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Analysis of Nitrosodiethylamin and Nitrosodiprophylamin in Sausage using Single Drop Microextraction Coupled with GC Zarah Nur Intissar (080710150) ,[object Object],[object Object],[object Object]
[object Object],CHAPTER I
BACKGROUND Food Preservative Nitrite Carcinogen Nitrosamine Nitrosodiethylamine (NDEA) Nitrosodiprophylamine (NDPA) Sausage
BACKGROUND Nitrosamine Low Concentration ( ppb ) Sample preparation (extraction) Single Drop Microextraction (SDME) Direct-SDME Headspace-SDME
PROBLEMS OF RESEARCH ,[object Object],[object Object],[object Object]
OBJECTIVE OF RESEARCH ,[object Object],[object Object],[object Object]
BENEFIT OF RESEARCH To produce a new method to the analysis NDEA and NDPA quickly, selective and cheap in sausage. To know the concentration of nitrosamine in sausage so that we can anticipation for the negative effect from nitrosamine.
[object Object],Tinjauan Pustaka
[object Object],[object Object],[object Object],Nitrosamin ,[object Object],[object Object],[object Object],Sosis
Single-Drop Microextraction (SDME) Direct-SDME Headspace-SDME (HS-SDME) Drop pelarut organik di rendam langsung di dalam larutan sampel Drop pelarut organik di letakkan di atas larutan sampel (menggantung)
Gas Chromatography (GC) Jenis kromatografi untuk memisahkan dan menganalisa campuran zat Komponen instrumen kromatografi gas
[object Object],Metode Penelitian
ALAT DAN BAHAN PENELITIAN ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
SKEMA KERJA
Proses Ekstraksi HS-SDME Syringe berisi pelarut organik Jarum syringe Larutan pengekstraksi (drop pelarut organik) Pengaduk magnetik Larutan Standar/sampel Setelah proses ekstraksi selesai, pelarut organik ditarik ke dalam syringe  kemudian diinjeksikan ke GC Botol kaca Penutup
 

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HS-SDME

  • 1.
  • 2.
  • 3. BACKGROUND Food Preservative Nitrite Carcinogen Nitrosamine Nitrosodiethylamine (NDEA) Nitrosodiprophylamine (NDPA) Sausage
  • 4. BACKGROUND Nitrosamine Low Concentration ( ppb ) Sample preparation (extraction) Single Drop Microextraction (SDME) Direct-SDME Headspace-SDME
  • 5.
  • 6.
  • 7. BENEFIT OF RESEARCH To produce a new method to the analysis NDEA and NDPA quickly, selective and cheap in sausage. To know the concentration of nitrosamine in sausage so that we can anticipation for the negative effect from nitrosamine.
  • 8.
  • 9.
  • 10. Single-Drop Microextraction (SDME) Direct-SDME Headspace-SDME (HS-SDME) Drop pelarut organik di rendam langsung di dalam larutan sampel Drop pelarut organik di letakkan di atas larutan sampel (menggantung)
  • 11. Gas Chromatography (GC) Jenis kromatografi untuk memisahkan dan menganalisa campuran zat Komponen instrumen kromatografi gas
  • 12.
  • 13.
  • 15. Proses Ekstraksi HS-SDME Syringe berisi pelarut organik Jarum syringe Larutan pengekstraksi (drop pelarut organik) Pengaduk magnetik Larutan Standar/sampel Setelah proses ekstraksi selesai, pelarut organik ditarik ke dalam syringe kemudian diinjeksikan ke GC Botol kaca Penutup
  • 16.