISO 9000 : 2000 Quality Management System
• KSE Top Companies Award for 2004, 2005, 2006
• Corporate Excellence Certificate 2001-02 & 2004
Contents
1. Introduction to Colgate Palmolive
2. Introduction to CDC Making
3. Process-Making-Packaging
4. Cleaning and Sanitization
1.Introduction to Colgate
Palmolive
Colgate-Palmolive(Pakistan)LimitedwasinitiallyincorporatedinPakistanonDecember5,
1977 as a public limited company with the name of National Detergents Limited. It started
its operations in Pakistan in 1977 as joint venture between Colgate Palmolive (USA) and
Lakson Group.
Colgate Palmolive is one of the largest ventures by the group. With assets of more than Rs.
400 million and a turnover of Rs. 1500 million, it has emerged as one of the largest
corporations in Pakistan.
Colgate–PalmolivePakistanLimited isaFast-MovingConsumerGoods(FMCG)industry.
FMCGaretheproductsthatarequitefrequentlyusedbytheconsumersintheirdaily
routine.
pg. 6
Company is equipped with two manufacturing plants across the country within,
1. KotriSindh 2. Sundhar Punjab.
The Companyis currently engaged in manufacturing of following
related products.
Categories of Products in CPPL:
a. Oralcare b.Personalcare c.SurfaceCare d. Fabriccare
OralCare:Oralcarereferstotakingcareofyourmouth;specifically,the
insideofyourmouth.Practicingoralcarekeepsyourgumsandteethhealthy,
whichisimportantnotonlyforyourmouth,butforoverallhealth.Thewell-
beingofyourmouthisknownasoralhealth.Oralcareincludestoothbrushing,
flossing,eatingwellandregularvisitstothedentist.Oralcare productsinclude
toothpasteandtoothbrushes.
Toothpastes:
pg. 7
PersonalCare:Personalcarereferstothetakingcareofyourbodyitscleanliness
and do something for its beautification which includes bathing. Personal care includes the
soaps.
Beauty Soaps:
Palmolive Naturals Balanced & Mild
Palmolive Naturals Moisture Care
Palmolive Naturals Nourishing Sensation
Palmolive Naturals Luxurious Softness
Palmolive Naturals Refreshing Moisture
Palmolive Naturals Saver Pack
Hand Wash:
PalmoliveHandWashAloeVerawithChamomile
Palmolive Hand Wash Antibacterial
Palmolive Hand Wash Antibacterial Sea Minerals
Shampoo:
Palmolive Naturals Healthy and Smooth Shampoo
PalmoliveNaturalsIntensiveMoistureShampoo
Palmolive Naturals Silky Straight Shampoo
Palmolive Naturals Anti-Hair Fall Shampoo
PalmoliveNaturalsAnti-DandruffShampoo
Surface Care:
Surface care refers to the taking care of dishes and products including
cleanliness of the dishes and that includes the dish wash bar and dish
wash liquid.
Dish wash Liquid:
Max Regular
Max Ultra
Max Lemon Fresh
Max Anti-Bacterial
pg. 8
Dish wash Paste:
Max Original
Max Lime
All Purpose Cleaner:
Max Rose Fresh (Red)
Max Lemon Fresh (Yellow)
Max Lavender Fresh (Purple)
Fabric Care
Fabric care refers to the taking care of wearing means
cleanliness of the clothes. In fabric Care laundrydetergents and
laundry bars areincluded.
Laundry detergents:
Brite Maximum Power
Brite Anti- Bacterial
Brite Machine Wash
Express Power
Bonus tristar
Bonus Active
Liquid Softener:
Softlan Liquid.
I along with my fellows, did 6 days internship here. The main purpose of our
internship was to study and learn about different production processes that are being
performedinCPPL.ButthemainconcernofmyinternshipwasonCOLGATEDENTAL
CREAM(CDC),WhereIhavelearntlotofprocessesregardingtheGelPowderusedto
manufacture Dental Creams.
pg. 9
2. Introduction to CDCMaking:
CDCAreaisdedicatedtoproducevariousDentalCreamsusedfororalcare.. In making
ofthese dental creams different raw materials are used as per requirement of
products.
a) PRODUCTS:
1. GRF
2. Sparkle
3. Herbal White
4. Herbal Green
5. Misvak White
6. Misvak Beige
7. Max Fresh Red
8. Max Fresh Blue
9. Max Fresh Green
10. Sensitive White
11. Sensifoam White
12. Charcoal White
13.CharcoalGrey
14. Colgate Total Advance Health
b) Raw MaterialsUsed:
The raw materials used for CDC Making are divided into four categories.
i) Major Solids
ii) Major Liquids
iii) Minor Solids
iv) Minor Liquids
They include:
 Zeodent 114/Absil 100
 SLS-Foaming Agent
 Hisil Silica
 MFP/CMC TMS
 Zeodent 165/MFILP
 Colors
 Natural Calcium Carbonate (NCC)
 Di CalciumPhosphate
 Precepetated CalciumCarbonate
c) Day Store:
Daystoreiswherethesolidmaterialsarekeptbeforetheiruse.Allof
theraw mateialsareimportedformothercountriesandtransportedto
the industry and stored for their usage. Each of the solid raw material
is contained in Polyethylene bag, each weighing 25 kg of bags.
d) FLAVOR ROOM:
Flavor room is where favors are kept. Which are used in different dental creams.
They are also imported from other countries. They are:
 PEG 600
 Silicate
 GRF Flavors
 Benzyl Alcohol
 Sorriso Herbal Flavor
 Sodium Hydoxide
4 Mixers are mainly used.
Brogli Mixer Fryma Mixer Li-Yuan-1 Mixer Li-Yuan-2 Mixer
350 kg 600 kg 1100 kg
GRF and Sparkle
1100 kg
GRF and Herbal
(White and
Green)
Process of Making CDC:
At very first step Raw materials are added toweighing tanks according to their
need of quantity and then are transfered to GEL tank with some level of steam to
maintain the temperature of GEL.
When GEL is prepared then it is sent to desired Mixer.
In that Mixer Powder comes from Powder Hoppers while flavor is added in flavor
hopper.
After mixing of all the desired ingredients in GEL mixer, batch is sent to Storage
tanks then to the Packing Section.
Accessories:
1.Agetator:
Placed in GEL Tank and GEL Mixer, takes the paste from their sides
and mix them.
2.Homogenizer:
Placed in GEL Tank and GEL Mixer, makes lumps free paste.
3.Purolator Filter:
Attached with GEL Mixer to make lumps free batch and then send back to
storage tanks.
4.Micro Filter:
Attachedfromupper sidesof Rawmaterial tanks andGEL Mixers whose function
is to stop the entrance of microorganisms into tanks.
5.Dispax Reactor:
Used in Brogli Mixer which does not allow Out Burst Film (Cooling
Crystals) to be dissolved in GELMixer when making Max Fresh.
6.Gear Box:
Works on the principle of gear ratio.
Used when we need less revolution per minute (rpm) for agitator or homogenizer.
Glycerine is only used in making of sensitive.
e) Common Raw Mateials InPaste:
7.
Pasteurized Water
Sodium CMC
Sodium Sacchharin
Sodium Lauryl Sulphate (SLS)
f) Utilities:
1. Screw Compressor
2. Chiller
3 Compressors
6 Fans (2 for each compressor)
45 KW (Capacity)
25-28’C (Outlet Temperature)
3. Dryer
4. Air Vessels
5. Filters
1. BROGLI MIXER:
FORMALIN
WATER
GLYCERINE SORBITOL
BROGLI
GEL TANK POWDER
HOPPER
FLAVOUR
HOPPER
BROGLI
GEL MIXER
PUROL-
ATOR
FILTER
STORAGE
TANK
pg. 12
2. FRYMA MIXER:
F O R M A L I N
W A T E R
GLYCERINE SORBITOL
FRYMA
GEL TANK POWDER
HOPPER
FLAVOUR
HOPPER
FR YMA
GEL MIXER
PUROL-
ATOR
FILTER
STORAGE
TANK
pg. 13
SMALL
MIXER
3. LI-YUAN-1 MIXER:
FORMALIN
WATER GLYCERINE SORBITOL
GEL TANK
LI-YUAN
POWDER
HOPPER
PUROLATE
R
FILTER
LI-YUAN
MIXER
FLAVOR
HOPPER
SPARKLE GRF
pg. 14
3. LI-YUAN-2 MIXER:
FORMALIN
WATER GLYCERINE SORBITOL
GEL
TANK
SILICATE
FLAVOR
SLS
LI-YUAN
MIXER
STORAGE TANK
pg. 15
Packaging:
Area where final products are packed and transferred to the markets.
There are six machines operationg in CDC Packing.
1. NORDEN-1
2. NORDEN-2
3. NORDEN-3
4. NORDEN-4
5. NORDEN-5
6. HARMETIC
Parts:
 Casset:
Where tubes arekept.
 Lifting Plate:
Which up lifts the tube.
 Tube Holder:
Carries the tube.
 Air Cleaning Nozzel:
Removes dust/air from the tube.
 Photocell Resistant Tube:
 Filling Nozzle:
Fills paste in the tube.
 Heater:
Heats up the tube.
 Code Device:
Strikes code ontube.
 Cutter:
pg. 20
Cuts the unnecessary part of tube.
 Tube Ejecter:
Ejects the tube from machine and tube falls on Conveyer Belt.
 Conveyer Belt
Transfers the tube towards packing section.
Shrinkwrapping Procedure:
Step-1:
Take 6 tubes from Conveyer Belt.
Step-2:
Put the bundle of 6 tubes in poly film.
Step-3:
Pass the bundle through shrinkwrap heater.
Step-4:
Crease the poly film by pressing the side of tubes bundle manually.
Step-5:
Put the shrink packed tubes bundleon weigh scale.
Step-6:
If the bundle is within range put in CWC.
Step-7:
Seal and code the packrite.
Hanger Packing Working Instructions:
1. Take tubes from Conveyer Belt.
2. Place the tubes on hanger.
3. Insert longer flap in Cartons.
4. 2nd
flap over laps the folding flap.
5. Place the hanger on weight scale check the weight.
6. Hangers meet the specification place in CWC.
7. Seal the packrite.
3. CLEANING AND SANITIZATION (CNS):
Sanitization is the process to halt the growth of microorganisms in lines and tanks.
In Lines Sanitization is carried out by Citric acid while in Tanks, It is carried out by
Steam.
Time for Citric acid to be poured in Lines/Hoppers is 30 minutes.
InCNSdetector machine(CharmNovalumII)ADPofmicroorganismsis
detected from the sample which is taken from hopper/tank (to be sanitized).
CNS
ALERTLEVEL ACTION LEVEL
(CNSonduedate) (CNS after due date but
not More than 10 days)
Difference Between Sanitization and Sterilization:
In Sterilization, Growth of Micro Organisms is halted while in Sterilization Micro
Organisms are completelykilled.
Step 7.
Sanitization
Step 5.
Post Rinse
Step 4.
Cleaning
Process of Sanitization:
C&S Critical ParametersTactwins:
Time Water
Action Individual
Concentration Nature of Soil
Temperature SurfacetobeCleaned
Step 8.
Final Rinse
STEP 1.
Residue
Removal
YES
Step 2.
Pre Rinse

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sagarkhan-181207182013.pdf

  • 2. University: SAGAR ALI 16 CH 56 Chemical Engineering Mehran University Of EngineeringandTechnology,Jamshoro (MUET) Industry: Colgate Palmolive PakistanLtd. Department: Colgate Dental Cream(CDC) pg. 2 Name: Class Roll No: Technology:
  • 3. Background of Colgate Palmolive Pakistan Acknowledgement BeingastudentofChemicalEngineeringMehranUET,I’mgratefulto ColgateStaffandEngineerswhogavemeawarmwelcomeandadetailed orientation regarding Colgate-Palmolive Pakistan Limited. They have beenverycooperativeandmotivatedinternstolearnhereasmuchas they want. I’malsowhole-heartedlybeholdentotheManagement,Supervisorsand Workers,andspecialthankstoMr.SALEEM,whoencouraged,guidedand supported us (the internes) throughout this internship program. We have hadveryhonorabletimeworkinghere,inspectingtheirwaysofworking things out. Me along with my fellows learnt very much incompetitive environment of theindustry. Ialso express my gratitude to Mr. FURQAN AHMED, Mr. SHEERAZ JUNEJO and Mr.MUHAMMADUZAIRwhohavebeenverysupportiveatevery step.Theyhavegiventheirprecioustimefromtheirdailytoughroutine and guided me throughout this whole period of Internship. • In 1984 started as a license manufacturer of Colgate-Palmolive products in Pakistan • In 1990 Colgate-Palmolive Inc. (USA) joined as a 30% equity partner • Market leaders in Oral Care, Surface Care & Fabric Care categories • 450 Distributors acrossPakistan • ISO 9000 : 2000 Quality Management System • KSE Top Companies Award for 2004, 2005, 2006 • Corporate Excellence Certificate 2001-02 & 2004
  • 4. Contents 1. Introduction to Colgate Palmolive 2. Introduction to CDC Making 3. Process-Making-Packaging 4. Cleaning and Sanitization
  • 5. 1.Introduction to Colgate Palmolive Colgate-Palmolive(Pakistan)LimitedwasinitiallyincorporatedinPakistanonDecember5, 1977 as a public limited company with the name of National Detergents Limited. It started its operations in Pakistan in 1977 as joint venture between Colgate Palmolive (USA) and Lakson Group. Colgate Palmolive is one of the largest ventures by the group. With assets of more than Rs. 400 million and a turnover of Rs. 1500 million, it has emerged as one of the largest corporations in Pakistan. Colgate–PalmolivePakistanLimited isaFast-MovingConsumerGoods(FMCG)industry. FMCGaretheproductsthatarequitefrequentlyusedbytheconsumersintheirdaily routine. pg. 6
  • 6. Company is equipped with two manufacturing plants across the country within, 1. KotriSindh 2. Sundhar Punjab. The Companyis currently engaged in manufacturing of following related products. Categories of Products in CPPL: a. Oralcare b.Personalcare c.SurfaceCare d. Fabriccare OralCare:Oralcarereferstotakingcareofyourmouth;specifically,the insideofyourmouth.Practicingoralcarekeepsyourgumsandteethhealthy, whichisimportantnotonlyforyourmouth,butforoverallhealth.Thewell- beingofyourmouthisknownasoralhealth.Oralcareincludestoothbrushing, flossing,eatingwellandregularvisitstothedentist.Oralcare productsinclude toothpasteandtoothbrushes. Toothpastes: pg. 7
  • 7. PersonalCare:Personalcarereferstothetakingcareofyourbodyitscleanliness and do something for its beautification which includes bathing. Personal care includes the soaps. Beauty Soaps: Palmolive Naturals Balanced & Mild Palmolive Naturals Moisture Care Palmolive Naturals Nourishing Sensation Palmolive Naturals Luxurious Softness Palmolive Naturals Refreshing Moisture Palmolive Naturals Saver Pack Hand Wash: PalmoliveHandWashAloeVerawithChamomile Palmolive Hand Wash Antibacterial Palmolive Hand Wash Antibacterial Sea Minerals Shampoo: Palmolive Naturals Healthy and Smooth Shampoo PalmoliveNaturalsIntensiveMoistureShampoo Palmolive Naturals Silky Straight Shampoo Palmolive Naturals Anti-Hair Fall Shampoo PalmoliveNaturalsAnti-DandruffShampoo Surface Care: Surface care refers to the taking care of dishes and products including cleanliness of the dishes and that includes the dish wash bar and dish wash liquid. Dish wash Liquid: Max Regular Max Ultra Max Lemon Fresh Max Anti-Bacterial pg. 8
  • 8. Dish wash Paste: Max Original Max Lime All Purpose Cleaner: Max Rose Fresh (Red) Max Lemon Fresh (Yellow) Max Lavender Fresh (Purple) Fabric Care Fabric care refers to the taking care of wearing means cleanliness of the clothes. In fabric Care laundrydetergents and laundry bars areincluded. Laundry detergents: Brite Maximum Power Brite Anti- Bacterial Brite Machine Wash Express Power Bonus tristar Bonus Active Liquid Softener: Softlan Liquid. I along with my fellows, did 6 days internship here. The main purpose of our internship was to study and learn about different production processes that are being performedinCPPL.ButthemainconcernofmyinternshipwasonCOLGATEDENTAL CREAM(CDC),WhereIhavelearntlotofprocessesregardingtheGelPowderusedto manufacture Dental Creams. pg. 9
  • 9. 2. Introduction to CDCMaking: CDCAreaisdedicatedtoproducevariousDentalCreamsusedfororalcare.. In making ofthese dental creams different raw materials are used as per requirement of products. a) PRODUCTS: 1. GRF 2. Sparkle 3. Herbal White 4. Herbal Green 5. Misvak White 6. Misvak Beige
  • 10. 7. Max Fresh Red 8. Max Fresh Blue 9. Max Fresh Green 10. Sensitive White 11. Sensifoam White 12. Charcoal White 13.CharcoalGrey 14. Colgate Total Advance Health
  • 11. b) Raw MaterialsUsed: The raw materials used for CDC Making are divided into four categories. i) Major Solids ii) Major Liquids iii) Minor Solids iv) Minor Liquids They include:  Zeodent 114/Absil 100  SLS-Foaming Agent  Hisil Silica  MFP/CMC TMS  Zeodent 165/MFILP  Colors
  • 12.  Natural Calcium Carbonate (NCC)  Di CalciumPhosphate  Precepetated CalciumCarbonate c) Day Store: Daystoreiswherethesolidmaterialsarekeptbeforetheiruse.Allof theraw mateialsareimportedformothercountriesandtransportedto the industry and stored for their usage. Each of the solid raw material is contained in Polyethylene bag, each weighing 25 kg of bags.
  • 13. d) FLAVOR ROOM: Flavor room is where favors are kept. Which are used in different dental creams. They are also imported from other countries. They are:  PEG 600  Silicate  GRF Flavors  Benzyl Alcohol  Sorriso Herbal Flavor  Sodium Hydoxide 4 Mixers are mainly used. Brogli Mixer Fryma Mixer Li-Yuan-1 Mixer Li-Yuan-2 Mixer 350 kg 600 kg 1100 kg GRF and Sparkle 1100 kg GRF and Herbal (White and Green)
  • 14. Process of Making CDC: At very first step Raw materials are added toweighing tanks according to their need of quantity and then are transfered to GEL tank with some level of steam to maintain the temperature of GEL. When GEL is prepared then it is sent to desired Mixer. In that Mixer Powder comes from Powder Hoppers while flavor is added in flavor hopper. After mixing of all the desired ingredients in GEL mixer, batch is sent to Storage tanks then to the Packing Section. Accessories: 1.Agetator: Placed in GEL Tank and GEL Mixer, takes the paste from their sides and mix them. 2.Homogenizer: Placed in GEL Tank and GEL Mixer, makes lumps free paste.
  • 15. 3.Purolator Filter: Attached with GEL Mixer to make lumps free batch and then send back to storage tanks. 4.Micro Filter: Attachedfromupper sidesof Rawmaterial tanks andGEL Mixers whose function is to stop the entrance of microorganisms into tanks. 5.Dispax Reactor: Used in Brogli Mixer which does not allow Out Burst Film (Cooling Crystals) to be dissolved in GELMixer when making Max Fresh. 6.Gear Box: Works on the principle of gear ratio. Used when we need less revolution per minute (rpm) for agitator or homogenizer. Glycerine is only used in making of sensitive.
  • 16. e) Common Raw Mateials InPaste: 7. Pasteurized Water Sodium CMC Sodium Sacchharin Sodium Lauryl Sulphate (SLS) f) Utilities: 1. Screw Compressor 2. Chiller 3 Compressors 6 Fans (2 for each compressor) 45 KW (Capacity) 25-28’C (Outlet Temperature) 3. Dryer 4. Air Vessels 5. Filters
  • 17. 1. BROGLI MIXER: FORMALIN WATER GLYCERINE SORBITOL BROGLI GEL TANK POWDER HOPPER FLAVOUR HOPPER BROGLI GEL MIXER PUROL- ATOR FILTER STORAGE TANK pg. 12
  • 18. 2. FRYMA MIXER: F O R M A L I N W A T E R GLYCERINE SORBITOL FRYMA GEL TANK POWDER HOPPER FLAVOUR HOPPER FR YMA GEL MIXER PUROL- ATOR FILTER STORAGE TANK pg. 13
  • 19. SMALL MIXER 3. LI-YUAN-1 MIXER: FORMALIN WATER GLYCERINE SORBITOL GEL TANK LI-YUAN POWDER HOPPER PUROLATE R FILTER LI-YUAN MIXER FLAVOR HOPPER SPARKLE GRF pg. 14
  • 20. 3. LI-YUAN-2 MIXER: FORMALIN WATER GLYCERINE SORBITOL GEL TANK SILICATE FLAVOR SLS LI-YUAN MIXER STORAGE TANK pg. 15
  • 21. Packaging: Area where final products are packed and transferred to the markets. There are six machines operationg in CDC Packing. 1. NORDEN-1 2. NORDEN-2 3. NORDEN-3 4. NORDEN-4 5. NORDEN-5 6. HARMETIC Parts:  Casset: Where tubes arekept.  Lifting Plate: Which up lifts the tube.  Tube Holder: Carries the tube.  Air Cleaning Nozzel: Removes dust/air from the tube.  Photocell Resistant Tube:  Filling Nozzle: Fills paste in the tube.  Heater: Heats up the tube.  Code Device: Strikes code ontube.  Cutter: pg. 20
  • 22. Cuts the unnecessary part of tube.  Tube Ejecter: Ejects the tube from machine and tube falls on Conveyer Belt.  Conveyer Belt Transfers the tube towards packing section. Shrinkwrapping Procedure: Step-1: Take 6 tubes from Conveyer Belt. Step-2: Put the bundle of 6 tubes in poly film. Step-3: Pass the bundle through shrinkwrap heater. Step-4: Crease the poly film by pressing the side of tubes bundle manually. Step-5: Put the shrink packed tubes bundleon weigh scale. Step-6: If the bundle is within range put in CWC. Step-7: Seal and code the packrite.
  • 23. Hanger Packing Working Instructions: 1. Take tubes from Conveyer Belt. 2. Place the tubes on hanger. 3. Insert longer flap in Cartons. 4. 2nd flap over laps the folding flap. 5. Place the hanger on weight scale check the weight. 6. Hangers meet the specification place in CWC. 7. Seal the packrite.
  • 24. 3. CLEANING AND SANITIZATION (CNS): Sanitization is the process to halt the growth of microorganisms in lines and tanks. In Lines Sanitization is carried out by Citric acid while in Tanks, It is carried out by Steam. Time for Citric acid to be poured in Lines/Hoppers is 30 minutes. InCNSdetector machine(CharmNovalumII)ADPofmicroorganismsis detected from the sample which is taken from hopper/tank (to be sanitized). CNS ALERTLEVEL ACTION LEVEL (CNSonduedate) (CNS after due date but not More than 10 days) Difference Between Sanitization and Sterilization: In Sterilization, Growth of Micro Organisms is halted while in Sterilization Micro Organisms are completelykilled.
  • 25. Step 7. Sanitization Step 5. Post Rinse Step 4. Cleaning Process of Sanitization: C&S Critical ParametersTactwins: Time Water Action Individual Concentration Nature of Soil Temperature SurfacetobeCleaned Step 8. Final Rinse STEP 1. Residue Removal YES Step 2. Pre Rinse