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Silicon Photomultiplier
Slawomir Piatek
Technical Consultant, Hamamatsu Corp.
Operation, Performance & Possible Applications
Introduction
Very high intrinsic gain together with minimal excess noise make
silicon photomultiplier (SiPM) a possible choice of a photodetector in
those applications where the input light is in the photon-counting
range.
2
Introduction
This webinar is a high-level review of SiPM’s structure, operation,
and opto-electronic characteristics, followed by a discussion of
some possible applications.
3
Outline
• Structure and operation
• Opto-electronic characteristics
• Applications
+ Automotive ToF LiDAR
+ Flow cytometry
+ Radiation detection and monitoring
• Summary and conclusions
4
SiPM
Structure and Operation of a SiPM
Portraits of SiPMs (images not to scale)
5
SiPM structure
SiPM is an array of microcells
=
APD
RQ
p+
π
n+
p+
oxide
Single microcell
electrical equivalent
circuit of a microcell
Side
view
Top
view
6
SiPM structure
...
Anode
Cathode
single microcell
RQ
APD
All of the microcells are connected in parallel
7
SiPM specifications
Active area: 1.3×1.3 − 6×6 mm2
Microcell size (pitch): 10×10, 15×15, 25×25, 50×50, 75×75 μm2
Number of microcells: (active area)/(microcell size), from 100’s to
10,000’s
Overvoltage: ΔV = VBIAS – VBD; recommended by the manufacturer
8
SiPM operation
VBIAS > VBD
K
A
× G
RL
time [ns]
Amplitude
[mV]
Example of single-photoelectron
waveform (1 p.e.)
Gain = area under the curve in electrons
9
SiPM operation
time [ns]
Amplitude
[mV]
Fast component
Slow component
RC time constant of the slow component
depends on microcell size (all else being equal)
Recovery time tR ≈ 5 times the RC time
constant
tR is on the order of 10’s to 100’s ns but in
practical situations, it is also a function of
detection bandwidth
10
SiPM operation
time
Arb.
The output of an SiPM is a chronological superposition of current
pulses
Current pulses due to photons
SiPM also outputs current pulses even in absence of light: dark
counts (dark current)
11
Dark Counts
time
Arb.
Dark-count pulses are indistinguishable from those due to photons
The rate of dark counts depends on overvoltage, temperature, and
size of the active area
Current pulses due to photons and dark
counts are indistinguishable
12
Crosstalk
Primary discharge can trigger
a secondary discharge in
neighboring microcells. This is
crosstalk.
time
Arb.
2 p.e. crosstalk event
Crosstalk probability depends on
overvoltage
13
Operation
VBIAS
1, 2, 3,….
VBIAS
If the pulses are distinguishable,
SiPM can be operated in a photon
counting mode.
If the pulses overlap, the SiPM can be
operated in an analog mode. The
measured output is voltage or current.
counter
SiPM V or I
0 100
light
14
SiPM detection circuits
V/V
RL
C
R
VBIAS
SiPM
Vout
C
R
VBIAS
SiPM
Vout
RF
TIA
+
-
15
SiPM
Performance and characteristics
16
Characteristics of a SiPM
• Photon detection efficiency
• Gain
• Crosstalk probability
• Dark current & dark counts
• Linearity & dynamic range
• Temperature effects
17
Photon detection efficiency
wavelength [nm]
Photon
detection
efficiency
[%]
• Photon detection efficiency (PDE) is
a probability that an incident photon
is detected. It depends on:
- wavelength
- overvoltage
- microcell size
Peak PDE 20% − 50%
18
Photon detection efficiency
wavelength [nm]
Photon
detection
efficiency
[%]
5
10
15
20
25
30 Examples of PDE curves for
SiPMs optimized for NIR, VIS,
and UV response.
19
Gain
Overvoltage [V] Crosstalk
prob.
&
PDE
• Gain of SiPM is comparable
to that of a PMT.
Excess noise very low:
F ~ 1.1, mostly due to crosstalk
Gain
S13720, 1.3×1.3 mm2
• Gain depends linearly on
overvoltage
25 μm
20
Gain versus temperature
Does gain of an SiPM depend on temperature?
Yes – if the bias voltage is fixed
Reverse bias voltage [V]
Gain
[×10
6
]
Otte et al. (2016)
21
Gain versus temperature
Does gain of an SiPM depend on temperature?
No – if the overvoltage is fixed
Temperature [°C]
Gain
variation
[%]
Fixed overvoltage
22
Crosstalk
Overvoltage [V]
Crosstalk
prob.
&
PDE
PCT increases with overvoltage
Crosstalk is the main contributor to
excess noise
F ≈ (1+PCT)
S13720, 1.3×1.3 mm2
25 μm
23
Dark Current
Overvoltage [V]
Dark
current
[A]
S13720, 1.3×1.3 mm2 Example of dark current versus overvoltage
DCR = ID/eμ
ID = 1×10-7 A (at 7 V)
μ = 1.2×106 (at 7 V)
-> DCR ≈ 520 kHz
or once per about 2 μs
25 μm
24
Linearity and dynamic range
Incident light level (850 nm) [W]
Output
current
[A]
S13720, 1.3×1.3 mm2 Example of output current versus incident light
level.
Photon irradiance (at 850 nm) = 4.3×1018×P[W]
P = 10-8 W −> 4.3×1010 photons per second
Linearity depends on the number of
microcells for a given active area
25 μm
25
SiPM, PMT & APD
This webinar will compare and contrast SiPM with a photomultiplier
tube (PMT) and APD.
Let’s briefly review the operation of a PMT and APD
Examples of a PMT (left) and APD (right).
26
Operation of a PMT
R1 R2 R3 R4 R5 R6 R7
C1 C2 C3
K P
D1 D2 D3 D4 D5 D6
V ~ 1000 V
e−
Rf
IP
IK
2 ns/div
100
mV/div
Typical voltage
divider
27
SiPM versus PMT
• Solid state versus vacuum tube
technology
• Comparable gains
• Comparable excess noise
• Dark count rate per unit active area
larger in SiPM
• E & B field immunity in SiPM
• Comparable photosensitivity in the
spectral overlap region
• Greater optimization for PMTs
28
Operation of an APD
self-quenching avalanche
VBIAS
RL
electrons
holes
IPH
APD biased below breakdown voltage
Single photon can lead up to about
100 of electron-hole pairs
Avalanche is self-quenching
Thus gain up to ~100
photon
29
SiPM versus APD
log(Gain)
Gain = 1
linear
region
Geiger
region
VBIAS
VBD
APDs SiPMs
• Differ in construction
• GainSiPM >> GainAPD
• FSiPM << FAPD
30
Possible applications of SiPMs
• Flow cytometry
• Automotive time-of-flight LiDAR
• Radiation detection and monitoring
31
Automotive time-of-flight LiDAR
How far is this tree?
LiDAR
LiDAR = Light Detection and Ranging
32
Automotive ToF LiDAR: basic concept
to target
emitted pulse
“start” pulse
“stop” pulse
emission optics
timer
collection optics
laser
returned pulse after Δt
beam splitter
w = cτ
“fast” photodetector
33
Automotive ToF LiDAR: basic concept
Measure round-trip time-of-flight Δt
Range (distance to the reflection point) = cΔt/2; here c is the
speed of light
By scanning the surroundings, a 3D map can be constructed
34
Characteristics of received light
• Wavelength: 905 nm or 1550 nm
• Pulse: duration 2 – 5 ns
• No. of photons per returned pulse: 100’s – 10,000’s on
detector’s active area
• Repetition frequency: kHz - MHz
• DC photon background
35
Photodetector requirements
• High quantum efficiency at 905 nm and/or 1550 nm (affects
detection range)
• High detector (intrinsic) gain (reduces importance of electronic noise)
• Small excess noise (affects timing error)
• Small time jitter (affects distance resolution)
APD has been a default detector. Could SiPM be a better choice?
36
Photosensitivity
Wavelength [nm]
Photon
detection
efficiency
[%]
Wavelength [nm]
Quantum
efficiency
[%]
S10341 Si APD
S13720 SiPM
37
Intrinsic gain
Overvoltage [V]
Gain
S13720 SiPM
Reverse voltage [V]
S10341 Si APD
Gain 38
Excess noise
Overvoltage [V]
Crosstalk
probability
[%]
F ≈ 1+PCT = 1.06
S13720 SiPM
Gain
Excess
noise
factor
S10341 Si APD
F ≈ (Gain)0.3 = 3.2 for gain = 50
39
Time jitter
There are two contributions to timing jitter:
1. “Classical” jitter – variation in response time, often reported for
a single photon illumination. This contribution is on the order of
100 ps for SiPMs and APDs
2. Time-walk effect. For a constant trigger level, timing depends
gain variation and signal intensity.
40
Time jitter
time
arb.
trig. level
Different trigger times:
time walk effect
For a given light level SiPM has
smaller time-walk effect because
of its lower excess noise.
41
Take-away points
1. SiPMs are likely to compete successfully with APDs at 905 nm
because of their higher gain and much lower excess noise.
Empirical evidence is forthcoming.
2. Sensitivity at 905 nm will improve in a new generation SiPMs
3. SiPMs with sensitivity at 1550 nm are being developed.
42
Flow cytometry
Studying biological cells with light
43
Flow cytometry (basic concept)
Laser
Forward-scatter
photodetector
Side-scatter photodetector
Data processing
flow
flow
44
Flow cytometry
Excitation light
Fluorescent
light
cell
fluorescent dye
Flow cytometry also uses fluorescence tagging to study cells
45
Flow cytometry
• Used to study and sort biological cells
• Side-scatter signal vs. forward scatter signal depends on cell
properties
• Fluorescence is also employed (dyes attached to cells) to
produce a variety of plots using fluorescence signal(s)
• The optical system employs a combination of lasers (different
wavelengths), optical filters, and photodetectors
46
Flow cytometry data
Forward scatter signal
Side
scatter
signal
Side scatter vs. forward scatter plot – the
most fundamental in flow cytometry
Cell’s characteristics such as size,
complexity, or refractive index affect the
relative strengths of side scatter and
forward scatter signals
47
Characteristics of received light
• Wavelength: can be selected depending on cell sizes and
fluoresce
• Pulses − duration dependent on sheath flow speed and cell size
and is on the order of μs.
• No. of photons per pulse varies from few to thousands
• Rate of pulses in kHz
48
Side-scatter photodetector requirements
• High photodetection efficiency (affects S/N of detection)
• High dynamic range (affects accuracy of the scatter plot; systematic errors)
• High intrinsic gain (reduces importance of electronic noise)
• Minimal excess noise (affects accuracy of the scatter plots; random noise)
• High linearity (affects accuracy of the scatter plot; systematic errors)
PMT is commonly used. Could SiPM be a better choice?
49
Photosensitivity
S13360
3×3 mm2, 25 μm
14,400 microcells
Wavelength [nm]
PDE
[%]
Wavelength [nm]
Cathode
radiant
sensitivity
[mA/W]
H10720
QE ≈ 28%
at 450 nm
50
Gain
Gain
Overvoltage [V]
14,400 μcells
S13360
3×3 mm2, 25 μm
Gain
Control voltage [V]
H10720
51
Excess Noise
F ≈ 1+PCT (SiPM)
F ≈ δ/(δ – 1) (PMT; δ – gain of the first dynode )
Excess noise increases with gain
Excess noise decreases with gain
52
Linearity/dynamic range (PMT)
Output current [mA]
Deviation
[%]
H10720 10% nonlinearity: 75 mA, TP = 500 ns
Gain = 2×106, QE = 28%
No. of incident photons at 450 nm:
4.2×105
53
Linearity/dynamic range (SiPM)
Ntot = 14,400; PDE = 25%, tr = 50 ns
Nγ
.PDE = 1.1×105 (ideal response)
Nfired = 0.75×105 or 32% below an ideal response
54
Take-away points
1. The major weakness of SiPMs in flow cytometry is limited
dynamic range and linearity
2. However, out of dozens of optical channels in a flow cytometer,
SIPM can be suitable for some
3. There is a great interest in using SiPMs in flow cytometry but
little published work on this subject exists
55
Radiation monitoring and spectroscopy
56
Radiation monitoring (basic idea)
Scintillator Photodetector
Ionizing
radiation
time
Output
trigger level
radiation events
An event is registered if the output signal exceeds the threshold
level.
57
Radiation monitoring (basic idea)
Amplifier Discriminator Counter
• Used to detect the presence of specific radiation
• Monitoring devices are often portable and hand-held.
• Information provided: radiation rate (flux can be derived)
1,2,3…
58
Characteristics of received light
• Wavelength dependent on the choice of scintillator often in the
300 nm – 500 nm range
• Pulses
• Number of photons per pulse depends on energy of ionizing
radiation and type of scintillator
• Duration of the pulse depends on the size and type of the
scintillator (decay time constants range from ns to μs)
• Frequency of pulses depends on the rate of incoming radiation
59
Photodetector requirements
• High photodetection efficiency
• High intrinsic gain
• Ability to couple to a scintillator
• Suitable for portable hand-held devices
• Large active area
60
Radiation spectroscopy
Scintillator Photodetector
Ionizing
radiation
C
R
Charge integrator
61
Radiation spectroscopy (basic idea)
V/V
Discriminator
A/D
Computer
Charge
integrator
Energy
No.
of
events
Resolution =
FWHM
E
FWHM
E
Resolution is affected by the
properties of the photodetector
and the scintillator.
62
Photodetector requirements
• High photodetection efficiency (affects S/N of the detection and thus
resolution)
• High intrinsic gain (reduces the importance of electronic noise and, thus,
better count rate and measurable lower energy levels)
• Ability to couple to a scintillator
• Low excess noise (affects energy resolution)
• High linearity (affects systematic errors and energy range)
63
Radiation detection photodetectors
PMTs used to dominate the detector choice in radiation detection,
monitoring, and spectroscopy.
SiPMs are becoming a viable alternative.
Due to a multitude of possible detection scenarios, it is best to
perform a side-by-side comparison between an SiPM and a PMT.
64
SiPM vs. PMT in γ-ray detection
SiPM PMT
Energy [MeV] Energy [MeV]
Number
of
counts
Number
of
counts
Example of energy spectra from Grodzicka et al. 2017 [Nuclear Inst. and Methods in
Physics Research, A 874 (2017) 137–148]
65
SiPM vs. PMT in γ-ray detection
SiPM – PMT comparison for different energies and scintillators from
Grodzicka et al. 2017 [Nuclear Inst. and Methods in Physics Research, A 874 (2017) 137–148]
66
Take-away points
1. SiPMs provide comparable performance to PMTs in radiation
monitoring and spectroscopy
2. It is likely that the majority of hand-held devices will employ
SiPMs
3. Side-by-side comparison is the best approach in deciding if an
SiPM or a PMT should be used for a given detection application
67
Summary and conclusions
• High gain, low excess noise, magnetic immunity, and ease of
use are some of the highly desirable characteristics of SiPMs
• There is a great interest in using SiPMs instead of APDs and
PMTs in a variety of applications
• New generation SiPMs will have improved characteristics
making the transition more likely
68
Visit Booth #521 & Presentations at PW18
Development of an InGaAs SPAD 2D array for Flash LIDAR
Presentation by Takashi Baba, January 29, 2018 (11:00 AM - 11:30 AM)
Development of an InGaAs MPPC for NIR photon counting applications
Presentation by Yusei Tamura, January 30, 2018 (5:50 PM - 6:10 PM)
Photodetectors, Raman Spectroscopy, and SiPMs versus PMTs
One-day Workshop with Slawomir Piatek, January 31, 2018 (8:30 AM - 5:30 PM) – Free Registration Needed
Development of a Silicon hybrid SPAD 1D array for LIDAR and spectrometers
Poster session with Shunsuke Adachi, January 31, 2018 (6:00 PM - 8:00 PM)
69
Thank you for listening!
Slawomir Piatek
piatek@njit.edu
70

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foto multiplicador de silicio

  • 1. Silicon Photomultiplier Slawomir Piatek Technical Consultant, Hamamatsu Corp. Operation, Performance & Possible Applications
  • 2. Introduction Very high intrinsic gain together with minimal excess noise make silicon photomultiplier (SiPM) a possible choice of a photodetector in those applications where the input light is in the photon-counting range. 2
  • 3. Introduction This webinar is a high-level review of SiPM’s structure, operation, and opto-electronic characteristics, followed by a discussion of some possible applications. 3
  • 4. Outline • Structure and operation • Opto-electronic characteristics • Applications + Automotive ToF LiDAR + Flow cytometry + Radiation detection and monitoring • Summary and conclusions 4
  • 5. SiPM Structure and Operation of a SiPM Portraits of SiPMs (images not to scale) 5
  • 6. SiPM structure SiPM is an array of microcells = APD RQ p+ π n+ p+ oxide Single microcell electrical equivalent circuit of a microcell Side view Top view 6
  • 7. SiPM structure ... Anode Cathode single microcell RQ APD All of the microcells are connected in parallel 7
  • 8. SiPM specifications Active area: 1.3×1.3 − 6×6 mm2 Microcell size (pitch): 10×10, 15×15, 25×25, 50×50, 75×75 μm2 Number of microcells: (active area)/(microcell size), from 100’s to 10,000’s Overvoltage: ΔV = VBIAS – VBD; recommended by the manufacturer 8
  • 9. SiPM operation VBIAS > VBD K A × G RL time [ns] Amplitude [mV] Example of single-photoelectron waveform (1 p.e.) Gain = area under the curve in electrons 9
  • 10. SiPM operation time [ns] Amplitude [mV] Fast component Slow component RC time constant of the slow component depends on microcell size (all else being equal) Recovery time tR ≈ 5 times the RC time constant tR is on the order of 10’s to 100’s ns but in practical situations, it is also a function of detection bandwidth 10
  • 11. SiPM operation time Arb. The output of an SiPM is a chronological superposition of current pulses Current pulses due to photons SiPM also outputs current pulses even in absence of light: dark counts (dark current) 11
  • 12. Dark Counts time Arb. Dark-count pulses are indistinguishable from those due to photons The rate of dark counts depends on overvoltage, temperature, and size of the active area Current pulses due to photons and dark counts are indistinguishable 12
  • 13. Crosstalk Primary discharge can trigger a secondary discharge in neighboring microcells. This is crosstalk. time Arb. 2 p.e. crosstalk event Crosstalk probability depends on overvoltage 13
  • 14. Operation VBIAS 1, 2, 3,…. VBIAS If the pulses are distinguishable, SiPM can be operated in a photon counting mode. If the pulses overlap, the SiPM can be operated in an analog mode. The measured output is voltage or current. counter SiPM V or I 0 100 light 14
  • 17. Characteristics of a SiPM • Photon detection efficiency • Gain • Crosstalk probability • Dark current & dark counts • Linearity & dynamic range • Temperature effects 17
  • 18. Photon detection efficiency wavelength [nm] Photon detection efficiency [%] • Photon detection efficiency (PDE) is a probability that an incident photon is detected. It depends on: - wavelength - overvoltage - microcell size Peak PDE 20% − 50% 18
  • 19. Photon detection efficiency wavelength [nm] Photon detection efficiency [%] 5 10 15 20 25 30 Examples of PDE curves for SiPMs optimized for NIR, VIS, and UV response. 19
  • 20. Gain Overvoltage [V] Crosstalk prob. & PDE • Gain of SiPM is comparable to that of a PMT. Excess noise very low: F ~ 1.1, mostly due to crosstalk Gain S13720, 1.3×1.3 mm2 • Gain depends linearly on overvoltage 25 μm 20
  • 21. Gain versus temperature Does gain of an SiPM depend on temperature? Yes – if the bias voltage is fixed Reverse bias voltage [V] Gain [×10 6 ] Otte et al. (2016) 21
  • 22. Gain versus temperature Does gain of an SiPM depend on temperature? No – if the overvoltage is fixed Temperature [°C] Gain variation [%] Fixed overvoltage 22
  • 23. Crosstalk Overvoltage [V] Crosstalk prob. & PDE PCT increases with overvoltage Crosstalk is the main contributor to excess noise F ≈ (1+PCT) S13720, 1.3×1.3 mm2 25 μm 23
  • 24. Dark Current Overvoltage [V] Dark current [A] S13720, 1.3×1.3 mm2 Example of dark current versus overvoltage DCR = ID/eμ ID = 1×10-7 A (at 7 V) μ = 1.2×106 (at 7 V) -> DCR ≈ 520 kHz or once per about 2 μs 25 μm 24
  • 25. Linearity and dynamic range Incident light level (850 nm) [W] Output current [A] S13720, 1.3×1.3 mm2 Example of output current versus incident light level. Photon irradiance (at 850 nm) = 4.3×1018×P[W] P = 10-8 W −> 4.3×1010 photons per second Linearity depends on the number of microcells for a given active area 25 μm 25
  • 26. SiPM, PMT & APD This webinar will compare and contrast SiPM with a photomultiplier tube (PMT) and APD. Let’s briefly review the operation of a PMT and APD Examples of a PMT (left) and APD (right). 26
  • 27. Operation of a PMT R1 R2 R3 R4 R5 R6 R7 C1 C2 C3 K P D1 D2 D3 D4 D5 D6 V ~ 1000 V e− Rf IP IK 2 ns/div 100 mV/div Typical voltage divider 27
  • 28. SiPM versus PMT • Solid state versus vacuum tube technology • Comparable gains • Comparable excess noise • Dark count rate per unit active area larger in SiPM • E & B field immunity in SiPM • Comparable photosensitivity in the spectral overlap region • Greater optimization for PMTs 28
  • 29. Operation of an APD self-quenching avalanche VBIAS RL electrons holes IPH APD biased below breakdown voltage Single photon can lead up to about 100 of electron-hole pairs Avalanche is self-quenching Thus gain up to ~100 photon 29
  • 30. SiPM versus APD log(Gain) Gain = 1 linear region Geiger region VBIAS VBD APDs SiPMs • Differ in construction • GainSiPM >> GainAPD • FSiPM << FAPD 30
  • 31. Possible applications of SiPMs • Flow cytometry • Automotive time-of-flight LiDAR • Radiation detection and monitoring 31
  • 32. Automotive time-of-flight LiDAR How far is this tree? LiDAR LiDAR = Light Detection and Ranging 32
  • 33. Automotive ToF LiDAR: basic concept to target emitted pulse “start” pulse “stop” pulse emission optics timer collection optics laser returned pulse after Δt beam splitter w = cτ “fast” photodetector 33
  • 34. Automotive ToF LiDAR: basic concept Measure round-trip time-of-flight Δt Range (distance to the reflection point) = cΔt/2; here c is the speed of light By scanning the surroundings, a 3D map can be constructed 34
  • 35. Characteristics of received light • Wavelength: 905 nm or 1550 nm • Pulse: duration 2 – 5 ns • No. of photons per returned pulse: 100’s – 10,000’s on detector’s active area • Repetition frequency: kHz - MHz • DC photon background 35
  • 36. Photodetector requirements • High quantum efficiency at 905 nm and/or 1550 nm (affects detection range) • High detector (intrinsic) gain (reduces importance of electronic noise) • Small excess noise (affects timing error) • Small time jitter (affects distance resolution) APD has been a default detector. Could SiPM be a better choice? 36
  • 38. Intrinsic gain Overvoltage [V] Gain S13720 SiPM Reverse voltage [V] S10341 Si APD Gain 38
  • 39. Excess noise Overvoltage [V] Crosstalk probability [%] F ≈ 1+PCT = 1.06 S13720 SiPM Gain Excess noise factor S10341 Si APD F ≈ (Gain)0.3 = 3.2 for gain = 50 39
  • 40. Time jitter There are two contributions to timing jitter: 1. “Classical” jitter – variation in response time, often reported for a single photon illumination. This contribution is on the order of 100 ps for SiPMs and APDs 2. Time-walk effect. For a constant trigger level, timing depends gain variation and signal intensity. 40
  • 41. Time jitter time arb. trig. level Different trigger times: time walk effect For a given light level SiPM has smaller time-walk effect because of its lower excess noise. 41
  • 42. Take-away points 1. SiPMs are likely to compete successfully with APDs at 905 nm because of their higher gain and much lower excess noise. Empirical evidence is forthcoming. 2. Sensitivity at 905 nm will improve in a new generation SiPMs 3. SiPMs with sensitivity at 1550 nm are being developed. 42
  • 43. Flow cytometry Studying biological cells with light 43
  • 44. Flow cytometry (basic concept) Laser Forward-scatter photodetector Side-scatter photodetector Data processing flow flow 44
  • 45. Flow cytometry Excitation light Fluorescent light cell fluorescent dye Flow cytometry also uses fluorescence tagging to study cells 45
  • 46. Flow cytometry • Used to study and sort biological cells • Side-scatter signal vs. forward scatter signal depends on cell properties • Fluorescence is also employed (dyes attached to cells) to produce a variety of plots using fluorescence signal(s) • The optical system employs a combination of lasers (different wavelengths), optical filters, and photodetectors 46
  • 47. Flow cytometry data Forward scatter signal Side scatter signal Side scatter vs. forward scatter plot – the most fundamental in flow cytometry Cell’s characteristics such as size, complexity, or refractive index affect the relative strengths of side scatter and forward scatter signals 47
  • 48. Characteristics of received light • Wavelength: can be selected depending on cell sizes and fluoresce • Pulses − duration dependent on sheath flow speed and cell size and is on the order of μs. • No. of photons per pulse varies from few to thousands • Rate of pulses in kHz 48
  • 49. Side-scatter photodetector requirements • High photodetection efficiency (affects S/N of detection) • High dynamic range (affects accuracy of the scatter plot; systematic errors) • High intrinsic gain (reduces importance of electronic noise) • Minimal excess noise (affects accuracy of the scatter plots; random noise) • High linearity (affects accuracy of the scatter plot; systematic errors) PMT is commonly used. Could SiPM be a better choice? 49
  • 50. Photosensitivity S13360 3×3 mm2, 25 μm 14,400 microcells Wavelength [nm] PDE [%] Wavelength [nm] Cathode radiant sensitivity [mA/W] H10720 QE ≈ 28% at 450 nm 50
  • 51. Gain Gain Overvoltage [V] 14,400 μcells S13360 3×3 mm2, 25 μm Gain Control voltage [V] H10720 51
  • 52. Excess Noise F ≈ 1+PCT (SiPM) F ≈ δ/(δ – 1) (PMT; δ – gain of the first dynode ) Excess noise increases with gain Excess noise decreases with gain 52
  • 53. Linearity/dynamic range (PMT) Output current [mA] Deviation [%] H10720 10% nonlinearity: 75 mA, TP = 500 ns Gain = 2×106, QE = 28% No. of incident photons at 450 nm: 4.2×105 53
  • 54. Linearity/dynamic range (SiPM) Ntot = 14,400; PDE = 25%, tr = 50 ns Nγ .PDE = 1.1×105 (ideal response) Nfired = 0.75×105 or 32% below an ideal response 54
  • 55. Take-away points 1. The major weakness of SiPMs in flow cytometry is limited dynamic range and linearity 2. However, out of dozens of optical channels in a flow cytometer, SIPM can be suitable for some 3. There is a great interest in using SiPMs in flow cytometry but little published work on this subject exists 55
  • 56. Radiation monitoring and spectroscopy 56
  • 57. Radiation monitoring (basic idea) Scintillator Photodetector Ionizing radiation time Output trigger level radiation events An event is registered if the output signal exceeds the threshold level. 57
  • 58. Radiation monitoring (basic idea) Amplifier Discriminator Counter • Used to detect the presence of specific radiation • Monitoring devices are often portable and hand-held. • Information provided: radiation rate (flux can be derived) 1,2,3… 58
  • 59. Characteristics of received light • Wavelength dependent on the choice of scintillator often in the 300 nm – 500 nm range • Pulses • Number of photons per pulse depends on energy of ionizing radiation and type of scintillator • Duration of the pulse depends on the size and type of the scintillator (decay time constants range from ns to μs) • Frequency of pulses depends on the rate of incoming radiation 59
  • 60. Photodetector requirements • High photodetection efficiency • High intrinsic gain • Ability to couple to a scintillator • Suitable for portable hand-held devices • Large active area 60
  • 62. Radiation spectroscopy (basic idea) V/V Discriminator A/D Computer Charge integrator Energy No. of events Resolution = FWHM E FWHM E Resolution is affected by the properties of the photodetector and the scintillator. 62
  • 63. Photodetector requirements • High photodetection efficiency (affects S/N of the detection and thus resolution) • High intrinsic gain (reduces the importance of electronic noise and, thus, better count rate and measurable lower energy levels) • Ability to couple to a scintillator • Low excess noise (affects energy resolution) • High linearity (affects systematic errors and energy range) 63
  • 64. Radiation detection photodetectors PMTs used to dominate the detector choice in radiation detection, monitoring, and spectroscopy. SiPMs are becoming a viable alternative. Due to a multitude of possible detection scenarios, it is best to perform a side-by-side comparison between an SiPM and a PMT. 64
  • 65. SiPM vs. PMT in γ-ray detection SiPM PMT Energy [MeV] Energy [MeV] Number of counts Number of counts Example of energy spectra from Grodzicka et al. 2017 [Nuclear Inst. and Methods in Physics Research, A 874 (2017) 137–148] 65
  • 66. SiPM vs. PMT in γ-ray detection SiPM – PMT comparison for different energies and scintillators from Grodzicka et al. 2017 [Nuclear Inst. and Methods in Physics Research, A 874 (2017) 137–148] 66
  • 67. Take-away points 1. SiPMs provide comparable performance to PMTs in radiation monitoring and spectroscopy 2. It is likely that the majority of hand-held devices will employ SiPMs 3. Side-by-side comparison is the best approach in deciding if an SiPM or a PMT should be used for a given detection application 67
  • 68. Summary and conclusions • High gain, low excess noise, magnetic immunity, and ease of use are some of the highly desirable characteristics of SiPMs • There is a great interest in using SiPMs instead of APDs and PMTs in a variety of applications • New generation SiPMs will have improved characteristics making the transition more likely 68
  • 69. Visit Booth #521 & Presentations at PW18 Development of an InGaAs SPAD 2D array for Flash LIDAR Presentation by Takashi Baba, January 29, 2018 (11:00 AM - 11:30 AM) Development of an InGaAs MPPC for NIR photon counting applications Presentation by Yusei Tamura, January 30, 2018 (5:50 PM - 6:10 PM) Photodetectors, Raman Spectroscopy, and SiPMs versus PMTs One-day Workshop with Slawomir Piatek, January 31, 2018 (8:30 AM - 5:30 PM) – Free Registration Needed Development of a Silicon hybrid SPAD 1D array for LIDAR and spectrometers Poster session with Shunsuke Adachi, January 31, 2018 (6:00 PM - 8:00 PM) 69
  • 70. Thank you for listening! Slawomir Piatek piatek@njit.edu 70