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FULL HD PLASTIC ™ REPORT
ΔL Δa Δ
20462
22% 82%
278%
Volume cavity (µm3
)
Note: L* = 0 yields black and L* = 100 indicates diffuse white. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values
indicate yellow. ΔE> , usual olor toleran e.
Roughness profile - Conventional VS Roctool Technology
T=160°C - Roctool - WITHT=90°C - Conventional - WITHOUT
PICTURES OF INJECTED SAMPLES
3D TEXTURATION RESULTS
T=80°C - Conventional - WITHOUT T=160°C - Roctool - WITH
Conventional (µm3
) Roctool technology (µm3
) Improvement (%)Roughness parameters
5416
Rate replication from the mold surface (%)
DC0041PQ
DATE
DELTACOLOR SCALE
L* ( Lightness)
MEASUREMENTS
PROCESS TECHNOLOGY
-0,01
T=160°C - Roctool - WITH
SUPPLIER SABIC
0,19
ΔE
COLOR
DIFFERENCE
LAB - COLOR DEPHT RESULTS (DIN 5033 Standard)
0,03
T=80°C - Conventional - WITHOUT
28,85 -0,04 -0,39
28,66
a*
-0,05
b*
-0,36
Rev.: A
GLOSS RESULTS (ISO 2813 Standard)
T=80°C - Conventional - WITHOUT 21,7 102,6T=160°C - Roctool - WITH
TRADE NAME
-0,19
17/01/2018 TRIAL # HDP-17-023 MOLD HD PLAQUE
MATERIAL
FAMILY PC
FORM
FOR-TEC-111
Page 1 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
LNP™ THERMOCOMP™ COMPOUND GRADE
COMMENTS
1,00
Quality surface characterization:
1) Visible improvements using Roctool technology are observed: weld line and sink marks are removed. Glass fibers and defects are removed from
the surface.
2) Significant improvement on the gloss value up to 365%. However, we measured a slight impact of the mold temperature on the color perception.
However the surface finish with Roctool is drastically improved with high level of gloss compared to conventional process.
3) The different textured areas hightlight the positive impact on the replication using Roctool technology. The different roughnesses are well felt
when touched. The roughness measurement carried out using optical rugosimeter confirms the above with repliction rate of up to 82% : an
improvement of 278% with Roctool compared to conventional technology (CIM).
Also, the Rz value has been carried out and shows the positive impact of Roctool with an important reduction of the roughness on high gloss surface
due to the elimination of glass fibers at the surface.
FORM
FOR-TEC-111 Rev.: A
Page 2 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
2,461,56
TEXTURE RESULTS - Ra (Amplitude roughness parameter)
Roctool technology 160°C
VDI 18 (Ra=±0.80 µm) VDI 22 (Ra=±1.26 µm) VDI 27 (Ra=±2.20 µm)
TEXTURE RESULTS - Rz (Mean roughness depth)
Roughness parameters Conventional (80°C) Roctool technology (160°C) Improvement (%)
CHEMICAL 1,12 1,76 2,91 Ra (µm)
EDM 0,97 1,18 2,09 Ra (µm)
Rz (µm) 7,05 2,01 -71%
T=80°C - Conventional - WITHOUT T=160°C - Roctool - WITH
LASER Ra (µm)
Note: In conventional molding, the measurements of the VDI roughness are not mentionned as the presence of glass fibers on the surface disturb the measurement impacting the Ra value.
GLOSS PRINCIPLE
FORM
FOR-TEC-111 Rev.: A
Page 3 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
ANNEXES
MEASUREMENT AREAS
1) The high gloss area framed in blue is the measurement area for the gloss,
color and specific roughness Rz* .
2) The red rectangle define the nano-replication area.
3) The green box correspond to the multi-textured (VDI) area were the
roughness is measured.
*Rz: Maximal amplitude roughness mesured for filled materials
ROUGHNESS MEASUREMENT PRINCIPLE
Optical rugosimeter is a measuring instrument used to measure a surface's
profile, in order to quantify its roughness.
In the context of HD Plastics™, two information are carried out using Alicona
equipment according to the standard ISO 4287:
- Replication rate : volume of the specific texture defined versus the one
textured on the mold surface quavity
- The surface roughness parameters : Arithmetical mean deviation (Ra) which
evaluate the roughness amplitude on a profile and Mean roughness depth
(Rz) which measure the maximal amplitude roughness average of the profile.
LAB COLOR PRINCIPLE
The Lab color space describes all perceivable colors in the three dimensions L
for lightness and a and for the olor opponents green–red and lue– ello .
In the context of HD Plastics™, a spectrophotometer is used to carried out
the LAB alue : spe tro-guide / gloss BYK . HD Plasti s™ is follo ing the
DIN 5033 Standard.
The graph shows the LAB color scale. The lightness, L*, represents the
darkest black at L* = 0, and the brightest white at L* = 100. The a* and b*
value represent the color channels. a*: negative values indicate green while
positive values indicate red. b*: negative values indicate blue and positive
values indicate yellow
Gloss is an optical property which indicates how well a surface reflects light
in a specular direction. It is one of important parameters that are used to
describe the visual appearance of an object. The factors that affect gloss are
the refractive index of the material, the angle of incident light and the
surface topography.
In the onte t of HD Plasti s™, a glossmeter is used to carried out the gloss
value with a incident angle of 60° : spectro-guide 45/0 gloss (BYK). HD
Plasti s™ is follo ing the ISO 8 Standard.
The graph shows the gloss scale using glossmeter following 60° angle in the
gloss unit. Low Gloss corresponds to a textured surface, Semi Gloss and High
Gloss to high polished surface.
White
L* = 100
Black
L* = 0
Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2
376,83 45,167 842,5 395,5 1275 717,33 501,83 350,5 1007,8 759,17 1468 1112
88,01% 53,06% 43,74% 30,16% 24,67% 24,27%
FORM
FOR-TEC-101 Rev.: B
Page 1 of 3
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY
TRADE NAME Thermocomp GRADE DC0041PQ
PICTURES OF INJECTED SAMPLES
TRIAL # HDP-17-023 MOLD Spiral 1 mm
MATERIAL
FAMILY
70
12/10/2017DATE
SUPPLIER
180°C 136,9% 94,0% 85,7% 180°C - 74,2% - 69,2%
T=180°C - RocTool - WITH (1000 Bar)
160°C
140°C 57,2% 36,3% -35,5% -38,3% _
98,5% 70,8% 62,0% 160°C -58,7% -55,8%
20
Sabic
36,3% 140°C
500 1000 1500 Flow Length (cm) 10 15
Flow length improvement IMM Pressure improvement
T=80°C - Conventional - WITHOUT (1000 Bar)
PC CF FR
MELT TEMPERATURE (°C) DRYING TEMPERATURE (°C)280
Pressure (Bar)
Mold Pressure Avg
Pressure Drop (%)
PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS
CONVENTIONAL TECHNOLOGY (80°C) ROCTOOL TECHNOLOGY (180°C)
Pressure (Bar) 500 1000 1500 500 1000 1500
_
_
FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE IMM PRESSURE DROP AT ISO FLOW LENGTH
Sensors
Sensor 1
Sensor 2
Sensor 1
Sensor 2
Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2
483,33 293,83 982,17 703,33 1433 1067,2 471,67 393,67 978,33 825,33 1460,8 1228,8
Pressure (Bar) 500 1000 1500 500 1000
18,2% 140°C -26,8% -18,5%
31,3% 160°C
140°C 21,4% 10,4%
34,7%
- 45,0%
15,88%Pressure Drop (%)
Sensors
FORM
T=180°C - RocTool - WITH (1000 Bar)
MATERIAL
FAMILY PC CF FR Sabic
TRADE NAME Thermocomp GRADE DC0041PQ
FOR-TEC-101 Rev.: B
Page 2 of 3
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
DATE 12/10/2017
MELT TEMPERATURE (°C) 280 DRYING TEMPERATURE (°C) 70
PICTURES OF INJECTED SAMPLES
T=80°C - Conventional - WITHOUT (1000 Bar)
HDP-17-023 MOLD Spiral 1.5 mm
SUPPLIER
Flow length improvement IMM Pressure improvement
30
-26,5%
500 1000
TRIAL #
Flow Length (cm)1500 20Pressure (Bar)
FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE
39,21% 28,39% 25,53% 16,54%
PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS
-42,1%
25
ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY
-35,0% -38,6%
- 52,9%180°C 52,5% 40,5% 48,4% 180°C
23,7%
1500
ROCTOOL TECHNOLOGY (180°C)CONVENTIONAL TECHNOLOGY (80°C)
IMM PRESSURE DROP AT ISO FLOW LENGTH
160°C
Mold Pressure Avg
15,64%
- 62,2%
Sensor 1
Sensor 2
Sensor 1
Sensor 2
Flow Length improvement vs Injection Pressure in function of Mold Temperature/Mold Thickness
Note : All the injection trials and the pressure measurements were carried out according to the protocol defined by RocTool (injection process, 2 heating
sides, cold sprue, mold design).
All pressure data are measured using eDart system (RJG).
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
DATE 12/10/2017 TRIAL #
MELT TEMPERATURE (°C) 280 DRYING TEMPERATURE (°C) 70
HDP-17-023 MOLD Spiral
FORM
FOR-TEC-101
MATERIAL
FAMILY PC CF FR SUPPLIER Sabic
TRADE NAME Thermocomp GRADE DC0041PQ
Rev.: B
Page 3 of 3
Pressure Drop between the 2 Sensors vs Mold Thickness at
Injection Pressure = 1000 Bars
Results Evaluations
The graph above shows a flow length for the two
thicknesses at two temperature (80°C and 180°C). By
comparing these curves, a significant reduction in thickness
can be observed.
With Roctool technology, we are able to achieve an
equivalent flow length at 1 mm compare to 1.5 mm in
conventional technology.
Also, the following diagram shows the pressure drop
measured between the two sensors for the two thicknesses
at 1000 bars of injection pressure. The reduction of
pressure
drop in the cavity is important up to 112%.
GLOBAL COMMENTS & RECOMMENDATIONS
The HD Plastics™ characterization trials shows a significant flow length and pressure drop improvment. The optimum
mold temperature is 180°C regarding to the trials performed with this material. We obtain the longest flow with an
important
reduction of the pressure drop compared to the conventional mold temperature.
Also, we demonstrated that we could reduce the thickness of injected parts from 1.5 mm to 1 mm.

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thermocomp DC0041PQ

  • 1. FULL HD PLASTIC ™ REPORT
  • 2. ΔL Δa Δ 20462 22% 82% 278% Volume cavity (µm3 ) Note: L* = 0 yields black and L* = 100 indicates diffuse white. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values indicate yellow. ΔE> , usual olor toleran e. Roughness profile - Conventional VS Roctool Technology T=160°C - Roctool - WITHT=90°C - Conventional - WITHOUT PICTURES OF INJECTED SAMPLES 3D TEXTURATION RESULTS T=80°C - Conventional - WITHOUT T=160°C - Roctool - WITH Conventional (µm3 ) Roctool technology (µm3 ) Improvement (%)Roughness parameters 5416 Rate replication from the mold surface (%) DC0041PQ DATE DELTACOLOR SCALE L* ( Lightness) MEASUREMENTS PROCESS TECHNOLOGY -0,01 T=160°C - Roctool - WITH SUPPLIER SABIC 0,19 ΔE COLOR DIFFERENCE LAB - COLOR DEPHT RESULTS (DIN 5033 Standard) 0,03 T=80°C - Conventional - WITHOUT 28,85 -0,04 -0,39 28,66 a* -0,05 b* -0,36 Rev.: A GLOSS RESULTS (ISO 2813 Standard) T=80°C - Conventional - WITHOUT 21,7 102,6T=160°C - Roctool - WITH TRADE NAME -0,19 17/01/2018 TRIAL # HDP-17-023 MOLD HD PLAQUE MATERIAL FAMILY PC FORM FOR-TEC-111 Page 1 of 3 QUALITY SURFACE CHARACTERIZATION REPORT LNP™ THERMOCOMP™ COMPOUND GRADE
  • 3. COMMENTS 1,00 Quality surface characterization: 1) Visible improvements using Roctool technology are observed: weld line and sink marks are removed. Glass fibers and defects are removed from the surface. 2) Significant improvement on the gloss value up to 365%. However, we measured a slight impact of the mold temperature on the color perception. However the surface finish with Roctool is drastically improved with high level of gloss compared to conventional process. 3) The different textured areas hightlight the positive impact on the replication using Roctool technology. The different roughnesses are well felt when touched. The roughness measurement carried out using optical rugosimeter confirms the above with repliction rate of up to 82% : an improvement of 278% with Roctool compared to conventional technology (CIM). Also, the Rz value has been carried out and shows the positive impact of Roctool with an important reduction of the roughness on high gloss surface due to the elimination of glass fibers at the surface. FORM FOR-TEC-111 Rev.: A Page 2 of 3 QUALITY SURFACE CHARACTERIZATION REPORT 2,461,56 TEXTURE RESULTS - Ra (Amplitude roughness parameter) Roctool technology 160°C VDI 18 (Ra=±0.80 µm) VDI 22 (Ra=±1.26 µm) VDI 27 (Ra=±2.20 µm) TEXTURE RESULTS - Rz (Mean roughness depth) Roughness parameters Conventional (80°C) Roctool technology (160°C) Improvement (%) CHEMICAL 1,12 1,76 2,91 Ra (µm) EDM 0,97 1,18 2,09 Ra (µm) Rz (µm) 7,05 2,01 -71% T=80°C - Conventional - WITHOUT T=160°C - Roctool - WITH LASER Ra (µm) Note: In conventional molding, the measurements of the VDI roughness are not mentionned as the presence of glass fibers on the surface disturb the measurement impacting the Ra value.
  • 4. GLOSS PRINCIPLE FORM FOR-TEC-111 Rev.: A Page 3 of 3 QUALITY SURFACE CHARACTERIZATION REPORT ANNEXES MEASUREMENT AREAS 1) The high gloss area framed in blue is the measurement area for the gloss, color and specific roughness Rz* . 2) The red rectangle define the nano-replication area. 3) The green box correspond to the multi-textured (VDI) area were the roughness is measured. *Rz: Maximal amplitude roughness mesured for filled materials ROUGHNESS MEASUREMENT PRINCIPLE Optical rugosimeter is a measuring instrument used to measure a surface's profile, in order to quantify its roughness. In the context of HD Plastics™, two information are carried out using Alicona equipment according to the standard ISO 4287: - Replication rate : volume of the specific texture defined versus the one textured on the mold surface quavity - The surface roughness parameters : Arithmetical mean deviation (Ra) which evaluate the roughness amplitude on a profile and Mean roughness depth (Rz) which measure the maximal amplitude roughness average of the profile. LAB COLOR PRINCIPLE The Lab color space describes all perceivable colors in the three dimensions L for lightness and a and for the olor opponents green–red and lue– ello . In the context of HD Plastics™, a spectrophotometer is used to carried out the LAB alue : spe tro-guide / gloss BYK . HD Plasti s™ is follo ing the DIN 5033 Standard. The graph shows the LAB color scale. The lightness, L*, represents the darkest black at L* = 0, and the brightest white at L* = 100. The a* and b* value represent the color channels. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values indicate yellow Gloss is an optical property which indicates how well a surface reflects light in a specular direction. It is one of important parameters that are used to describe the visual appearance of an object. The factors that affect gloss are the refractive index of the material, the angle of incident light and the surface topography. In the onte t of HD Plasti s™, a glossmeter is used to carried out the gloss value with a incident angle of 60° : spectro-guide 45/0 gloss (BYK). HD Plasti s™ is follo ing the ISO 8 Standard. The graph shows the gloss scale using glossmeter following 60° angle in the gloss unit. Low Gloss corresponds to a textured surface, Semi Gloss and High Gloss to high polished surface. White L* = 100 Black L* = 0
  • 5. Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 376,83 45,167 842,5 395,5 1275 717,33 501,83 350,5 1007,8 759,17 1468 1112 88,01% 53,06% 43,74% 30,16% 24,67% 24,27% FORM FOR-TEC-101 Rev.: B Page 1 of 3 FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY TRADE NAME Thermocomp GRADE DC0041PQ PICTURES OF INJECTED SAMPLES TRIAL # HDP-17-023 MOLD Spiral 1 mm MATERIAL FAMILY 70 12/10/2017DATE SUPPLIER 180°C 136,9% 94,0% 85,7% 180°C - 74,2% - 69,2% T=180°C - RocTool - WITH (1000 Bar) 160°C 140°C 57,2% 36,3% -35,5% -38,3% _ 98,5% 70,8% 62,0% 160°C -58,7% -55,8% 20 Sabic 36,3% 140°C 500 1000 1500 Flow Length (cm) 10 15 Flow length improvement IMM Pressure improvement T=80°C - Conventional - WITHOUT (1000 Bar) PC CF FR MELT TEMPERATURE (°C) DRYING TEMPERATURE (°C)280 Pressure (Bar) Mold Pressure Avg Pressure Drop (%) PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS CONVENTIONAL TECHNOLOGY (80°C) ROCTOOL TECHNOLOGY (180°C) Pressure (Bar) 500 1000 1500 500 1000 1500 _ _ FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE IMM PRESSURE DROP AT ISO FLOW LENGTH Sensors Sensor 1 Sensor 2 Sensor 1 Sensor 2
  • 6. Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 483,33 293,83 982,17 703,33 1433 1067,2 471,67 393,67 978,33 825,33 1460,8 1228,8 Pressure (Bar) 500 1000 1500 500 1000 18,2% 140°C -26,8% -18,5% 31,3% 160°C 140°C 21,4% 10,4% 34,7% - 45,0% 15,88%Pressure Drop (%) Sensors FORM T=180°C - RocTool - WITH (1000 Bar) MATERIAL FAMILY PC CF FR Sabic TRADE NAME Thermocomp GRADE DC0041PQ FOR-TEC-101 Rev.: B Page 2 of 3 FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD DATE 12/10/2017 MELT TEMPERATURE (°C) 280 DRYING TEMPERATURE (°C) 70 PICTURES OF INJECTED SAMPLES T=80°C - Conventional - WITHOUT (1000 Bar) HDP-17-023 MOLD Spiral 1.5 mm SUPPLIER Flow length improvement IMM Pressure improvement 30 -26,5% 500 1000 TRIAL # Flow Length (cm)1500 20Pressure (Bar) FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE 39,21% 28,39% 25,53% 16,54% PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS -42,1% 25 ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY -35,0% -38,6% - 52,9%180°C 52,5% 40,5% 48,4% 180°C 23,7% 1500 ROCTOOL TECHNOLOGY (180°C)CONVENTIONAL TECHNOLOGY (80°C) IMM PRESSURE DROP AT ISO FLOW LENGTH 160°C Mold Pressure Avg 15,64% - 62,2% Sensor 1 Sensor 2 Sensor 1 Sensor 2
  • 7. Flow Length improvement vs Injection Pressure in function of Mold Temperature/Mold Thickness Note : All the injection trials and the pressure measurements were carried out according to the protocol defined by RocTool (injection process, 2 heating sides, cold sprue, mold design). All pressure data are measured using eDart system (RJG). FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD DATE 12/10/2017 TRIAL # MELT TEMPERATURE (°C) 280 DRYING TEMPERATURE (°C) 70 HDP-17-023 MOLD Spiral FORM FOR-TEC-101 MATERIAL FAMILY PC CF FR SUPPLIER Sabic TRADE NAME Thermocomp GRADE DC0041PQ Rev.: B Page 3 of 3 Pressure Drop between the 2 Sensors vs Mold Thickness at Injection Pressure = 1000 Bars Results Evaluations The graph above shows a flow length for the two thicknesses at two temperature (80°C and 180°C). By comparing these curves, a significant reduction in thickness can be observed. With Roctool technology, we are able to achieve an equivalent flow length at 1 mm compare to 1.5 mm in conventional technology. Also, the following diagram shows the pressure drop measured between the two sensors for the two thicknesses at 1000 bars of injection pressure. The reduction of pressure drop in the cavity is important up to 112%. GLOBAL COMMENTS & RECOMMENDATIONS The HD Plastics™ characterization trials shows a significant flow length and pressure drop improvment. The optimum mold temperature is 180°C regarding to the trials performed with this material. We obtain the longest flow with an important reduction of the pressure drop compared to the conventional mold temperature. Also, we demonstrated that we could reduce the thickness of injected parts from 1.5 mm to 1 mm.