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고온고압반응기 인포그래픽(국문)-일신오토클레이브
- 1. 고온·고압의 환경에서 화학합성, 분해,승화 및 추출 등의 많은 연구를 수행할 수 있는 연구용 반응기입니다.
온도, 압력, 용량 선정이 가능하며, 반응조건에 따라 다양한 옵션선택이 가능합니다.
HIGH PRESSURE REACTOR
Magnedrive
Seal type
(O-ring/gasket)
Port(Inlet/Outlet)
Thermocouple
Pressure Vessel
Liner
압력(kg/㎠)
온도(℃)
용량(ℓ)
Hydrothermal Synthesis of Zeolite (ZSM-5) Hydrothermal Synthesis of ZrO2 Nanoparticles
Hydrothermal Synthesis of Amorphous SiO2 Hydrothermal Synthesis of MnO2 Nanorod
BET Surface Area: 186 m2
∙g-1
SEM (Size & Morphology) XRD (Crystal Structure)
Zirconia NanoparticlesH S
NH4OH Solution
10 20 30 40 50 60 70 80 90
Intensity(arb.unit)
2 Theta (degree)
KMnO4
Solution
Mn(CH3COOH)2
Solution
XRD (Crystal Structure)SEM (Size & Morphology)
Cal. 300-500 ℃ for 2h
10 20 30 40 50 60
Intensity(arb.unit)
2 Theta (degree)
M
SIO2
A12O2
H20
MOH(F)
SI-O, AI-O boundsMordenite(MOR) Rho(RHO) UZM-5(UFI) SSZ-13, SAPO-34(CHA)
200
150
100
50
0
0.0 0.2 0.4 0.6 0.8 1.0
P/P0
Adsorption
Desorption
VolumeAdsorbed(cm3
g-1
,STP)
PoreVolume(cm3g-1nm-1)
0.60
0.45
0.30
0.15
0.00
1 10010
Pore Width / nm
BET Surface Area TEM (Size & Morphology)
Ref. Journal of Colloid and Interface Science 350 (2010) 290–294
Hydrothermal
XRD (Crystal Structure)
Amorphous SiO2
M OR HOH ROHOH
Hydrolysis
Reesterification
M+ +
M OH OH HOHO
Water
Condensation
Hydrolysis
M M M+ +
M OH OR ROHO
Alcohol
Condensation
Alcoholysis
M M M+ +
10 20 30 40 50 60 70 80 90
Intesity(arb.unit)
2 Theta (degree)
AFM (Size & Morphology)
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