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Unit Operation: CHD 228
Instructor: Dr. Pratibha Biswal
Lecture 2
Particle Size, Screen analysis
20-11-2018 1Shiv Nadar University
• Large quantities of particles are handled on the industrial scale
• It is frequently necessary to define the system as a whole.
• It is necessary to know the distribution of particle sizes in the
mixture.
• It is necessary to define a mean size which in some way
represents the behaviour of the particulate mass as a whole in
the system.
Why we need Particle Size Distribution?
20-11-2018 Shiv Nadar University 2
Particle Size Distribution: Need
• In general, "diameters" may be specified for any equidimensional particle.
• Particles that are not equidimensional, i.e., that are longer in one direction than in others,
are often characterized by the second longest major dimension.
• For needle like particles, for example, size would refer to the thickness of the particles, not
their length.
• Conventionally, particle sizes are expressed in different units depending on the size range
involved.
• Coarse particles are measured in inches or millimetres.
• Fine particles in terms of screen size; very fine particles in micrometers or nanometers.
• Ultrafine particles are described in terms of their surface area per unit mass.
Particle Size
20-11-2018 Shiv Nadar University 3
Particle Size Range
Particle size is characterized
using these terms:
i. Very coarse
ii. Coarse
iii. Moderately coarse
iv. Fine
v. Very fine
20-11-2018 Shiv Nadar University 4
20-11-2018 Shiv Nadar University 5
Wood Chips
Urea
Granulated
Sugar
Flour
Ceramic
Powder
Magnetic
Pigment
Organic
Pigment
Carbon Black
Particle Size Range
20-11-2018 Shiv Nadar University 6
Particle size can influence variety of
important factors:
• Dissolution rate
• Suspendability
• Uniform distribution
• Penetrability
• Chemical Reaction
• Heating and Combustion etc.
Effects of Particle Size
Screen Analysis: Nomenclature
• Particles at a specified size range can
be measured by screens or testing
sieves.
• Testing sieves (screens) are
constructed with square openings of
woven wires.
• Mesh: A single opening measured from
the center of each wire.
• Screen Aperture: Minimum clear space
between the wires
• Coarse Screens: “Mesh size” refers to
the distance between adjacent wires.
• Fine Screen: “Mesh number or sieve
number” is the number of openings per
linear inch.
20-11-2018 Shiv Nadar University 7
Mesh
Mesh Number: Number of
meshes in 1 inch length from
the center of a wire
Screen Aperture
20-11-2018 Shiv Nadar University 8
Screen Analysis: Standard Screens
• Sieves (Screens) are available in a number of standard series. (See Table 1.1 in Coulson
and Richardson; Appendix 20 in Mccabe, Smith and Harriot)
• The screen type is dependent on the diameter of the wire and mesh number.
Tyler Standard
Screen Series
Mostly used
US Sieve Series
Almost similar to
Tyler screen series
with slight
modifications
UK British
Standard
Smaller and
fragile
Institute of
Mining and
Metallurgy
Robust and
Expensive
20-11-2018 Shiv Nadar University 9
Screen Analysis: Standard Screens
• Wire Diameter is 0.0053
mm (0.0021 in)
• Screen Aperture: 0.0029
in
 In general, when screens are in
series,
𝐴𝑟𝑒𝑎 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑙𝑎𝑟𝑔𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛
𝐴𝑟𝑒𝑎 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑠𝑚𝑎𝑙𝑙𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛
=2
𝐿𝑒𝑛𝑔𝑡ℎ 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑙𝑎𝑟𝑔𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛
𝐿𝑒𝑛𝑔𝑡ℎ 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑠𝑚𝑎𝑙𝑙𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛
=√2
 Intermediate screens are also
available for closer size
distribution (As shown in table).
20-11-2018 Shiv Nadar University 10
Screen Analysis
 Screens are stacked with the coarsest screen at the
top and finest screen at the bottom.
 The sieves are shaken either manually or
mechanically for a fixed time.
 Material retained in each screen is removed and
weighed separately. Amount of material in each
screen is expressed as weight fraction.
 Any particles that pass the finest screen are caught
in a pan at the bottom of the stack.
 The results of a screen analysis are tabulated to
show the relationship between mass fraction and
mesh size.
20-11-2018 Shiv Nadar University 11
 Tabulate this increment as a
function of the average particle
size.
Differential Screen Analysis
6
8
10
200
Pan
Mixture
20-11-2018 Shiv Nadar University 12
 Plotting the cumulative sums against
the maximum particle diameter or
screen opening
Cumulative Screen Analysis
6
8
10
200
Pan
Mixture
Mixed Particle Sizes And Size Analysis
• In a sample mass ms, density ρt and uniform particles of diameter Dp, total volume of the sample is
• Number of particles in the sample is
• The total surface area of the sample is
𝑉𝑠 =
𝑚 𝑠
𝜌𝑡
Mass of the sample
Density of the sample
(Equals Density of total mixture)
….(2)
𝑁 =
𝑉𝑠
𝑉𝑝
Total Volume of the Sample
Volume of Single Particle in the Sample
𝑁 =
𝑚 𝑠
𝜌𝑡 𝑉𝑝 …(3)
𝐴 𝑠 = 𝑁𝑆 𝑝 = 𝑁𝐴 𝑝 =
6𝑚 𝑠
Φ 𝑠 𝜌𝑡 𝐷 𝑝 …(4)
20-11-2018 Shiv Nadar University 13
Surface Area of Single Particle in the Sample
Which Method is Better??
20-11-2018 Shiv Nadar University 14

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Lec2

  • 1. Unit Operation: CHD 228 Instructor: Dr. Pratibha Biswal Lecture 2 Particle Size, Screen analysis 20-11-2018 1Shiv Nadar University
  • 2. • Large quantities of particles are handled on the industrial scale • It is frequently necessary to define the system as a whole. • It is necessary to know the distribution of particle sizes in the mixture. • It is necessary to define a mean size which in some way represents the behaviour of the particulate mass as a whole in the system. Why we need Particle Size Distribution? 20-11-2018 Shiv Nadar University 2 Particle Size Distribution: Need
  • 3. • In general, "diameters" may be specified for any equidimensional particle. • Particles that are not equidimensional, i.e., that are longer in one direction than in others, are often characterized by the second longest major dimension. • For needle like particles, for example, size would refer to the thickness of the particles, not their length. • Conventionally, particle sizes are expressed in different units depending on the size range involved. • Coarse particles are measured in inches or millimetres. • Fine particles in terms of screen size; very fine particles in micrometers or nanometers. • Ultrafine particles are described in terms of their surface area per unit mass. Particle Size 20-11-2018 Shiv Nadar University 3
  • 4. Particle Size Range Particle size is characterized using these terms: i. Very coarse ii. Coarse iii. Moderately coarse iv. Fine v. Very fine 20-11-2018 Shiv Nadar University 4
  • 5. 20-11-2018 Shiv Nadar University 5 Wood Chips Urea Granulated Sugar Flour Ceramic Powder Magnetic Pigment Organic Pigment Carbon Black Particle Size Range
  • 6. 20-11-2018 Shiv Nadar University 6 Particle size can influence variety of important factors: • Dissolution rate • Suspendability • Uniform distribution • Penetrability • Chemical Reaction • Heating and Combustion etc. Effects of Particle Size
  • 7. Screen Analysis: Nomenclature • Particles at a specified size range can be measured by screens or testing sieves. • Testing sieves (screens) are constructed with square openings of woven wires. • Mesh: A single opening measured from the center of each wire. • Screen Aperture: Minimum clear space between the wires • Coarse Screens: “Mesh size” refers to the distance between adjacent wires. • Fine Screen: “Mesh number or sieve number” is the number of openings per linear inch. 20-11-2018 Shiv Nadar University 7 Mesh Mesh Number: Number of meshes in 1 inch length from the center of a wire Screen Aperture
  • 8. 20-11-2018 Shiv Nadar University 8 Screen Analysis: Standard Screens • Sieves (Screens) are available in a number of standard series. (See Table 1.1 in Coulson and Richardson; Appendix 20 in Mccabe, Smith and Harriot) • The screen type is dependent on the diameter of the wire and mesh number. Tyler Standard Screen Series Mostly used US Sieve Series Almost similar to Tyler screen series with slight modifications UK British Standard Smaller and fragile Institute of Mining and Metallurgy Robust and Expensive
  • 9. 20-11-2018 Shiv Nadar University 9 Screen Analysis: Standard Screens • Wire Diameter is 0.0053 mm (0.0021 in) • Screen Aperture: 0.0029 in  In general, when screens are in series, 𝐴𝑟𝑒𝑎 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑙𝑎𝑟𝑔𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛 𝐴𝑟𝑒𝑎 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑠𝑚𝑎𝑙𝑙𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛 =2 𝐿𝑒𝑛𝑔𝑡ℎ 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑙𝑎𝑟𝑔𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛 𝐿𝑒𝑛𝑔𝑡ℎ 𝑜𝑓 𝑆𝐴 𝑜𝑓 𝑠𝑚𝑎𝑙𝑙𝑒𝑟 𝑠𝑐𝑟𝑒𝑒𝑛 =√2  Intermediate screens are also available for closer size distribution (As shown in table).
  • 10. 20-11-2018 Shiv Nadar University 10 Screen Analysis  Screens are stacked with the coarsest screen at the top and finest screen at the bottom.  The sieves are shaken either manually or mechanically for a fixed time.  Material retained in each screen is removed and weighed separately. Amount of material in each screen is expressed as weight fraction.  Any particles that pass the finest screen are caught in a pan at the bottom of the stack.  The results of a screen analysis are tabulated to show the relationship between mass fraction and mesh size.
  • 11. 20-11-2018 Shiv Nadar University 11  Tabulate this increment as a function of the average particle size. Differential Screen Analysis 6 8 10 200 Pan Mixture
  • 12. 20-11-2018 Shiv Nadar University 12  Plotting the cumulative sums against the maximum particle diameter or screen opening Cumulative Screen Analysis 6 8 10 200 Pan Mixture
  • 13. Mixed Particle Sizes And Size Analysis • In a sample mass ms, density ρt and uniform particles of diameter Dp, total volume of the sample is • Number of particles in the sample is • The total surface area of the sample is 𝑉𝑠 = 𝑚 𝑠 𝜌𝑡 Mass of the sample Density of the sample (Equals Density of total mixture) ….(2) 𝑁 = 𝑉𝑠 𝑉𝑝 Total Volume of the Sample Volume of Single Particle in the Sample 𝑁 = 𝑚 𝑠 𝜌𝑡 𝑉𝑝 …(3) 𝐴 𝑠 = 𝑁𝑆 𝑝 = 𝑁𝐴 𝑝 = 6𝑚 𝑠 Φ 𝑠 𝜌𝑡 𝐷 𝑝 …(4) 20-11-2018 Shiv Nadar University 13 Surface Area of Single Particle in the Sample
  • 14. Which Method is Better?? 20-11-2018 Shiv Nadar University 14