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By : Hammad Wali
BS Biotechnology
Quaid e Azam University
GRAVIMETRIC
ANALYSIS
INTRODUCTION
Gravimetric analysis is a class of lab techniques used to determine
the mass or concentration of a substance by measuring a change in
mass.
PRINCIPAL : mass of an ion in a pure compound can be determined
and then used to find the mass percent of the same ion in a known
quantity of an impure compound.
TYPES
Volatilization
Volatilization Gravimetry
involves separating
components of our mixture
by heating or chemically
decomposing the sample.
Precipitation
Precipitation Gravimetry
uses a precipitation reaction
to separate one or more
parts of a solution by
incorporating it into a solid.
Electrogravimetry
Electrogravimetry is a
method used to separate
and quantify ions of a
substance
Thermogravimetric
Thermogravimetric is a
method in which changes in
physical and chemical
properties of materials are
measured as a function of
function of time
STEPS FOLLOWED IN GRAVIMETRIC
ANALYSIS
Computation of the
amount of the
particular
constituent in the
sample from the
observed weight of
the isolated
substance
Separation of the
desired constituent
and
Weighing the
isolated constituent.
Preparation of a
solution containing a
known weight of the
sample.
1. Preparation 2. Seperation 3.Calculation
GENERAL
PROCEDURE
• Preparation of the solution
• Precipitation
• Filtration
• Drying
• Ignition
• Weighing
• Calculations
ADVANTAGES
It provides a little room for
instrumental error and does
not require a series of
standards for calculation
Gravitmertic analysis is
potentially more accurate
and precise
ACCURATE LESS ERRORS
It is an ABSOLUTE
METHOD , avoid
problems with
temperature fluctuations,
Calibration errors
ABSOLUTE
METHOD
It is relatively inexpensive
compared to other
methods of analysis
INEXPENSIVE
1.
4.
2. 3.
DISADVANTAGES
It usually provides
only for the
analysis of a
single element, or
a limited group of
elements, at a
time
Glassware should
be very clean
Proper Lab
technique is
critical
Very Accurate
weighing
Requires Care
and is very Time
consuming
1 3 5
4
2
Thank You :)
THE END

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Gravimetric Analysis

  • 1. By : Hammad Wali BS Biotechnology Quaid e Azam University GRAVIMETRIC ANALYSIS
  • 2. INTRODUCTION Gravimetric analysis is a class of lab techniques used to determine the mass or concentration of a substance by measuring a change in mass. PRINCIPAL : mass of an ion in a pure compound can be determined and then used to find the mass percent of the same ion in a known quantity of an impure compound.
  • 3. TYPES Volatilization Volatilization Gravimetry involves separating components of our mixture by heating or chemically decomposing the sample. Precipitation Precipitation Gravimetry uses a precipitation reaction to separate one or more parts of a solution by incorporating it into a solid. Electrogravimetry Electrogravimetry is a method used to separate and quantify ions of a substance Thermogravimetric Thermogravimetric is a method in which changes in physical and chemical properties of materials are measured as a function of function of time
  • 4. STEPS FOLLOWED IN GRAVIMETRIC ANALYSIS Computation of the amount of the particular constituent in the sample from the observed weight of the isolated substance Separation of the desired constituent and Weighing the isolated constituent. Preparation of a solution containing a known weight of the sample. 1. Preparation 2. Seperation 3.Calculation
  • 5. GENERAL PROCEDURE • Preparation of the solution • Precipitation • Filtration • Drying • Ignition • Weighing • Calculations
  • 6. ADVANTAGES It provides a little room for instrumental error and does not require a series of standards for calculation Gravitmertic analysis is potentially more accurate and precise ACCURATE LESS ERRORS It is an ABSOLUTE METHOD , avoid problems with temperature fluctuations, Calibration errors ABSOLUTE METHOD It is relatively inexpensive compared to other methods of analysis INEXPENSIVE 1. 4. 2. 3.
  • 7. DISADVANTAGES It usually provides only for the analysis of a single element, or a limited group of elements, at a time Glassware should be very clean Proper Lab technique is critical Very Accurate weighing Requires Care and is very Time consuming 1 3 5 4 2