CU2Se

1. Anchor Scan Parameters
Dataset Name: 6
File name: D:xrd data-14th Jan 166.rd
Comment: Configuration=Stage for flat samples, Ow
Goniometer=Theta/Theta; Minimum step siz
Measurement Date / Time: 13-01-2016 16:40:00
Raw Data Origin: PHILIPS-binary (scan) (.RD)
Scan Axis: Gonio
Start Position [°2Th.]: 10.0234
End Position [°2Th.]: 89.9734
Step Size [°2Th.]: 0.0260
Scan Step Time [s]: 17.1808
Scan Type: Continuous
Offset [°2Th.]: 0.0000
Divergence Slit Type: Fixed
Divergence Slit Size [°]: 0.5000
Specimen Length [mm]: 10.00
Receiving Slit Size [mm]: 12.7500
Measurement Temperature [°C]: -273.15
Anode Material: Cu
K-Alpha1 [Å]: 1.54060
K-Alpha2 [Å]: 1.54443
K-Beta [Å]: 1.39225
K-A2 / K-A1 Ratio: 0.50000
Generator Settings: 40 mA, 45 kV
Diffractometer Type: XPert MPD
Diffractometer Number: 1
Goniometer Radius [mm]: 200.00
Dist. Focus-Diverg. Slit [mm]: 91.00
Incident Beam Monochromator: No
Spinning: No
Graphics

2. Peak List
Pos.[°2Th.] Height[cts] FWHM[°2Th.] d-spacing[Å] Rel.Int.[%]
26.6031 333.79 0.2047 3.35080 6.14
28.2698 1640.22 0.2558 3.15691 30.17
29.0065 404.00 0.1535 3.07839 7.43
29.3636 1681.00 0.1535 3.04176 30.92
29.9216 503.76 0.1279 2.98630 9.27
30.4985 266.55 0.2558 2.93111 4.90
31.4008 5437.14 0.1791 2.84892 100.00
32.8893 1038.75 0.1535 2.72331 19.10
33.3190 397.23 0.1279 2.68916 7.31
34.1738 1302.63 0.1535 2.62382 23.96
36.1040 1063.95 0.1535 2.48786 19.57
38.8667 178.78 0.1535 2.31714 3.29
41.9492 319.33 0.2047 2.15373 5.87
45.5700 415.99 0.1535 1.99068 7.65
46.0210 1177.14 0.1791 1.97221 21.65
46.6917 362.67 0.2047 1.94544 6.67
48.0750 561.56 0.1535 1.89264 10.33
49.5522 809.74 0.1023 1.83962 14.89
50.2527 1847.00 0.2047 1.81561 33.97
53.0712 199.57 0.1535 1.72564 3.67
54.1727 506.32 0.0768 1.69313 9.31
56.0248 285.52 0.1279 1.64147 5.25
56.3888 693.36 0.0768 1.63173 12.75
57.1361 273.48 0.2047 1.61216 5.03
57.9907 110.29 0.3070 1.59042 2.03

3. 60.7299 169.48 0.3070 1.52508 3.12
65.2787 86.90 0.8187 1.42938 1.60
70.6129 210.56 0.5117 1.33392 3.87
71.6891 112.05 0.4093 1.31652 2.06
78.3408 105.56 0.3070 1.22055 1.94
81.9079 311.47 0.0936 1.17522 5.73
83.7497 360.73 0.2047 1.15495 6.63
85.6149 81.02 0.3070 1.13450 1.49
87.8483 101.84 0.7488 1.11041 1.87
Pattern List
Visible Ref.Code Score Compound Name Displ.[°2Th]
Scale Fac. Chem. Formula
* 00-012-0115 49 Copper Selenide 0.000
0.080 Cu Se2
* 00-020-1020 33 Copper Selenide 0.000
0.163 Cu Se
* 00-024-0376 26 Copper Selenide Su.. 0.000
0.185 Cu2 S Se
Document History
Insert Measurement:
- File name = 6.rd
- Modification time = "28-01-2016 12:41:09"
- Modification editor = "Guest"
Interpolate Step Size:
- Step Size = "Derived"
- Modification time = "01-11-2004"
- Modification editor = "PANalytical"
Determine Background:
- Correction method = "Automatic"
- Bending factor = "5"
- Use smoothed input data = "Yes"
- Granularity = "20"
- Add to net scan = "Nothing"
- Modification time = "22-02-2001 10:17:43"
- Modification editor = "PANalytical"
Search Peaks:
- Minimum significance = "2.00"
- Minimum tip width = "0.01"
- Maximum tip width = "1.00"
- Peak base width = "2.00"
- Method = "Minimum 2nd derivative"
- Modification time = "20-02-2001 11:55:18"
- Modification editor = "PANalytical"
Search & Match:
- Data source = "Profile and peak list"
- Restriction = "Restriction set"
- Description = "Default - All ref. patterns possible"
- All of: elements = ""
- At least one of: elements = "Cu, Zn, Se, Sn"
- None of: elements = ""

4. - Maximum no. of elements = "105"
- Skip marked as deleted by ICDD = "No"
- Skip marked as deleted by a user = "No"
- Skip non ambient pressure = "No"
- Skip non ambient temperature = "No"
- Quality marks set = ""
- Subfiles = ""
- Scoring schema = "Multi phase"
- Auto residue = "Yes"
- Match intensity = "Yes"
- Demote unmatched strong = "Yes"
- Allow pattern shift = "No"
- Two theta shift = "0"
- Identify = "No"
- Modification time = "28-01-2016 12:42:47"
- Modification editor = "Guest"