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Engineering tips in sampling systems
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Pouriya Niknam , Dec 2016 Piramoonco.com
Table of content
• NOx converter
• gas pump
• Gas coolers
• Filters
NOx converter
type Temp eff Max NO2
Content
Carbon
Based
200C 95% 150ppm
Same Price
Metal
Based
400C 97% 300ppm
•Maintenance calculator NOxCal for service life monitoring
 NOX Converter
 NOx converter types
No ATEX NOx converter, Purge the Cabinet to keep it ex-free
400C-->450C: trick for temporarily reactivate the NOx, 3week…
NO2--- NO+O2
Less Side effects:
◦ No O2 added to sample
◦ No SO2 reduction
◦ No CO Production
◦ No Pressure Drop
(140mbar)
 Basics: Pump head
NL/H
Long distance from tapping point -- decrease flow rate
defective bellow
SUCTION FROM AMBIENT
For bellow Test
Pump
Compressor
Cooler
Analyzer
Dual Stage
Comp.
Cooler
pump Analyzer
Pump/Dual Stage
Comp. Cooler
Analyzer
Some discussion about Components Order…
Notformining
Zone1(outsidepump)
Equipmentprotection(Gas)atmosphere
Zone1(insidepump)
ConstructivelySafe
Justforsurrounding
TemperatureRange(alsocoverT1/T2)
Special
Pump Tips & Notes:
These items will reduce lifetime:
 Operation with non atmospheric pressure
 Operation under high temperature condition
item sample pressure
Buhler Nox Converter <1.5 bar absolute
GMS800 –200 hPa ... 1,000 hPa
Siemens ultramat23 (BA5000) 0.5 to 1.5 bar absolute
Siemens OXYMAT 64 (High P) 2 000 hPa (abs.)
(Low P) 30 hPa more than atmospheric
BA3 100 to 200 mbar (gauge)
BA 3500 Pressure 10 - 200 mbar
BA 6000-O2 0.5 to 1.5 bar absolute
Pump Tips & Notes:
 No ATEX version for 800L/hr pump
 New product with ATEX cert. as 700L/hr, but
◦ No option for head material
◦ T3 only
 Temperature will be limit by the bottleneck
 ATEX will be expired after 5 years (from production date and not
operation)
◦ They can be used in non hazardous area for another 10 years
period.
◦ Or sending to Buhler for complete service.
 Membrane like KNF are using Glue (Acid, Solvent,…)
 Buhler specific Sample pump without any glue
◦ (Honeywell Changed from KNF to Buhler )
Pump Tips & Notes:
The sample gas pump is suitable for gases only, not for liquids.
The sample gas pump should be operated without pressure.
A system pressure above 0.3bar is not allowed.
The gas outlet must not be closed.
The flow rate must be at least 50 l/h (150 l/h with system pressure
0.3 bar).
If the flow rate continuously is throttled below 150 l/h during
operation, the flow rate must be controlled with a bypass valve.
Extreme throttling reduces the life time of the bellow.
If the pump is equipped with a bypass valve, the flow rate can be
adjusted
rated current of the circuit breaker switch
 230 V = 0.48 A,
 115 V = 0.84 A,
 24 V DC = 0.8 A
Peltier gas coolers (PKE)
compact /one gas path Per Heat exchanger/cheaper than compressor coolers
standard application:
volume flow of 150 l/h at 1 bar@ 70°C , inlet dew point of 40°C.
Compressor coolers (EGK)
working principle as refrigerator/ more cooling power than peltier coolers.
 Cooler selection
• energy to cool the gas about doubles with a rise of dew point of 10°C
• double pressure = double energy to cool
• the factory setting of the gas outlet temperature and dew point
of approximately 5°C
Exchanger material
•Steel >the best choice
•aggressive components > glass then
•Only in certain applications PVDF
We suggest to limit the load on the heat exchanger to a range of 60..80%.
•For M&C glass type is cheaper than SS.
•For Buhler SS is cheaper with better performance for non-corrosive cased
Cooler tips
Buhler double stream exchangers
EGK 1/2, PKE 42 or EGK 2 Ex
saves money and time for mounting
Cross-sensitivity is very low:
Vari0ating one path in the whole energy range of the exchanger will variate
the other path in a maximum of 0,5K!
In case of same gas energies  variations of the one streams outlet
dewpoint by switching on and off the other stays below 0,2K
 Compact size: approx. 250 x 220 x 200 mm
 Peltier cooler with 1 heat exchanger
 Adjustable dew point 3/5/10/15 °C
 Adjustable Delta T Control
 Analogue signal output
 Power supply 24 V DC
 Power max. 70 W
Dual P. Pump

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Engineering tips for sampling systems [Piramoon & Buhler Technologies], by Pouriya Niknam

  • 1. Engineering tips in sampling systems with & Pouriya Niknam , Dec 2016 Piramoonco.com
  • 2. Table of content • NOx converter • gas pump • Gas coolers • Filters
  • 4. type Temp eff Max NO2 Content Carbon Based 200C 95% 150ppm Same Price Metal Based 400C 97% 300ppm •Maintenance calculator NOxCal for service life monitoring
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  • 8. No ATEX NOx converter, Purge the Cabinet to keep it ex-free 400C-->450C: trick for temporarily reactivate the NOx, 3week… NO2--- NO+O2 Less Side effects: ◦ No O2 added to sample ◦ No SO2 reduction ◦ No CO Production ◦ No Pressure Drop (140mbar)
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  • 11. NL/H Long distance from tapping point -- decrease flow rate
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  • 13. defective bellow SUCTION FROM AMBIENT For bellow Test
  • 14. Pump Compressor Cooler Analyzer Dual Stage Comp. Cooler pump Analyzer Pump/Dual Stage Comp. Cooler Analyzer Some discussion about Components Order…
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  • 24. Pump Tips & Notes: These items will reduce lifetime:  Operation with non atmospheric pressure  Operation under high temperature condition item sample pressure Buhler Nox Converter <1.5 bar absolute GMS800 –200 hPa ... 1,000 hPa Siemens ultramat23 (BA5000) 0.5 to 1.5 bar absolute Siemens OXYMAT 64 (High P) 2 000 hPa (abs.) (Low P) 30 hPa more than atmospheric BA3 100 to 200 mbar (gauge) BA 3500 Pressure 10 - 200 mbar BA 6000-O2 0.5 to 1.5 bar absolute
  • 25. Pump Tips & Notes:  No ATEX version for 800L/hr pump  New product with ATEX cert. as 700L/hr, but ◦ No option for head material ◦ T3 only  Temperature will be limit by the bottleneck  ATEX will be expired after 5 years (from production date and not operation) ◦ They can be used in non hazardous area for another 10 years period. ◦ Or sending to Buhler for complete service.  Membrane like KNF are using Glue (Acid, Solvent,…)  Buhler specific Sample pump without any glue ◦ (Honeywell Changed from KNF to Buhler )
  • 26. Pump Tips & Notes: The sample gas pump is suitable for gases only, not for liquids. The sample gas pump should be operated without pressure. A system pressure above 0.3bar is not allowed. The gas outlet must not be closed. The flow rate must be at least 50 l/h (150 l/h with system pressure 0.3 bar). If the flow rate continuously is throttled below 150 l/h during operation, the flow rate must be controlled with a bypass valve. Extreme throttling reduces the life time of the bellow. If the pump is equipped with a bypass valve, the flow rate can be adjusted rated current of the circuit breaker switch  230 V = 0.48 A,  115 V = 0.84 A,  24 V DC = 0.8 A
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  • 29. Peltier gas coolers (PKE) compact /one gas path Per Heat exchanger/cheaper than compressor coolers standard application: volume flow of 150 l/h at 1 bar@ 70°C , inlet dew point of 40°C. Compressor coolers (EGK) working principle as refrigerator/ more cooling power than peltier coolers.
  • 30.  Cooler selection • energy to cool the gas about doubles with a rise of dew point of 10°C • double pressure = double energy to cool • the factory setting of the gas outlet temperature and dew point of approximately 5°C Exchanger material •Steel >the best choice •aggressive components > glass then •Only in certain applications PVDF We suggest to limit the load on the heat exchanger to a range of 60..80%. •For M&C glass type is cheaper than SS. •For Buhler SS is cheaper with better performance for non-corrosive cased
  • 31. Cooler tips Buhler double stream exchangers EGK 1/2, PKE 42 or EGK 2 Ex saves money and time for mounting Cross-sensitivity is very low: Vari0ating one path in the whole energy range of the exchanger will variate the other path in a maximum of 0,5K! In case of same gas energies  variations of the one streams outlet dewpoint by switching on and off the other stays below 0,2K
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  • 34.  Compact size: approx. 250 x 220 x 200 mm  Peltier cooler with 1 heat exchanger  Adjustable dew point 3/5/10/15 °C  Adjustable Delta T Control  Analogue signal output  Power supply 24 V DC  Power max. 70 W