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UNIVERSITY OF NORTHUMBRIA AT NEWCASTLE 
SCHOOL OF THE BUILT ENVIRONMENT 
The Effects of Adding Waste Wood Chippings and Silica Fume to the Flexural Strength 
Capacity of Concrete 
A DISSERTATION SUBMITTED TO THE SCHOOOL OF THE BUILT 
ENVIRONMENT IN PARTIAL FULFILMENT OF THE REQUIREMENTS FOR 
THE DEGREE OF 
BSc Architectural Technology 
By 06012242 
APRIL 2010
3 
Abstract 
This piece of research investigates the effects of adding waste wood chippings form the 
timber industry, and silica fume, to the flexural strength capacity of concrete. Three groups of 
concrete beams were made, group 1 consisting of plain concrete, group 2 had wood chippings 
added to the mix and group 3 was a hybrid of wood chippings and silica fume. After 
compiling a suitable methodology and carrying out a flexural test programme, results showed 
that additions of wood and silica fume reduce flexural strength, however wood and silica 
additions are shown to increase maximum deflection before failure of the concrete beams. 
The results were encouraging towards the research and production of more sustainable 
concrete technologies. 
i
4 
Table of Contents 
Abstract i 
1.0 Proposal 5 
1.1 Hypothesis 5 
1.2 Research Aims 5 
1.3 Objectives 6 
2.0 Literature Review 7 
2.1 An overview of sustainable concrete 7 
2.1.1 Fly Ash Concrete 7 
2.1.2 Wood Chippings in Concrete 8 
2.2 Flexural Testing of Fly Ash and Wood Chip Concrete 8 
2.3 Mineral Based Composites 9 
2.4 Optimum Ratios 9 
2.5 Conclusion 9 
3.0 Methodology 10 
3.1 Structural Elements and the Need to Perform Flexural Testing 10 
3.2 Production of Beams 10 
3.2.1 Materials 10 
3.2.2 Mix Design 11 
3.2.3 Quantities 11 
3.2.4 Slump Testing 11 
3.2.5 Pouring and Compacting the Concrete 12 
3.3 Curing 12 
3.4 Methods of Performing Flexural Tests 12 
3.4.1 Loading Rate 13 
3.5 Calculating Flexural Strength 13 
4.0 Results and Analysis 14 
4.1 Results of Plain Concrete Beam Flexural Testing Programme 14 
4.2 Results from using Wood Chippings as Addition to the Concrete Beams 15 
4.3 Results from using Wood Chippings and Silica Fume as Addition 
to the Concrete Beams 16 
4.4 Overview of Flexural Strength Results 17 
4.5 Analysis of Results 17 
4.6 Determining the Density Characteristics of the Concrete Mixes 18 
4.7 Drying Curve 20 
5.0 Conclusions 23 
5.1 Research Limitations 23 
6.0 Recommendations 25 
7.0 References 26 
8.0 Appendices 28
5 
1.0 Proposal 
There has been extensive research into trying to increase the sustainability of concrete whilst 
retaining high levels of flexural strength. 
The core of this research seems to be investigating the use of mineral based composites 
(MBCs). Research conducted by Blanksvard (2009), highlights the drawbacks of using 
epoxies, and concludes that in compressive strength tests that MBCs contribute to increasing 
load bearing capacity for strengthened concrete considerably. 
Further research into MBCs reveals that there is actually however, conflicting results to the 
levels of strength improvement in concrete. One such study tested flexural strength as oppose 
to compressive and concluded that the ‘stress at the cut off point is considerably smaller for 
the MBC system compared to that of the epoxy based carbon fibre reinforced polymer 
(CFRP) system’ (Johansson, 2005). 
Increased research into mineral bonding agents (MBAs) brings to attention that the use of fly 
ash in concrete is very common practice, as well as other recycled agents such as crushed 
glass and silica fume. A research paper on the effects of fly ash in concrete concluded that 
each tonne of cement that can be replaced by fly ash reduces CO² emissions by 1 tonne also 
(Bjork, 1999). Another piece of research also uses fly ash as well as mixing in waste wood 
ash, replacing 25-35% of cement used. This was found to significantly improve the 
performance of concrete in both compression and flexural testing (Naik, 2002). 
A research publication that tested the effects of untreated sawdust as an additive to polymer 
concrete, concluded wood waste did improve flexural strength and fracture toughness when 
applied as reinforcement to polymer concrete, (Reis, 2006). However, this is thought not to 
be the same case for compression, as research by Becchio (2009), concluded that when wood 
waste was used as an aggregate, compression strength tests indicate a reduced performance in 
mechanical properties such as crushing resistance and bulk density. 
Research by Coatanlem (2005), and concluded that by saturating wood chippings with 
sodium silicate, improves significantly the compressive strength of concrete. However, it also 
concluded that without the sodium silicate, the compressive strength was reduced. This is 
thought to be as the sodium silicate improves the bond between the wood – cement interface. 
This research conducted tests on compression alone, failing to expand the investigation 
beyond this parameter. Therefore the behaviour of this mix design on flexural strength has to 
be investigated. 
As no tests have currently been done on flexural performance and with conflicting research 
conclusions, a further investigation may be proposed to research into the effects of using 
untreated wood chippings as reinforcement, with the additive of silica fume to improve the 
bond interface, thus filling this knowledge gap. 
1.1 Hypothesis 
It is suggested that if waste wood chippings and silica fume is added as reinforcement to a 
concrete beam, then the flexural strength of concrete beams will be improved. 
1.2 Research Aims 
To test to see if the use of waste wood chippings from the timber industry and the addition of 
silica fume, can improve flexural performance of concrete.
6 
1.3 Objectives 
1) To test 10 concrete beams with no reinforcement 
2) To test 10 concrete beams with waste wood chipping added as reinforcement 
3) To test 10 concrete beams with waste wood chipping and silica fume added as 
reinforcement 
4) To record results appropriately 
5) To compare and analyse the 3 groups of test results 
6) To evaluate the effectiveness of adding waste wood chippings and silica fume to 
concrete mixes. 
The following chapter will consider existing research into sustainable concrete, looking at the 
additions of by-products to concrete to improve sustainability as well as maintaining adequate 
levels of strength.
7 
2.0 Literature Review 
This chapter intends to review existing pieces of research into the production of sustainable 
concrete. The need for sustainable concrete and the search for suitable by-products, with 
specific reference to mineral based composites, will be addressed within this chapter. 
Extensive research has been carried out into trying to increase the sustainability of concrete, 
Li-hua (2009), Naik (2002), Becchio (2009), Turgut (2007), whilst retaining high levels of 
both compressive and flexural strength. The following section will outline research that has 
been conducted into improving sustainability of concrete whilst trying to retain high 
compressive strength values. 
2.1 An Overview of Sustainable Concrete. 
Research carried out by Canbaz et al. (2004) used waste glass, as a course aggregate within 
concrete. The glass used was between 4-16mm and used in a mix proportion of up to 60%. 
Testing of this determined that it actually had a slight reduction in compressive strength. A 
study was conducted by Shayan (2002) looks at glass ground in to a fine powder and added to 
the mix, replacing 30% of the cement used. The results from this test found that this did 
provide a significant increase to the concrete’s compressive strength. In addition to this, 
Soroushian et al, (2003) found that the addition of recycled plastics also has a positive effect 
of concrete compressive strengths. Galetakis (2004) also conducted compression tests using 
limestone dust as an addition with Portland cement mix, while the dust/cement ratio was 
found to be the key factor, results showed that compressive strengths can be increased. 
The studies discussed above show that many materials have been used as aggregates in 
concrete. However, whilst many different pieces of research have been carried out using 
different waste materials as additions to the concrete mix, the most extensive amounts with 
the most positive results, come from testing carried out using ash or wood chipping additions. 
Focusing on compression tests, the next section reviews studies that have used ash as an 
addition to the concrete mix. 
2.1.1 Fly Ash Concrete 
Very early research was carried out by Miller et al. (1975) into the use of fly ash, as well as 
other reclaimed materials, as alternative aggregates. The research found that fly ash offered 
the most improvement to concretes compressive strength. The most recent and in depth piece 
of research conducted undertaken by Naik (2002) using fly ash alone, tests were conducted 
using between 25-35% of fly ash blended with the concrete mix. After a 28 day curing period 
it was concluded that the compressive strength of the concrete was significantly increased. 
Research previous to this was also carried out by Carette (1993) using between 55-60% fly 
ash in a concrete mix, concluded that after 91 days curing that the concretes compressive 
strength was up to 50 N/mm². However, another study conducted by Bjork (1999) found that 
by using a water/cement ratio of 0.3, can have as much as 60% of the cement replaced with 
fly ash and can produce a 55 N/mm² a compressive strength concrete after 28 days. A study 
by Li-hua (2009) confirmed that the addition of fly ash content between 10-55% will improve 
compressive strengths as well as improving workability and durability, however more than 
55% content will reduce compressive values after 90 days, as the compressive strength of fly 
itself is less that concrete. 
The above research shows that the addition of fly ash to concrete can significantly improve 
compressive strength; this is because fly ash is comprised of the non-combustible mineral 
portion of coal consumed in a coal fuelled power plant. The particles are glassy and spherical
shaped that are typically finer than cement particles. The fly ash undergoes a ‘pozzolanic 
reaction’ with the lime created by the hydration (chemical reaction) of cement and water, to 
create the same binder (calcium silicate hydrate) as cement. The pozzolanic reaction that 
takes place is the fly ash changing into a siliceous material that reacts with the lime, forming 
a compound that is cementitious at normal temperatures. It is this pozzolanic reaction that 
will be looked at in section 2.3, when silica is looked at as a mineral based composite. 
After looking at the effects of fly ash, as previously mentioned, the addition of waste wood 
also has had extensive research carried out on its effect to compressive strengths on concrete. 
Section 2.1.2 will give an overview to these. 
8 
2.1.2 Wood Chippings in Concrete 
Research by Becchio (2009) tried to increase sustainability of concrete by replacing natural 
aggregates in the mix, with waste wood chippings. Different mix proportions were of 
cement/admixture/water was made and cubes formed. Their compressive strength was tested 
after a 28 day curing period. The testing concluded that in all cases the addition of wood 
waste decreased the compressive strength of the concrete, the decrease in strength was found 
to be in proportion to the drop in density as wood in less dense than aggregate. A previous 
study to this was performed by Turgut (2007) who investigated the use of high levels of 
waste sawdust to concrete mixes, and the results obtained were enough to satisfy international 
standards. Although this test does not increase the compressive strength, it shows that equal 
strengths can be achieved by using sustainable methods. A much earlier piece of research was 
carried out by Al Rim et. al. (2000) also reused wood waste as an aggregate for concrete, 
although the research was aimed at the thermal properties of this, it did conclude that the 
addition of the wood waste reduced the compressive strength. 
The studies and tests in the previous paragraph show contradicting results for the addition of 
wood wastes to the concrete mixes, this could be due to a number of factors. However, all of 
the previous research looked at, measured concrete under compression testing. The next 
section will focus on tests that have been carried out to increase the flexural strength of 
concrete, and see if the same materials have the same effects. 
2.2 Flexural Testing of Fly Ash and Wood Chip Concrete 
Coatanlem (2002) conducted research using waste wood chippings as fibres for concrete 
reinforcement. The wood chippings were between 0.5-10.0mm and the beams were 
40x40x160mm. The optimum wood/cement ratio was 3.6, and the optimum water cement 
ratio was 0.75. After 28 days, the beams were tested and it was found that the flexural 
strength of all the samples was less than 10MPa; this is a significant reduction to that of 
normal Portland cement, recording 45MPa. Research by Reis (2006) tested plain epoxy 
polymer concrete reinforced with wood waste. Mixes were made with varying proportions of 
cement and waste wood. Flexural strengths were then tested and compared to that of plain 
epoxy polymer concrete. The results obtained showed that flexural strength increased by 
6.03%. 
The comparison between the two above studies by Coatanlem (2002) and Reis (2006) show 
that wood chippings alone will not increase the flexural strength of concrete, but adding 
wood waste to an epoxy polymer concrete will improve the strength. However, the use of 
epoxy concrete poses disadvantages such as hazardous working environments for the 
workers, as well as being sensitive to moisture and thermal conditions, (Tliljsten et al. 2006).
9 
The next section will discuss research into Mineral based Composites; these are designed to 
be a more sustainable, replacement to epoxy adhesives. 
2.3 Mineral Based Composites 
Blanksvard (2009) has carried out extensive research into the use of Mineral Based 
Composites (MBCs) as an addition to carbon fibre reinforced concrete. The first part of his 
research uses MBCs as a strengthening system to repair concrete. However flexural tests 
were also conducted within this research to expand the data collection. This research 
concluded that the uses of minerals, such as silica fume, improve the bond between the 
cement, to the reinforcement fibres. The reaction that improves the bond is the same as 
discussed in section 2.1.1, as the use of minerals like silica fume undergoes a pozzolanic 
reaction. This result would explain the difference in the two previously discussed tests carried 
out by Coatanlem (2002) and Reis (2006), as Reis used the wood chippings in epoxy 
concrete, so the epoxy would have created a stronger bond between the cement and the wood 
chippings. Blanksvard also concluded that for flexural strength to be improved, optimum 
ratios of water/cement and also polymer/cement ratios need to be found. These are addressed 
in the following section. 
2.4 Optimum Ratios 
Research conducted by Schulze (1999) show that the flexural strength of concrete can be 
increased substantially by altering the water/cement ratio, within a modified mortar. This 
confirmed earlier research by Beton (1990). Research into polymer/cement ratios was 
conducted by Pascal et al. (2004) and Van Gemert et al. (2005) who found that increases in 
flexural strength were found significant when polymer/cement ratios were between 10% and 
15% weight content. Ratios higher than this are shown to result in a decrease in the strength 
properties. The research by Pascal et al. (2004) and Van Gemert et al. (2005) confirmed the 
earlier findings from Rao (2003) and Huang Cheng-Yi et. al. (1985), whose work addressed 
the performance of silica fume within concrete. Both of these researchers tested silica fume 
levels between 0% and 30% content by weight within a mix and found that optimum levels 
for increasing flexural strength lie between 15% and 22% by weight. 
2.5 Conclusion 
From the research presented, it has been shown that the flexural strength of concrete can 
actually decrease by replacing aggregates and fibres with only recycled materials such as 
wood, ash and glass. It has also been shown that in many cases the addition of epoxies and 
Mineral Based Composites can then go on to increase the flexural strength of concrete as the 
bond between the recycled fibres and the cementitious material is strengthened. Further 
research into these bonds concluded that water/cement and polymer/cement ratios are of 
significance to the flexural strength. The use of Mineral Based Composites, such as silica 
fume, increase sustainability of concrete as it is a by product of producing silicon metal. 
Silica fume also increases workability, compared to an epoxy resin. The tests looked at above 
use silica fume with polymer fibres, and no tests were found that adopted silica fume as an 
additive to concrete reinforced with waste wood chippings acting as a fibre addition. The 
study by Reis (2006) did use wood chippings, but with epoxy concrete. 
The intention of this work is to address the knowledge gap in the research, as presented 
within this chapter, by exploring the use of silica fume as an epoxy replacement to concrete 
reinforced with waste wood chippings. Chapter 3.0 identifies the methodology used to 
explore this work.
10 
3.0 Methodology 
The previous chapter indentified an apparent lack of data on sustainable methods to improve 
the flexural strength of concrete, with specific reference to the use of silica fume and waste 
wood chippings. This chapter will justify the use of a flexural test programme and determine 
the materials used in the production of the beam test programme in address. 
3.1 Structural Elements and the Need to Perform Flexural Testing 
From research presented in the literature review, it is shown that tests have been carried out 
on improving both compressive and flexural strengths of concrete. However the research 
presented does not focus on increasing the sustainability of concrete. In order to collect data 
for the improvement of flexural strength of a concrete beam then a test was required. Whilst 
other forms of data collection, such as comparing case studies, may have given an indication 
of what is likely to happen to the flexural strength, actual first hand data could not be 
obtained without testing. 
There are also a number of different practical uses for flexural strength improvement, 
as concrete is widely used as a material for structural elements such as beams and other 
framing members. It is important that when adopted for this type of application, it can 
withstand loads without failing. Beams spanning across any length within a building will be 
under flexural loading, whether it be carrying dead or live loads. 
With a huge pressure on the modern day construction industry to increase 
sustainability and reduce carbon emissions, it is important that methods for meeting 
sustainability criteria are explored without compromising strength. The implications of this 
are that higher strength and sustainability within concrete will offer greater opportunities for 
architects, technologists, contractors and clients to want to use concrete. As well as this, with 
higher flexural strengths, larger spans can be reached allowing architects to design more 
diverse buildings. The next chapter will look at the how the beams to be tested were 
produced. 
3.2 Production of Beams 
As discussed within the literature review, beams will be tested with the addition of waste 
wood chippings and silica fume. The following sections will look at beam design, including 
acquiring the materials, ratios of materials used and the quantities of beams made. 
3.2.1 Materials 
The wood chippings that were added to the mix came from a local timber merchant, and were 
ungraded, untreated and from a variety of trees. The decision to use chippings like these was 
to add to the sustainability of the beams, as costs are incurred to sort and grade the wood, as 
well as treat it. The idea was that the wood chippings were used as ‘raw’ waste from the 
timber industry. The silica fume was obtained from an international chemical company who 
specialize in making environmentally friendly metals and materials. The silica fume used was 
undensified meaning that the grains are slightly larger than those of densified silica, also the 
undensified silica fume is easier to work with and offers no hazardous working conditions 
with regard to skin contact and inhalation. The silica fume fully conformed to the American 
Society for testing Materials code C1240 for the Standard Specification for Silica Fume Used 
in Cementitious Mixtures (ASTM C1240 -05). The cement used was ordinary Portland 
cement which conforms to BS 12, this was the same as all of the tests presented within the 
literature review and is the most readily available to use. The aggregates, sand and water 
were all readily available from the universities laboratory.
11 
3.2.2 Mix Design 
As presented in the literature review Schulze (1999) and Rao (2003) showed that optimum 
ratios of water/cement and silica fume/cement can have major influences on the flexural 
strength of concrete. The optimum silica fume amount was found to be between 15-22% of 
the mix, however later research by Van Gemert et al. (2005) suggested 15% of a silica 
addition was the maximum before a decrease in flexural strength would appear. For that 
reason a 15% addition was added to the mix. 
The ratio of wood chippings to the mix was chosen at cement/wood ratio of 3. This 
was due to recent research by Becchio (2009) suggesting this was the optimum ratio. Earlier 
research by Coatanlem (2002) as presented in the literature review suggested 3.6, however 
this was also rounded down to 3 for the testing. This research also concluded that the 
optimum water/cement ratio was 0.75 so in order to maintain validity the same ratio was 
used. 
The ratio of mix between cement/sand/gravel was 3/6/10 in accordance to BS 8500. 
For all beams made, the cement sand and gravel were mixed first, and then the correct 
amount of water added accordingly. Mixing was followed by the addition of the wood 
chippings to the batches that included both wood and silica fume. The silica fume was added 
last and mixed in full accordance with the manufacturer’s guidelines for mixing (See 
Appendix 1). 
3.2.3 Quantities 
With the above ratios used, this section will look at exactly how much of each material was 
added to the mix. 30 beams were made in total, 10 beams in a control group with plain 
concrete. 10 beams with wood chipping alone and the final 10 beams were a hybrid of silica 
fume and wood chipping. The decision to use 10 beams within each group was made by 
looking at research in the literature review, where research carried out by Shayan (2002), 
Galetakis (2004), Naik (2002) and Becchio (2009) all used between 6 and 10 specimens for 
each group. By using 10, it is also easier to identify any anomalous results and calculate 
levels of significant difference between groups. Table 1 below shows the quantities for all 
materials used. 
All amounts are based on batching 10 beams per group and include a 10% waste addition. 
Cement Sand Gravel Wood Silica Fume Water 
Plain group 21.56kg 38.81kg 58.00kg 0.00kg 0.00kg 16.17kg 
Wood alone 21.56kg 38.81kg 58.00kg 21.56kg 0.00kg 16.17kg 
Hybrid 21.56kg 38.81kg 58.00kg 21.56kg 3.25kg 16.17kg 
Table 1. 
3.2.4 Slump Testing 
A slump test measures the workability of the concrete, showing how easy the concrete is to 
place handle and compact. Slump tests must measure within a set range or tolerance from the 
target slump. A slump test was not carried out within this experiment as the mix would give 
different slump values due to the wood and silica additions and no target slump are values are 
specified for this type of mix. As well as this, all the quantities of materials were carefully 
measured and mixed in the exact same way; there were also time constraints within the 
laboratories making it difficult to complete a slump test. For producing plain concrete without 
limitations, a slump test must always be carried out.
12 
3.2.5 Pouring and Compacting the Concrete. 
All beams dimensions were the same at 100mm x 100mm x 500mm; this size was chose as it 
was the same dimensions as flexural testing carried out by Reis (2006). Pouring the concrete 
into the moulds must be carried out in a precise method. Using a trowel, the beams moulds 
were filled half way then compacted using steel hand tamp. Compaction takes place in order 
to reduced air content within the concrete, improving its performance, there should be a 
minimum of 100 compactions before pouring the remaining half into the mould, before a 
further 100 compactions are made (www.brmca.org.uk/Placing, 2009). The beam should be 
finished with a float to remove excess mix from the edges of the mould, this makes it easier 
to remove the beams from the moulds after curing. This process was repeated for each beam. 
3.3 Curing 
The curing period for the beams was 28 days; this was the same as all of the tests presented in 
the literature review. 28 days is also the advised time given by Portland cement 
(http://www.concrete.net.au, 2004). During the curing period, the mass of each beam was 
obtained by weighing the beams every 2 days in order to monitor their change in mass over 
the 28 day period. This gave the opportunity to look at the beams’ densities and compare 
differences between the groups. 
3.4 Methods of Performing Flexural Tests. 
The two main methods of testing flexural capacity of concrete are known as either the ‘single 
point’ load test or the ‘third point’ load test. Figure 1 below shows diagrammatically the two 
tests.. 
A B 
Figure 1. Flexure testing diagrams (Taken from www.nrmca.org/aboutconcrete, 2005) 
Figure 1A, shows the third point test as it applies the loads across two points at one third 
proportions of the beam. Figure 1B shows the single point test where the entire load is 
applied to the centre of the beam. 
With a brittle material such as concrete, the single point test is more common, although this 
test only provides data for flexural strength only, not stiffness 
(http://www.instron.co.uk/application /flexure, 2010). Research was also carried out into the 
difference between single point and third point tests, concluding that after testing 4 different 
types of polymers, that between the two tests no significant difference could be found in the 
results for modulus of rupture, (Chitchumnong et al. 1989). Figure 2 below shows the 
difference in between the two types of flexural test, displayed using a bending moment 
diagram.
13 
A B 
Figure 2. Bending Moment Diagrams (Taken from www.nrmca.org/aboutconcrete, 
2005) 
The areas shaded in red are the areas of the beam to which load will be exerted. Figure 2A 
shows how the stress is applied constantly over a large area. With this method the position of 
the first crack is unforced and can appear anywhere within the shaded region. However this 
means that the crack will follow the weakest path through the concrete beam that it can find. 
Figure 2B shows that the stress is applied to a smaller area than the third point test. The 
position of the first crack in the single point test is forced at a single point meaning that the 
crack cannot just follow the weakest path. 
With these pieces of research presented, a single point test was used, as use of the third point 
loading machine was limited and also was unable to be linked to a computer programme 
measuring the applied loads and deflection. All testing carried out conformed to BS EN 
12390-5:2009, which specifies a method for testing the flexural strength of specimens of 
hardened concrete. 
3.4.1 Loading Rate 
The loading rate applied was 1.1mm/minute, this is the rate proposed in research by 
Coatanlem (2002). There is no set rate at which the load can be applied, however for tests 
similar to this, it is recommended between 0.5 and 1.5 mm/minute 
(http://www.astm.org/Standards, 2010). 
3.5 Calculating Flexural Strength 
Flexural strength, considered as the strength under normal stresses, was determined by 
applying the following equation known from the strength of materials: 
R = 3P L Where, 
2bd² R = Modulus, measured in N/mm². 
P = Correct load indicated, Newtons. 
L = Span length between supports, mm. 
b = Width of beam, mm. 
d = Depth of beam, mm. 
(www.astm.org, 2009)
First crack 
0 0.15 0.30 0.45 0.60 0.75 0.90 1.05 1.20 1.35 1.50 
14 
4.0 Results and Analysis 
In this chapter the results for the flexural tests of the three groups are presented. Each groups 
individual beams maximum load, deflection and flexural strength have been placed in a table 
of results along with a graph representing the relationship between load and deflection. The 
results for the plain concrete beams are shown in Section 4.1. 
4.1 Results of Plain Concrete Beam Flexural Testing Programme. 
After completing the flexural test programme for the plain concrete beams, the results were 
recorded and are displayed below in Table 2. 
Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) 
Plain 1 10792.82 2.60 4.86 
Plain 2 11400.82 1.87 5.13 
Plain 3 13835.71 1.77 6.22 
Plain 4 11370.79 2.28 5.11 
Plain 5 13106.59 0.98 5.89 
Plain 6 11398.64 0.55 5.12 
Plain 7 10749.95 1.60 4.83 
Mean Value 11807.90 1.66 5.31 
Table 2. The table shows the maximum load, deflection and flexural strength for plain 
concrete beams. 
The maximum loads for the 7 plain beams were averaged and plotted against the average 
maximum deflection in the graph shown in Figure 3 below. 
14000 
12000 
10000 
8000 
6000 
4000 
2000 
0 
Load applied (N) 
Deflection mm 
Deflection (mm) 
Figure 3. Graph showing the relationship between load and deflection for plain concrete 
beams.
First crack 
0 1.50 3.00 4.50 6.00 Axi7s. 5T0it le 9.00 10.50 12.00 13.50 15.00 
15 
4.2 Results from using Wood Chippings as Addition to the Concrete Beams. 
The results for wood chippings alone are presented within Table 3 below. 
Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) 
Wood 1 6057.04 22.00 2.73 
Wood 2 8660.77 12.15 3.89 
Wood 3 10137.44 10.73 4.56 
Wood 4 5758.72 20.19 2.59 
Wood 5 6883.53 15.14 3.09 
Wood 6 7428.96 12.47 3.45 
Wood 7 6575.69 9.81 2.96 
Wood 8 8187.26 14.69 3.68 
Mean Value 7461.18 14.65 3.36 
Table 3. Results from the flexural testing programme for using wood chippings alone as an 
additive to concrete beams. 
As was done for the plain concrete group beams, the maximum loads for the 8 beams were 
averaged and plotted against the average maximum deflection in the graph shown in Figure 4 
below. 
8000 
7000 
6000 
5000 
4000 
3000 
2000 
1000 
0 
Load applied (N) 
Deflection (mm) 
Figure 4. Graph showing the relationship between load and deflection for concrete beams 
with wood chipping added
4.3 Results from using Wood Chippings and Silica Fume as Addition to the Concrete Beams. 
First crack 
0 1.50 3.00 4.50 6.00 7.50 9.A00x i s T 1it0le.50 12.00 13.50 15.00 16.5 18.00 
16 
The results recorded from the flexural testing of wood chippings and silica fume within 
concrete beams are presented within Table 4 below. 
Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) 
Hybrid 1 4115.64 22.36 1.85 
Hybrid 2 4454.58 23.44 2.01 
Hybrid 3 3665.14 19.99 1.65 
Hybrid 4 5561.08 17.44 2.50 
Hybrid 5 4217.87 19.35 1.89 
Hybrid 6 6531.98 12.41 2.93 
Hybrid 7 5463.34 14.89 2.74 
Hybrid 8 6100.41 19.52 2.89 
Hybrid 9 7310.51 19.36 3.29 
Mean Value 5268.95 18.75 2.41 
Table 4. Results from the flexural testing programme for using wood chippings and silica 
fume as an additive to concrete beams. 
The maximum loads for the 9 hybrid beams were averaged and plotted against the average 
maximum deflection in the graph shown in Figure 5 below. 
6000 
5000 
4000 
3000 
2000 
1000 
0 
Load applied (N) 
Deflection (mm) 
Figure 5. Graph showing the relationship between load and deflection for concrete beams 
with both silica fume and wood chippings added
17 
4.4 Overview of Flexural Strength Results. 
The table below gives an overview comparison between the 3 groups, comparing average 
maximum loads, maximum deflection and flexural strength. 
Group Average Max load 
(N) 
Average Max 
Deflection (mm) 
Average Flexural 
strength (N/mm²) 
Plain 11807.90 1.66 5.31 
Wood alone 7461.18 14.65 3.36 
Hybrid 5268.95 18.75 2.41 
Table 5. Showing the average results for the 3 groups maximum load, maximum deflection 
and flexural strength. 
When comparing the wood alone to plain concrete, the maximum load achieved is decreased 
by 36.8%, however the average maximum deflection reached before complete shear is 
increased by 782.5%. When comparing the hybrid concrete group average maximum load to 
the average for plain concrete maximum load, the maximum load before first crack is 56.5% 
lower. The position of first crack is shown in Figures 3, 4 and 5. However, the maximum 
deflection recorded for the hybrid concrete beams is 1029.5% greater than that of the plain 
concrete beams. The flexural strength of the hybrid beams decreased by 55.6% when 
compared to the plain beams. The flexural strength of the beams with wood chippings alone 
decreased by 37.7% when compared to the plain group. 
4.5 Analysis of Results. 
In order to explain these results, a more detailed look at what is happening to the beams must 
be taken. As presented within the literature review, Section 2.3, silica fume undergoes a 
pozzolanic reaction, improving the bonds between the cementitious materials to the wood 
reinforcement. The improvement of the bonds between the wood and the concrete suggests 
this is why maximum deflection values are increased even between the wood chipping 
beams, and the hybrid beams, as the bonds are stronger and pull out is resisted further. The 
term ‘pull out’ refers to the wood reinforcement being de-bonded from the concrete due to 
the load applied, and removed without the wood breaking. Plate 1 below shows a photograph 
of a beam that exhibits pull out after it had failed and had been removed from the flexural 
testing machine. 
Plate 1. Photograph of a failed beam showing pull 
out of the wood reinforcement 
Large areas are left where the wood 
chipping reinforcement has been de-bonded 
and pulled out from the 
concrete beam.
Here, a length of wood chipping is shown 
to have been pulled out from the concrete 
beam 
It can be seen here that wood chippings 
within the beam are spanning the crack and 
acting as reinforcement to the beam. 
18 
Plate 2, shows a concrete beam where it possible to see the wood chippings within acting a 
reinforcement to the beam. 
Plate 2. Shows the wood waste within the 
beam acting as reinforcement. 
Whilst the addition of silica fume increased the maximum deflection, it also reduced the 
maximum load the beams can withstand as well as reducing the flexural strength. The basic 
theory of concrete flexural strength is that flexural strength of concrete decreases as density 
decreases, (Rossignolo, 2002. Park, 1975). This may potentially explain the reason the plain 
concrete groups flexural strength is higher, as the density of the wood chippings present in 
the other two concrete group beams being a lot less than that of concrete, therefore reducing 
the density of the beam. The next section will consider the density of the beams as a reason 
for reduced flexural strength. 
4.6 Determining the Density Characteristics of the Concrete Mixes. 
After the beams were taken out of the moulds for testing they were weighed, and from this 
the density could be calculated. Figure 6 below shows the densities of the 3 groups. 
2500 
2400 
2300 
2200 
2100 
2000 
1900 
1800 
Plain Wood alone Wood & Silica fume 
Density (kg/m³) 
Density kg/m³ 
Figure 6. Bar chart showing the density of the 3 concrete groups after 28 days.
Comparing the plain beam densities, to that of the wood chipping group it can be shown that 
a 9.30% reduction in density is achieved. The hybrid beams have a 6.60% reduction in 
density compared to the wood alone, and a 15.30% reduction compared to the plain group. 
Table 6 below shows averages across the 3 groups for maximum load, maximum deflection, 
flexural strength and also density. 
19 
Group Average Max 
load, (N) 
Average Max 
Deflection,(mm) 
Average Flexural 
strength (N/mm²) 
Density (kg/m³) 
Plain 11807.90 1.66 5.31 2380 
Wood 7461.18 14.65 3.36 2160 
Hybrid 5268.95 18.75 2.41 2040 
Table 6. Shows averages for maximum loads, deflections, flexural strength and density. 
By presenting data from Table 6 in graphical form, such as Figures 7 and 8. It is possible to 
see that density and load are proportional, as well as density and flexural strength, as the lines 
on both graphs are straight. 
2500 
2400 
2300 
2200 
2100 
2000 
1900 
1800 
Wood 
Hybrid 
2 3 4 5 
Density (kg/m³) 
Flexural strength (N/mm²) 
Plain 
Figure 7. Graph showing the relationship between density and flexural strength for the three 
groups tested.
20 
2500 
2400 
2300 
2200 
2100 
2000 
1900 
1800 
Hybrid 
Wood 
Plain 
5115 
5480 
5845 
6211 
6576 
6941 
7306 
7672 
8037 
8402 
8767 
9133 
9498 
9863 
10228 
10594 
10959 
11324 
11689 
Density (kg/m³) 
Maximum load, (N) 
Figure 8. Graph showing the relationship between density and maximum load for the three 
groups tested. 
This means that by adding wood chippings to the mix, the density is reduced and this in turn 
reduces the flexural strength of the concrete. However by adding silica fume, the bonds at the 
interface between the concrete and the wood are improved, thus further deflection is 
measured before failure. 
Whilst the data above gives reason to why the flexural strength is the reduced with the 
addition of wood chippings, the hybrid group’s average maximum load and flexural strength 
decreases further than that of the wood chippings alone, this is an unexpected result as the 
same weight of wood chippings was use for both of the groups. One reason for this could be 
that although the same weight of wood chipping was used, the volume of the wood chippings 
may have increased; this would explain the drop in density therefore the decrease in flexural 
strength. However, other reasons may be established by looking at the rate of drying for all 
beams. The next section will consider the drying curves for the beams. 
4.7 Drying Curves. 
This section will look at the drying rates for the 3 groups and analyse factors that influence 
the final density of the beams. Figure 8 below shows the rate at which each group of beams 
dried out over 28 days.
21 
3000 
2500 
2000 
1500 
1000 
500 
0 
Density kg/m³ 
Days 
Plain 
Series1 
Wood 
Series2 
Series3 
0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 
Days 
Hybrid 
Figure 8. Graph showing the drying curves for the 3 groups over a 28 day drying period 
From the graph it is possible to see that the hybrid beams dry out and lose density the more 
rapidly over the 28 day drying process. Research by Kadri (2009) suggests that the presence 
of the silica fume in concrete will accelerate exothermic reactions during the hydration 
process. Exothermic reactions begin to occur when the cement first comes into contact with 
water in the mix and heat is produced. The main reaction that occurs is between the aluminate 
within the Portland cement, and water. This reaction forms an aluminate-rich gel; the gel will 
then react with sulphates within the solution to form what is known as ettringite 
(http://www.understanding-cement.com/hydration.html, 2010). Ettringite is a crystal like 
structure and forms in microscopic needles such as shown in Plate 3. 
In the photograph microscopic needles 
of white ettringite can be seen forming 
in tiny air voids within concrete. 
Plate 3. Photograph showing the microscopic needles 
of ettringite. (Taken from http://www.cement.org/tech, 
2010)
The silica fume within the concrete was added to improve the bond between the concrete by 
drawing in the ettringite needles to the woods surface in accordance to the findings of section 
2.1.1 of the literature review. However, this has meant that the spaces within the concrete 
where the ettringite crystals were before being drawn to the wood chippings are now tiny air 
voids (http://www.cement.org/tech, 2010). With these air voids present in the concrete, it is 
suggested that the concrete beams are able to dry out faster, become less dense and will have 
less flexural strength due to this. The hybrid beams have exhibited all of these properties, 
being less dense than both the other groups, and having a smaller flexural strength value than 
the plain concrete and the concrete with only wood chipping added. 
From this chapter it is possible to see clear differences between the plain, wood chipping 
alone and hybrid mixes. The results have been analysed and contextualised against our 
current knowledge of concrete materials behaviour and structure. From doing this it can be 
suggested that the introduction of silica fume to a mix can improve the deflection reached 
before complete failure occurs. It can also be suggested that silica fume and wood chippings 
decrease the flexural performance of concrete beams due to the decrease in density. 
22 
Chapter 5 will conclude the research and reflect upon the hypothesis, research aims and 
objectives of the flexural testing programme.
23 
5.0 Conclusions 
In this study the effects of adding waste wood chippings and silica fume to concrete were 
investigated and analyzed. The aims of the study were see if the use of waste wood chippings 
from the timber industry and the addition of silica fume, would improve flexural performance 
of concrete, or not. The main objectives of the study were (1) to test 10 concrete beams with 
no reinforcement, (2) test 10 concrete beams with waste wood chipping added as 
reinforcement (3) test 10 concrete beams with waste wood chipping and silica fume added as 
reinforcement, (4) to record the results appropriately, (5) to compare and analyse the 3 groups 
of test results and (6) to evaluate the effectiveness of adding waste wood chippings and silica 
fume to concrete mixes. By conducting testing in accordance with the method presented in 
Chapter 3, results of the flexural testing programme were obtained and analysed in Chapter 4. 
From analysing the results of the flexural testing programme carried out, the following 
conclusions were derived. 
1 The results of the flexural testing programme indicate that the addition of wood 
chippings and silica fume does not improve the flexural strength of concrete, the 
values for both wood chipping and silica fume groups were lower than that of 
plain concrete. 
2 The addition of wood chipping alone improves maximum deflection, compared to 
plain concrete. 
3 The addition of wood chippings and silica fume improves maximum deflection by 
the greatest value. 
4 Due to the addition of silica fume, ettringite crystals are drawn towards the wood, 
leaving air holes, reducing density and strength even further than wood chippings 
alone. 
The hypothesis in Section 1.1, suggested that if waste wood chippings and silica fume is 
added as reinforcement to a concrete beam, then the flexural strength of concrete beams will 
be improved. From the conclusions drawn, this can be rejected. The aims of the investigation 
stated in section 1.2 have been met, and the objectives stated in Section 1.3 have also been 
achieved. 
Although the hypothesis for this investigation was rejected, this study shows feasibility for 
producing a more sustainable concrete. There are many different reasons for the results 
obtained from this investigation; there are also many opportunities for further research and 
testing to be carried out within this area. Section 6.0 will suggest recommendations for 
further studies. 
5.1 Research Limitations 
The data gather from the flexural testing programme made for interesting analysis. By 
collecting data from previous similar studies in the literature review and compiling the 
methodology, it is apparent that many variations could be made within this research, with 
reference to mix design and testing methodology. 
It was extremely difficult to acquire the silica fume, as it was necessary for it to be shipped 
from Holland, in only very small amounts. With more accessibility to silica fume, further 
testing could have been conducted using different amounts of silica fume. 
Another major limitation was the time available to test concrete within the laboratories, as 
compression testing on concrete cubes would have provided a further insight into the effects
of adding waste wood and silica fume to concrete. If more time was available, a further 10 
beams would have been tested using silica fume as the only addition to the concrete mix, to 
allow for comparisons to the concrete beams with wood chipping alone and the hybrid 
concrete beams. It would also be useful to measure the flexural strengths of the 3 groups of 
concrete after a 60 day curing period, as this is suggested to increase flexural strengths further 
(Naik, 2002). 
Whilst this chapter has concluded the findings from this research and assessed the limitations. 
The next chapter will consider recommendations for future research. 
24
25 
6.0 Recommendations for Future Research 
The replacement of cement by materials that induce a pozzolanic reaction, such as fly ash 
Naik (2002), or silica fume, can have advantages for both sustainability and to the strength of 
concrete. Although this investigation rejected the hypothesis that suggested that if waste 
wood chippings and silica fume is added as reinforcement to a concrete beam, then the 
flexural strength of concrete beams will be improved, it is still important to drive forward 
sustainability issues by means of reducing carbon emissions, reducing materials used and 
costs of production. There are many different variations to the methodology of the flexural 
testing programme undertaken within this study, with reference to the mix design. This 
chapter will address these variations in order to recommend and benefit future studies within 
this area. 
By varying the content ratios between the water, silica fume and waste wood chippings is 
suggested to give different results for both flexural strength tests and compressive strength 
tests. (Schulze, 1999, Beton, 1990., Pascal et al., 2004. and Van Gemert et al. 2005) 
With reference to the mixing method of the batches, it is suggested that pre soaking the wood 
chippings to draw cementitious particles into the wood will improve the bond between the 
wood and the concrete further than if no pre soaking takes place, (Reis, 2006). As well as 
varying the method of adding the wood, the method of which the silica fume was batched 
could also be altered, for this research the silica was batched in accordance to the 
manufacturer and supplier, however there are different suggestions to mixing which 
potentially increase the strength of concrete, (Blanksvard, 2009). 
The above recommendations provide platforms for future research to improve upon current 
knowledge of concrete behaviour, and can potentially lead to more sustainable methods of 
making concrete. The recommendations made, are based upon researchers conducting tests 
without the limitations this paper has identified in Section 5.1.
26 
7.0 References. 
http://www.astm.org/Standards (2010) (Accessed 23 March 2010) 
Becchio, C. (2009) Improving environmental sustainability of concrete products, 
investigation of MWC thermal and mechanical properties. Published doctorate. Turin 
polytechnic, Italy. 
Bjork, F. (1999) ‘Concrete technology and sustainable development’ Vancouver symposium 
on concrete technology and sustainable development. December 1999. p.5. 
Blanksvard, T. (2009) Strengthening of concrete structures by the use of mineral based 
composites. Published doctoral thesis. Lulea University of technology. 
http://www.brmca.org.uk/downloads/Mpa_Placing_PrintR (2009) (Accessed 24 March 2010) 
Carette, G., (1993) “Mechanical Properties of Concrete Incorporating High Volumes of Fly 
Ash From Sources in the U.S” November 1, 1993. 
http://www.cement.org/tech, (2010) (Accessed 26 March 2010) 
Chitchumnong P, Brooks S.C., Stafford G.D. (1989), ‘Comparison of three- and four-point 
flexural strength testing of denture-base polymers’ Dental Materials Pp2-5 
Coatanlem, P. (2005) Lightweight wood chipping concrete durability. Published masters. 
Department of civil engineering. Rennes, France. 
Galetakis M. and Raka S., (2004) ‘Utilization of limestone dust for artificial stone 
production: an experimental approach’ Minerals Engineering 
Gemert V, D., Czarnecki, L., Maultzsch, M., Schorn, H., Beeldens, A., Lukowski, P and 
Knapen, E. (2005) Cement concrete and concrete–polymer composites: Two merging worlds: 
A report from 11th ICPIC Congress in Berlin, 2004. Cement and Concrete Composites 
Wendehorst, R. (1992) Baustoffkunde. Weinheim, Germany. 
Huang Cheng-yi and R.F. Feldman. (1985) Influence of silica fume on the micro structural 
development in cement mortars. Science direct [online]. Available at: 
https://www.sciencedirect.com (Accessed: 8 January 2010) 
http://www.instron.co.uk/wa/application /flexure (2010) (Accessed 22 March 2010) 
Johansson, J. (2005) ‘End peeling of mineral based CFRP strengthened concrete structures- a 
parametric study.’ Proceedings of the international symposium on bond behaviour of FRP in 
structures. BBFF 2005. 
Kadri, E., Duval, R., (2009) ‘Hydration heat kinetics of concrete with silica fume 
Construction’. Building Materials. Volume 23, Issue 11, November 2009. 
Miller, R. H., and Collins, R. J., (1975) “Waste Materials as Potential Replacements for 
Highway Aggregates,” NCHRP Report No. 166. 
Naik, T.R. (2002) ‘Greener concrete using recycled materials’ Concrete international. July 
2002.
27 
http://www.nrmca.org/aboutconcrete (2005) (Accessed 22 March 2010) 
Pascal, S., Alliche, A and Pilvin, Ph. (2004) ‘Mechanical behaviour of polymer modified 
mortars’ Materials Science and Engineering. Elsevier B.V. 
Rao, G. (2003) Investigations on the performance of silica fume-incorporated cement pastes 
and mortars. Swetswise [online]. Available at: https://www.swetswise.com (Accessed: 8 
January 2010) 
Reis, J.M.L. (2006) ‘Fracture and flexural characterisation of polymer concrete reinforced 
with wood waste’ Brazilian congress for engineering and science materials. November 19. 
Pp 2871-2878 
Rim, A. Ledhem, O. Douzane, (1999) R.M. Dheilly and M. Queneudec, ‘Influence of the 
proportion of wood on the thermal and mechanical performances of clay–cement–wood 
composites’, Cement and Concrete Composites. 
Rossignolo J.A, Agnesini M.V.C. (2002) ‘Mechanical properties of polymer-modified 
lightweight aggregate concrete’. Cement and Concrete Research. Volume 32, Issue 3. 
Schulze, J. (1999) ‘Influence of water-cement ration and cement content on the properties of 
polymer-modified mortars’ Cement and Concrete Research. 
Shao Y., Lefort T., Moras S. and D. Rodriguez, (2000) ‘Studies on concrete containing 
ground waste glass’ Cement and Concrete Research. Volume 30, Issue 1 
Shayan A., (2004) ‘Value-added utilization of waste glass in concrete’, Cement and Concrete 
Research. Volume 34, Issue 1 
Soroushian P., Plasencia, J and S. Ravanbakhsh (2003) ‘Assessment of reinforcing effect of 
recycled plastic and paper in concrete’ ACI Materials Journal. 
Topcu I.B. and Canbaz M., (2004) ‘Properties of concrete containing waste glass’ Cement 
and Concrete Research. Volume 21, Issue 7 
Tliljsten et al. (2006) ‘Strengthening of Concrete Beams in Shear with Mineral Based 
Composite Laboratory Tests and Theory’ Third International Conference on FRP 
Composites in Civil Engineering 
Turgut P., (2007), ‘Cement composites with limestone dust and different grades of wood 
sawdust’, Building and Environment
28 
8.0 Appendix 1.

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Dissertation

  • 1.
  • 2. 2 UNIVERSITY OF NORTHUMBRIA AT NEWCASTLE SCHOOL OF THE BUILT ENVIRONMENT The Effects of Adding Waste Wood Chippings and Silica Fume to the Flexural Strength Capacity of Concrete A DISSERTATION SUBMITTED TO THE SCHOOOL OF THE BUILT ENVIRONMENT IN PARTIAL FULFILMENT OF THE REQUIREMENTS FOR THE DEGREE OF BSc Architectural Technology By 06012242 APRIL 2010
  • 3. 3 Abstract This piece of research investigates the effects of adding waste wood chippings form the timber industry, and silica fume, to the flexural strength capacity of concrete. Three groups of concrete beams were made, group 1 consisting of plain concrete, group 2 had wood chippings added to the mix and group 3 was a hybrid of wood chippings and silica fume. After compiling a suitable methodology and carrying out a flexural test programme, results showed that additions of wood and silica fume reduce flexural strength, however wood and silica additions are shown to increase maximum deflection before failure of the concrete beams. The results were encouraging towards the research and production of more sustainable concrete technologies. i
  • 4. 4 Table of Contents Abstract i 1.0 Proposal 5 1.1 Hypothesis 5 1.2 Research Aims 5 1.3 Objectives 6 2.0 Literature Review 7 2.1 An overview of sustainable concrete 7 2.1.1 Fly Ash Concrete 7 2.1.2 Wood Chippings in Concrete 8 2.2 Flexural Testing of Fly Ash and Wood Chip Concrete 8 2.3 Mineral Based Composites 9 2.4 Optimum Ratios 9 2.5 Conclusion 9 3.0 Methodology 10 3.1 Structural Elements and the Need to Perform Flexural Testing 10 3.2 Production of Beams 10 3.2.1 Materials 10 3.2.2 Mix Design 11 3.2.3 Quantities 11 3.2.4 Slump Testing 11 3.2.5 Pouring and Compacting the Concrete 12 3.3 Curing 12 3.4 Methods of Performing Flexural Tests 12 3.4.1 Loading Rate 13 3.5 Calculating Flexural Strength 13 4.0 Results and Analysis 14 4.1 Results of Plain Concrete Beam Flexural Testing Programme 14 4.2 Results from using Wood Chippings as Addition to the Concrete Beams 15 4.3 Results from using Wood Chippings and Silica Fume as Addition to the Concrete Beams 16 4.4 Overview of Flexural Strength Results 17 4.5 Analysis of Results 17 4.6 Determining the Density Characteristics of the Concrete Mixes 18 4.7 Drying Curve 20 5.0 Conclusions 23 5.1 Research Limitations 23 6.0 Recommendations 25 7.0 References 26 8.0 Appendices 28
  • 5. 5 1.0 Proposal There has been extensive research into trying to increase the sustainability of concrete whilst retaining high levels of flexural strength. The core of this research seems to be investigating the use of mineral based composites (MBCs). Research conducted by Blanksvard (2009), highlights the drawbacks of using epoxies, and concludes that in compressive strength tests that MBCs contribute to increasing load bearing capacity for strengthened concrete considerably. Further research into MBCs reveals that there is actually however, conflicting results to the levels of strength improvement in concrete. One such study tested flexural strength as oppose to compressive and concluded that the ‘stress at the cut off point is considerably smaller for the MBC system compared to that of the epoxy based carbon fibre reinforced polymer (CFRP) system’ (Johansson, 2005). Increased research into mineral bonding agents (MBAs) brings to attention that the use of fly ash in concrete is very common practice, as well as other recycled agents such as crushed glass and silica fume. A research paper on the effects of fly ash in concrete concluded that each tonne of cement that can be replaced by fly ash reduces CO² emissions by 1 tonne also (Bjork, 1999). Another piece of research also uses fly ash as well as mixing in waste wood ash, replacing 25-35% of cement used. This was found to significantly improve the performance of concrete in both compression and flexural testing (Naik, 2002). A research publication that tested the effects of untreated sawdust as an additive to polymer concrete, concluded wood waste did improve flexural strength and fracture toughness when applied as reinforcement to polymer concrete, (Reis, 2006). However, this is thought not to be the same case for compression, as research by Becchio (2009), concluded that when wood waste was used as an aggregate, compression strength tests indicate a reduced performance in mechanical properties such as crushing resistance and bulk density. Research by Coatanlem (2005), and concluded that by saturating wood chippings with sodium silicate, improves significantly the compressive strength of concrete. However, it also concluded that without the sodium silicate, the compressive strength was reduced. This is thought to be as the sodium silicate improves the bond between the wood – cement interface. This research conducted tests on compression alone, failing to expand the investigation beyond this parameter. Therefore the behaviour of this mix design on flexural strength has to be investigated. As no tests have currently been done on flexural performance and with conflicting research conclusions, a further investigation may be proposed to research into the effects of using untreated wood chippings as reinforcement, with the additive of silica fume to improve the bond interface, thus filling this knowledge gap. 1.1 Hypothesis It is suggested that if waste wood chippings and silica fume is added as reinforcement to a concrete beam, then the flexural strength of concrete beams will be improved. 1.2 Research Aims To test to see if the use of waste wood chippings from the timber industry and the addition of silica fume, can improve flexural performance of concrete.
  • 6. 6 1.3 Objectives 1) To test 10 concrete beams with no reinforcement 2) To test 10 concrete beams with waste wood chipping added as reinforcement 3) To test 10 concrete beams with waste wood chipping and silica fume added as reinforcement 4) To record results appropriately 5) To compare and analyse the 3 groups of test results 6) To evaluate the effectiveness of adding waste wood chippings and silica fume to concrete mixes. The following chapter will consider existing research into sustainable concrete, looking at the additions of by-products to concrete to improve sustainability as well as maintaining adequate levels of strength.
  • 7. 7 2.0 Literature Review This chapter intends to review existing pieces of research into the production of sustainable concrete. The need for sustainable concrete and the search for suitable by-products, with specific reference to mineral based composites, will be addressed within this chapter. Extensive research has been carried out into trying to increase the sustainability of concrete, Li-hua (2009), Naik (2002), Becchio (2009), Turgut (2007), whilst retaining high levels of both compressive and flexural strength. The following section will outline research that has been conducted into improving sustainability of concrete whilst trying to retain high compressive strength values. 2.1 An Overview of Sustainable Concrete. Research carried out by Canbaz et al. (2004) used waste glass, as a course aggregate within concrete. The glass used was between 4-16mm and used in a mix proportion of up to 60%. Testing of this determined that it actually had a slight reduction in compressive strength. A study was conducted by Shayan (2002) looks at glass ground in to a fine powder and added to the mix, replacing 30% of the cement used. The results from this test found that this did provide a significant increase to the concrete’s compressive strength. In addition to this, Soroushian et al, (2003) found that the addition of recycled plastics also has a positive effect of concrete compressive strengths. Galetakis (2004) also conducted compression tests using limestone dust as an addition with Portland cement mix, while the dust/cement ratio was found to be the key factor, results showed that compressive strengths can be increased. The studies discussed above show that many materials have been used as aggregates in concrete. However, whilst many different pieces of research have been carried out using different waste materials as additions to the concrete mix, the most extensive amounts with the most positive results, come from testing carried out using ash or wood chipping additions. Focusing on compression tests, the next section reviews studies that have used ash as an addition to the concrete mix. 2.1.1 Fly Ash Concrete Very early research was carried out by Miller et al. (1975) into the use of fly ash, as well as other reclaimed materials, as alternative aggregates. The research found that fly ash offered the most improvement to concretes compressive strength. The most recent and in depth piece of research conducted undertaken by Naik (2002) using fly ash alone, tests were conducted using between 25-35% of fly ash blended with the concrete mix. After a 28 day curing period it was concluded that the compressive strength of the concrete was significantly increased. Research previous to this was also carried out by Carette (1993) using between 55-60% fly ash in a concrete mix, concluded that after 91 days curing that the concretes compressive strength was up to 50 N/mm². However, another study conducted by Bjork (1999) found that by using a water/cement ratio of 0.3, can have as much as 60% of the cement replaced with fly ash and can produce a 55 N/mm² a compressive strength concrete after 28 days. A study by Li-hua (2009) confirmed that the addition of fly ash content between 10-55% will improve compressive strengths as well as improving workability and durability, however more than 55% content will reduce compressive values after 90 days, as the compressive strength of fly itself is less that concrete. The above research shows that the addition of fly ash to concrete can significantly improve compressive strength; this is because fly ash is comprised of the non-combustible mineral portion of coal consumed in a coal fuelled power plant. The particles are glassy and spherical
  • 8. shaped that are typically finer than cement particles. The fly ash undergoes a ‘pozzolanic reaction’ with the lime created by the hydration (chemical reaction) of cement and water, to create the same binder (calcium silicate hydrate) as cement. The pozzolanic reaction that takes place is the fly ash changing into a siliceous material that reacts with the lime, forming a compound that is cementitious at normal temperatures. It is this pozzolanic reaction that will be looked at in section 2.3, when silica is looked at as a mineral based composite. After looking at the effects of fly ash, as previously mentioned, the addition of waste wood also has had extensive research carried out on its effect to compressive strengths on concrete. Section 2.1.2 will give an overview to these. 8 2.1.2 Wood Chippings in Concrete Research by Becchio (2009) tried to increase sustainability of concrete by replacing natural aggregates in the mix, with waste wood chippings. Different mix proportions were of cement/admixture/water was made and cubes formed. Their compressive strength was tested after a 28 day curing period. The testing concluded that in all cases the addition of wood waste decreased the compressive strength of the concrete, the decrease in strength was found to be in proportion to the drop in density as wood in less dense than aggregate. A previous study to this was performed by Turgut (2007) who investigated the use of high levels of waste sawdust to concrete mixes, and the results obtained were enough to satisfy international standards. Although this test does not increase the compressive strength, it shows that equal strengths can be achieved by using sustainable methods. A much earlier piece of research was carried out by Al Rim et. al. (2000) also reused wood waste as an aggregate for concrete, although the research was aimed at the thermal properties of this, it did conclude that the addition of the wood waste reduced the compressive strength. The studies and tests in the previous paragraph show contradicting results for the addition of wood wastes to the concrete mixes, this could be due to a number of factors. However, all of the previous research looked at, measured concrete under compression testing. The next section will focus on tests that have been carried out to increase the flexural strength of concrete, and see if the same materials have the same effects. 2.2 Flexural Testing of Fly Ash and Wood Chip Concrete Coatanlem (2002) conducted research using waste wood chippings as fibres for concrete reinforcement. The wood chippings were between 0.5-10.0mm and the beams were 40x40x160mm. The optimum wood/cement ratio was 3.6, and the optimum water cement ratio was 0.75. After 28 days, the beams were tested and it was found that the flexural strength of all the samples was less than 10MPa; this is a significant reduction to that of normal Portland cement, recording 45MPa. Research by Reis (2006) tested plain epoxy polymer concrete reinforced with wood waste. Mixes were made with varying proportions of cement and waste wood. Flexural strengths were then tested and compared to that of plain epoxy polymer concrete. The results obtained showed that flexural strength increased by 6.03%. The comparison between the two above studies by Coatanlem (2002) and Reis (2006) show that wood chippings alone will not increase the flexural strength of concrete, but adding wood waste to an epoxy polymer concrete will improve the strength. However, the use of epoxy concrete poses disadvantages such as hazardous working environments for the workers, as well as being sensitive to moisture and thermal conditions, (Tliljsten et al. 2006).
  • 9. 9 The next section will discuss research into Mineral based Composites; these are designed to be a more sustainable, replacement to epoxy adhesives. 2.3 Mineral Based Composites Blanksvard (2009) has carried out extensive research into the use of Mineral Based Composites (MBCs) as an addition to carbon fibre reinforced concrete. The first part of his research uses MBCs as a strengthening system to repair concrete. However flexural tests were also conducted within this research to expand the data collection. This research concluded that the uses of minerals, such as silica fume, improve the bond between the cement, to the reinforcement fibres. The reaction that improves the bond is the same as discussed in section 2.1.1, as the use of minerals like silica fume undergoes a pozzolanic reaction. This result would explain the difference in the two previously discussed tests carried out by Coatanlem (2002) and Reis (2006), as Reis used the wood chippings in epoxy concrete, so the epoxy would have created a stronger bond between the cement and the wood chippings. Blanksvard also concluded that for flexural strength to be improved, optimum ratios of water/cement and also polymer/cement ratios need to be found. These are addressed in the following section. 2.4 Optimum Ratios Research conducted by Schulze (1999) show that the flexural strength of concrete can be increased substantially by altering the water/cement ratio, within a modified mortar. This confirmed earlier research by Beton (1990). Research into polymer/cement ratios was conducted by Pascal et al. (2004) and Van Gemert et al. (2005) who found that increases in flexural strength were found significant when polymer/cement ratios were between 10% and 15% weight content. Ratios higher than this are shown to result in a decrease in the strength properties. The research by Pascal et al. (2004) and Van Gemert et al. (2005) confirmed the earlier findings from Rao (2003) and Huang Cheng-Yi et. al. (1985), whose work addressed the performance of silica fume within concrete. Both of these researchers tested silica fume levels between 0% and 30% content by weight within a mix and found that optimum levels for increasing flexural strength lie between 15% and 22% by weight. 2.5 Conclusion From the research presented, it has been shown that the flexural strength of concrete can actually decrease by replacing aggregates and fibres with only recycled materials such as wood, ash and glass. It has also been shown that in many cases the addition of epoxies and Mineral Based Composites can then go on to increase the flexural strength of concrete as the bond between the recycled fibres and the cementitious material is strengthened. Further research into these bonds concluded that water/cement and polymer/cement ratios are of significance to the flexural strength. The use of Mineral Based Composites, such as silica fume, increase sustainability of concrete as it is a by product of producing silicon metal. Silica fume also increases workability, compared to an epoxy resin. The tests looked at above use silica fume with polymer fibres, and no tests were found that adopted silica fume as an additive to concrete reinforced with waste wood chippings acting as a fibre addition. The study by Reis (2006) did use wood chippings, but with epoxy concrete. The intention of this work is to address the knowledge gap in the research, as presented within this chapter, by exploring the use of silica fume as an epoxy replacement to concrete reinforced with waste wood chippings. Chapter 3.0 identifies the methodology used to explore this work.
  • 10. 10 3.0 Methodology The previous chapter indentified an apparent lack of data on sustainable methods to improve the flexural strength of concrete, with specific reference to the use of silica fume and waste wood chippings. This chapter will justify the use of a flexural test programme and determine the materials used in the production of the beam test programme in address. 3.1 Structural Elements and the Need to Perform Flexural Testing From research presented in the literature review, it is shown that tests have been carried out on improving both compressive and flexural strengths of concrete. However the research presented does not focus on increasing the sustainability of concrete. In order to collect data for the improvement of flexural strength of a concrete beam then a test was required. Whilst other forms of data collection, such as comparing case studies, may have given an indication of what is likely to happen to the flexural strength, actual first hand data could not be obtained without testing. There are also a number of different practical uses for flexural strength improvement, as concrete is widely used as a material for structural elements such as beams and other framing members. It is important that when adopted for this type of application, it can withstand loads without failing. Beams spanning across any length within a building will be under flexural loading, whether it be carrying dead or live loads. With a huge pressure on the modern day construction industry to increase sustainability and reduce carbon emissions, it is important that methods for meeting sustainability criteria are explored without compromising strength. The implications of this are that higher strength and sustainability within concrete will offer greater opportunities for architects, technologists, contractors and clients to want to use concrete. As well as this, with higher flexural strengths, larger spans can be reached allowing architects to design more diverse buildings. The next chapter will look at the how the beams to be tested were produced. 3.2 Production of Beams As discussed within the literature review, beams will be tested with the addition of waste wood chippings and silica fume. The following sections will look at beam design, including acquiring the materials, ratios of materials used and the quantities of beams made. 3.2.1 Materials The wood chippings that were added to the mix came from a local timber merchant, and were ungraded, untreated and from a variety of trees. The decision to use chippings like these was to add to the sustainability of the beams, as costs are incurred to sort and grade the wood, as well as treat it. The idea was that the wood chippings were used as ‘raw’ waste from the timber industry. The silica fume was obtained from an international chemical company who specialize in making environmentally friendly metals and materials. The silica fume used was undensified meaning that the grains are slightly larger than those of densified silica, also the undensified silica fume is easier to work with and offers no hazardous working conditions with regard to skin contact and inhalation. The silica fume fully conformed to the American Society for testing Materials code C1240 for the Standard Specification for Silica Fume Used in Cementitious Mixtures (ASTM C1240 -05). The cement used was ordinary Portland cement which conforms to BS 12, this was the same as all of the tests presented within the literature review and is the most readily available to use. The aggregates, sand and water were all readily available from the universities laboratory.
  • 11. 11 3.2.2 Mix Design As presented in the literature review Schulze (1999) and Rao (2003) showed that optimum ratios of water/cement and silica fume/cement can have major influences on the flexural strength of concrete. The optimum silica fume amount was found to be between 15-22% of the mix, however later research by Van Gemert et al. (2005) suggested 15% of a silica addition was the maximum before a decrease in flexural strength would appear. For that reason a 15% addition was added to the mix. The ratio of wood chippings to the mix was chosen at cement/wood ratio of 3. This was due to recent research by Becchio (2009) suggesting this was the optimum ratio. Earlier research by Coatanlem (2002) as presented in the literature review suggested 3.6, however this was also rounded down to 3 for the testing. This research also concluded that the optimum water/cement ratio was 0.75 so in order to maintain validity the same ratio was used. The ratio of mix between cement/sand/gravel was 3/6/10 in accordance to BS 8500. For all beams made, the cement sand and gravel were mixed first, and then the correct amount of water added accordingly. Mixing was followed by the addition of the wood chippings to the batches that included both wood and silica fume. The silica fume was added last and mixed in full accordance with the manufacturer’s guidelines for mixing (See Appendix 1). 3.2.3 Quantities With the above ratios used, this section will look at exactly how much of each material was added to the mix. 30 beams were made in total, 10 beams in a control group with plain concrete. 10 beams with wood chipping alone and the final 10 beams were a hybrid of silica fume and wood chipping. The decision to use 10 beams within each group was made by looking at research in the literature review, where research carried out by Shayan (2002), Galetakis (2004), Naik (2002) and Becchio (2009) all used between 6 and 10 specimens for each group. By using 10, it is also easier to identify any anomalous results and calculate levels of significant difference between groups. Table 1 below shows the quantities for all materials used. All amounts are based on batching 10 beams per group and include a 10% waste addition. Cement Sand Gravel Wood Silica Fume Water Plain group 21.56kg 38.81kg 58.00kg 0.00kg 0.00kg 16.17kg Wood alone 21.56kg 38.81kg 58.00kg 21.56kg 0.00kg 16.17kg Hybrid 21.56kg 38.81kg 58.00kg 21.56kg 3.25kg 16.17kg Table 1. 3.2.4 Slump Testing A slump test measures the workability of the concrete, showing how easy the concrete is to place handle and compact. Slump tests must measure within a set range or tolerance from the target slump. A slump test was not carried out within this experiment as the mix would give different slump values due to the wood and silica additions and no target slump are values are specified for this type of mix. As well as this, all the quantities of materials were carefully measured and mixed in the exact same way; there were also time constraints within the laboratories making it difficult to complete a slump test. For producing plain concrete without limitations, a slump test must always be carried out.
  • 12. 12 3.2.5 Pouring and Compacting the Concrete. All beams dimensions were the same at 100mm x 100mm x 500mm; this size was chose as it was the same dimensions as flexural testing carried out by Reis (2006). Pouring the concrete into the moulds must be carried out in a precise method. Using a trowel, the beams moulds were filled half way then compacted using steel hand tamp. Compaction takes place in order to reduced air content within the concrete, improving its performance, there should be a minimum of 100 compactions before pouring the remaining half into the mould, before a further 100 compactions are made (www.brmca.org.uk/Placing, 2009). The beam should be finished with a float to remove excess mix from the edges of the mould, this makes it easier to remove the beams from the moulds after curing. This process was repeated for each beam. 3.3 Curing The curing period for the beams was 28 days; this was the same as all of the tests presented in the literature review. 28 days is also the advised time given by Portland cement (http://www.concrete.net.au, 2004). During the curing period, the mass of each beam was obtained by weighing the beams every 2 days in order to monitor their change in mass over the 28 day period. This gave the opportunity to look at the beams’ densities and compare differences between the groups. 3.4 Methods of Performing Flexural Tests. The two main methods of testing flexural capacity of concrete are known as either the ‘single point’ load test or the ‘third point’ load test. Figure 1 below shows diagrammatically the two tests.. A B Figure 1. Flexure testing diagrams (Taken from www.nrmca.org/aboutconcrete, 2005) Figure 1A, shows the third point test as it applies the loads across two points at one third proportions of the beam. Figure 1B shows the single point test where the entire load is applied to the centre of the beam. With a brittle material such as concrete, the single point test is more common, although this test only provides data for flexural strength only, not stiffness (http://www.instron.co.uk/application /flexure, 2010). Research was also carried out into the difference between single point and third point tests, concluding that after testing 4 different types of polymers, that between the two tests no significant difference could be found in the results for modulus of rupture, (Chitchumnong et al. 1989). Figure 2 below shows the difference in between the two types of flexural test, displayed using a bending moment diagram.
  • 13. 13 A B Figure 2. Bending Moment Diagrams (Taken from www.nrmca.org/aboutconcrete, 2005) The areas shaded in red are the areas of the beam to which load will be exerted. Figure 2A shows how the stress is applied constantly over a large area. With this method the position of the first crack is unforced and can appear anywhere within the shaded region. However this means that the crack will follow the weakest path through the concrete beam that it can find. Figure 2B shows that the stress is applied to a smaller area than the third point test. The position of the first crack in the single point test is forced at a single point meaning that the crack cannot just follow the weakest path. With these pieces of research presented, a single point test was used, as use of the third point loading machine was limited and also was unable to be linked to a computer programme measuring the applied loads and deflection. All testing carried out conformed to BS EN 12390-5:2009, which specifies a method for testing the flexural strength of specimens of hardened concrete. 3.4.1 Loading Rate The loading rate applied was 1.1mm/minute, this is the rate proposed in research by Coatanlem (2002). There is no set rate at which the load can be applied, however for tests similar to this, it is recommended between 0.5 and 1.5 mm/minute (http://www.astm.org/Standards, 2010). 3.5 Calculating Flexural Strength Flexural strength, considered as the strength under normal stresses, was determined by applying the following equation known from the strength of materials: R = 3P L Where, 2bd² R = Modulus, measured in N/mm². P = Correct load indicated, Newtons. L = Span length between supports, mm. b = Width of beam, mm. d = Depth of beam, mm. (www.astm.org, 2009)
  • 14. First crack 0 0.15 0.30 0.45 0.60 0.75 0.90 1.05 1.20 1.35 1.50 14 4.0 Results and Analysis In this chapter the results for the flexural tests of the three groups are presented. Each groups individual beams maximum load, deflection and flexural strength have been placed in a table of results along with a graph representing the relationship between load and deflection. The results for the plain concrete beams are shown in Section 4.1. 4.1 Results of Plain Concrete Beam Flexural Testing Programme. After completing the flexural test programme for the plain concrete beams, the results were recorded and are displayed below in Table 2. Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) Plain 1 10792.82 2.60 4.86 Plain 2 11400.82 1.87 5.13 Plain 3 13835.71 1.77 6.22 Plain 4 11370.79 2.28 5.11 Plain 5 13106.59 0.98 5.89 Plain 6 11398.64 0.55 5.12 Plain 7 10749.95 1.60 4.83 Mean Value 11807.90 1.66 5.31 Table 2. The table shows the maximum load, deflection and flexural strength for plain concrete beams. The maximum loads for the 7 plain beams were averaged and plotted against the average maximum deflection in the graph shown in Figure 3 below. 14000 12000 10000 8000 6000 4000 2000 0 Load applied (N) Deflection mm Deflection (mm) Figure 3. Graph showing the relationship between load and deflection for plain concrete beams.
  • 15. First crack 0 1.50 3.00 4.50 6.00 Axi7s. 5T0it le 9.00 10.50 12.00 13.50 15.00 15 4.2 Results from using Wood Chippings as Addition to the Concrete Beams. The results for wood chippings alone are presented within Table 3 below. Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) Wood 1 6057.04 22.00 2.73 Wood 2 8660.77 12.15 3.89 Wood 3 10137.44 10.73 4.56 Wood 4 5758.72 20.19 2.59 Wood 5 6883.53 15.14 3.09 Wood 6 7428.96 12.47 3.45 Wood 7 6575.69 9.81 2.96 Wood 8 8187.26 14.69 3.68 Mean Value 7461.18 14.65 3.36 Table 3. Results from the flexural testing programme for using wood chippings alone as an additive to concrete beams. As was done for the plain concrete group beams, the maximum loads for the 8 beams were averaged and plotted against the average maximum deflection in the graph shown in Figure 4 below. 8000 7000 6000 5000 4000 3000 2000 1000 0 Load applied (N) Deflection (mm) Figure 4. Graph showing the relationship between load and deflection for concrete beams with wood chipping added
  • 16. 4.3 Results from using Wood Chippings and Silica Fume as Addition to the Concrete Beams. First crack 0 1.50 3.00 4.50 6.00 7.50 9.A00x i s T 1it0le.50 12.00 13.50 15.00 16.5 18.00 16 The results recorded from the flexural testing of wood chippings and silica fume within concrete beams are presented within Table 4 below. Max. Load (N) Max. Deflection (mm) Flexural Strength (N/mm²) Hybrid 1 4115.64 22.36 1.85 Hybrid 2 4454.58 23.44 2.01 Hybrid 3 3665.14 19.99 1.65 Hybrid 4 5561.08 17.44 2.50 Hybrid 5 4217.87 19.35 1.89 Hybrid 6 6531.98 12.41 2.93 Hybrid 7 5463.34 14.89 2.74 Hybrid 8 6100.41 19.52 2.89 Hybrid 9 7310.51 19.36 3.29 Mean Value 5268.95 18.75 2.41 Table 4. Results from the flexural testing programme for using wood chippings and silica fume as an additive to concrete beams. The maximum loads for the 9 hybrid beams were averaged and plotted against the average maximum deflection in the graph shown in Figure 5 below. 6000 5000 4000 3000 2000 1000 0 Load applied (N) Deflection (mm) Figure 5. Graph showing the relationship between load and deflection for concrete beams with both silica fume and wood chippings added
  • 17. 17 4.4 Overview of Flexural Strength Results. The table below gives an overview comparison between the 3 groups, comparing average maximum loads, maximum deflection and flexural strength. Group Average Max load (N) Average Max Deflection (mm) Average Flexural strength (N/mm²) Plain 11807.90 1.66 5.31 Wood alone 7461.18 14.65 3.36 Hybrid 5268.95 18.75 2.41 Table 5. Showing the average results for the 3 groups maximum load, maximum deflection and flexural strength. When comparing the wood alone to plain concrete, the maximum load achieved is decreased by 36.8%, however the average maximum deflection reached before complete shear is increased by 782.5%. When comparing the hybrid concrete group average maximum load to the average for plain concrete maximum load, the maximum load before first crack is 56.5% lower. The position of first crack is shown in Figures 3, 4 and 5. However, the maximum deflection recorded for the hybrid concrete beams is 1029.5% greater than that of the plain concrete beams. The flexural strength of the hybrid beams decreased by 55.6% when compared to the plain beams. The flexural strength of the beams with wood chippings alone decreased by 37.7% when compared to the plain group. 4.5 Analysis of Results. In order to explain these results, a more detailed look at what is happening to the beams must be taken. As presented within the literature review, Section 2.3, silica fume undergoes a pozzolanic reaction, improving the bonds between the cementitious materials to the wood reinforcement. The improvement of the bonds between the wood and the concrete suggests this is why maximum deflection values are increased even between the wood chipping beams, and the hybrid beams, as the bonds are stronger and pull out is resisted further. The term ‘pull out’ refers to the wood reinforcement being de-bonded from the concrete due to the load applied, and removed without the wood breaking. Plate 1 below shows a photograph of a beam that exhibits pull out after it had failed and had been removed from the flexural testing machine. Plate 1. Photograph of a failed beam showing pull out of the wood reinforcement Large areas are left where the wood chipping reinforcement has been de-bonded and pulled out from the concrete beam.
  • 18. Here, a length of wood chipping is shown to have been pulled out from the concrete beam It can be seen here that wood chippings within the beam are spanning the crack and acting as reinforcement to the beam. 18 Plate 2, shows a concrete beam where it possible to see the wood chippings within acting a reinforcement to the beam. Plate 2. Shows the wood waste within the beam acting as reinforcement. Whilst the addition of silica fume increased the maximum deflection, it also reduced the maximum load the beams can withstand as well as reducing the flexural strength. The basic theory of concrete flexural strength is that flexural strength of concrete decreases as density decreases, (Rossignolo, 2002. Park, 1975). This may potentially explain the reason the plain concrete groups flexural strength is higher, as the density of the wood chippings present in the other two concrete group beams being a lot less than that of concrete, therefore reducing the density of the beam. The next section will consider the density of the beams as a reason for reduced flexural strength. 4.6 Determining the Density Characteristics of the Concrete Mixes. After the beams were taken out of the moulds for testing they were weighed, and from this the density could be calculated. Figure 6 below shows the densities of the 3 groups. 2500 2400 2300 2200 2100 2000 1900 1800 Plain Wood alone Wood & Silica fume Density (kg/m³) Density kg/m³ Figure 6. Bar chart showing the density of the 3 concrete groups after 28 days.
  • 19. Comparing the plain beam densities, to that of the wood chipping group it can be shown that a 9.30% reduction in density is achieved. The hybrid beams have a 6.60% reduction in density compared to the wood alone, and a 15.30% reduction compared to the plain group. Table 6 below shows averages across the 3 groups for maximum load, maximum deflection, flexural strength and also density. 19 Group Average Max load, (N) Average Max Deflection,(mm) Average Flexural strength (N/mm²) Density (kg/m³) Plain 11807.90 1.66 5.31 2380 Wood 7461.18 14.65 3.36 2160 Hybrid 5268.95 18.75 2.41 2040 Table 6. Shows averages for maximum loads, deflections, flexural strength and density. By presenting data from Table 6 in graphical form, such as Figures 7 and 8. It is possible to see that density and load are proportional, as well as density and flexural strength, as the lines on both graphs are straight. 2500 2400 2300 2200 2100 2000 1900 1800 Wood Hybrid 2 3 4 5 Density (kg/m³) Flexural strength (N/mm²) Plain Figure 7. Graph showing the relationship between density and flexural strength for the three groups tested.
  • 20. 20 2500 2400 2300 2200 2100 2000 1900 1800 Hybrid Wood Plain 5115 5480 5845 6211 6576 6941 7306 7672 8037 8402 8767 9133 9498 9863 10228 10594 10959 11324 11689 Density (kg/m³) Maximum load, (N) Figure 8. Graph showing the relationship between density and maximum load for the three groups tested. This means that by adding wood chippings to the mix, the density is reduced and this in turn reduces the flexural strength of the concrete. However by adding silica fume, the bonds at the interface between the concrete and the wood are improved, thus further deflection is measured before failure. Whilst the data above gives reason to why the flexural strength is the reduced with the addition of wood chippings, the hybrid group’s average maximum load and flexural strength decreases further than that of the wood chippings alone, this is an unexpected result as the same weight of wood chippings was use for both of the groups. One reason for this could be that although the same weight of wood chipping was used, the volume of the wood chippings may have increased; this would explain the drop in density therefore the decrease in flexural strength. However, other reasons may be established by looking at the rate of drying for all beams. The next section will consider the drying curves for the beams. 4.7 Drying Curves. This section will look at the drying rates for the 3 groups and analyse factors that influence the final density of the beams. Figure 8 below shows the rate at which each group of beams dried out over 28 days.
  • 21. 21 3000 2500 2000 1500 1000 500 0 Density kg/m³ Days Plain Series1 Wood Series2 Series3 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Days Hybrid Figure 8. Graph showing the drying curves for the 3 groups over a 28 day drying period From the graph it is possible to see that the hybrid beams dry out and lose density the more rapidly over the 28 day drying process. Research by Kadri (2009) suggests that the presence of the silica fume in concrete will accelerate exothermic reactions during the hydration process. Exothermic reactions begin to occur when the cement first comes into contact with water in the mix and heat is produced. The main reaction that occurs is between the aluminate within the Portland cement, and water. This reaction forms an aluminate-rich gel; the gel will then react with sulphates within the solution to form what is known as ettringite (http://www.understanding-cement.com/hydration.html, 2010). Ettringite is a crystal like structure and forms in microscopic needles such as shown in Plate 3. In the photograph microscopic needles of white ettringite can be seen forming in tiny air voids within concrete. Plate 3. Photograph showing the microscopic needles of ettringite. (Taken from http://www.cement.org/tech, 2010)
  • 22. The silica fume within the concrete was added to improve the bond between the concrete by drawing in the ettringite needles to the woods surface in accordance to the findings of section 2.1.1 of the literature review. However, this has meant that the spaces within the concrete where the ettringite crystals were before being drawn to the wood chippings are now tiny air voids (http://www.cement.org/tech, 2010). With these air voids present in the concrete, it is suggested that the concrete beams are able to dry out faster, become less dense and will have less flexural strength due to this. The hybrid beams have exhibited all of these properties, being less dense than both the other groups, and having a smaller flexural strength value than the plain concrete and the concrete with only wood chipping added. From this chapter it is possible to see clear differences between the plain, wood chipping alone and hybrid mixes. The results have been analysed and contextualised against our current knowledge of concrete materials behaviour and structure. From doing this it can be suggested that the introduction of silica fume to a mix can improve the deflection reached before complete failure occurs. It can also be suggested that silica fume and wood chippings decrease the flexural performance of concrete beams due to the decrease in density. 22 Chapter 5 will conclude the research and reflect upon the hypothesis, research aims and objectives of the flexural testing programme.
  • 23. 23 5.0 Conclusions In this study the effects of adding waste wood chippings and silica fume to concrete were investigated and analyzed. The aims of the study were see if the use of waste wood chippings from the timber industry and the addition of silica fume, would improve flexural performance of concrete, or not. The main objectives of the study were (1) to test 10 concrete beams with no reinforcement, (2) test 10 concrete beams with waste wood chipping added as reinforcement (3) test 10 concrete beams with waste wood chipping and silica fume added as reinforcement, (4) to record the results appropriately, (5) to compare and analyse the 3 groups of test results and (6) to evaluate the effectiveness of adding waste wood chippings and silica fume to concrete mixes. By conducting testing in accordance with the method presented in Chapter 3, results of the flexural testing programme were obtained and analysed in Chapter 4. From analysing the results of the flexural testing programme carried out, the following conclusions were derived. 1 The results of the flexural testing programme indicate that the addition of wood chippings and silica fume does not improve the flexural strength of concrete, the values for both wood chipping and silica fume groups were lower than that of plain concrete. 2 The addition of wood chipping alone improves maximum deflection, compared to plain concrete. 3 The addition of wood chippings and silica fume improves maximum deflection by the greatest value. 4 Due to the addition of silica fume, ettringite crystals are drawn towards the wood, leaving air holes, reducing density and strength even further than wood chippings alone. The hypothesis in Section 1.1, suggested that if waste wood chippings and silica fume is added as reinforcement to a concrete beam, then the flexural strength of concrete beams will be improved. From the conclusions drawn, this can be rejected. The aims of the investigation stated in section 1.2 have been met, and the objectives stated in Section 1.3 have also been achieved. Although the hypothesis for this investigation was rejected, this study shows feasibility for producing a more sustainable concrete. There are many different reasons for the results obtained from this investigation; there are also many opportunities for further research and testing to be carried out within this area. Section 6.0 will suggest recommendations for further studies. 5.1 Research Limitations The data gather from the flexural testing programme made for interesting analysis. By collecting data from previous similar studies in the literature review and compiling the methodology, it is apparent that many variations could be made within this research, with reference to mix design and testing methodology. It was extremely difficult to acquire the silica fume, as it was necessary for it to be shipped from Holland, in only very small amounts. With more accessibility to silica fume, further testing could have been conducted using different amounts of silica fume. Another major limitation was the time available to test concrete within the laboratories, as compression testing on concrete cubes would have provided a further insight into the effects
  • 24. of adding waste wood and silica fume to concrete. If more time was available, a further 10 beams would have been tested using silica fume as the only addition to the concrete mix, to allow for comparisons to the concrete beams with wood chipping alone and the hybrid concrete beams. It would also be useful to measure the flexural strengths of the 3 groups of concrete after a 60 day curing period, as this is suggested to increase flexural strengths further (Naik, 2002). Whilst this chapter has concluded the findings from this research and assessed the limitations. The next chapter will consider recommendations for future research. 24
  • 25. 25 6.0 Recommendations for Future Research The replacement of cement by materials that induce a pozzolanic reaction, such as fly ash Naik (2002), or silica fume, can have advantages for both sustainability and to the strength of concrete. Although this investigation rejected the hypothesis that suggested that if waste wood chippings and silica fume is added as reinforcement to a concrete beam, then the flexural strength of concrete beams will be improved, it is still important to drive forward sustainability issues by means of reducing carbon emissions, reducing materials used and costs of production. There are many different variations to the methodology of the flexural testing programme undertaken within this study, with reference to the mix design. This chapter will address these variations in order to recommend and benefit future studies within this area. By varying the content ratios between the water, silica fume and waste wood chippings is suggested to give different results for both flexural strength tests and compressive strength tests. (Schulze, 1999, Beton, 1990., Pascal et al., 2004. and Van Gemert et al. 2005) With reference to the mixing method of the batches, it is suggested that pre soaking the wood chippings to draw cementitious particles into the wood will improve the bond between the wood and the concrete further than if no pre soaking takes place, (Reis, 2006). As well as varying the method of adding the wood, the method of which the silica fume was batched could also be altered, for this research the silica was batched in accordance to the manufacturer and supplier, however there are different suggestions to mixing which potentially increase the strength of concrete, (Blanksvard, 2009). The above recommendations provide platforms for future research to improve upon current knowledge of concrete behaviour, and can potentially lead to more sustainable methods of making concrete. The recommendations made, are based upon researchers conducting tests without the limitations this paper has identified in Section 5.1.
  • 26. 26 7.0 References. http://www.astm.org/Standards (2010) (Accessed 23 March 2010) Becchio, C. (2009) Improving environmental sustainability of concrete products, investigation of MWC thermal and mechanical properties. Published doctorate. Turin polytechnic, Italy. Bjork, F. (1999) ‘Concrete technology and sustainable development’ Vancouver symposium on concrete technology and sustainable development. December 1999. p.5. Blanksvard, T. (2009) Strengthening of concrete structures by the use of mineral based composites. Published doctoral thesis. Lulea University of technology. http://www.brmca.org.uk/downloads/Mpa_Placing_PrintR (2009) (Accessed 24 March 2010) Carette, G., (1993) “Mechanical Properties of Concrete Incorporating High Volumes of Fly Ash From Sources in the U.S” November 1, 1993. http://www.cement.org/tech, (2010) (Accessed 26 March 2010) Chitchumnong P, Brooks S.C., Stafford G.D. (1989), ‘Comparison of three- and four-point flexural strength testing of denture-base polymers’ Dental Materials Pp2-5 Coatanlem, P. (2005) Lightweight wood chipping concrete durability. Published masters. Department of civil engineering. Rennes, France. Galetakis M. and Raka S., (2004) ‘Utilization of limestone dust for artificial stone production: an experimental approach’ Minerals Engineering Gemert V, D., Czarnecki, L., Maultzsch, M., Schorn, H., Beeldens, A., Lukowski, P and Knapen, E. (2005) Cement concrete and concrete–polymer composites: Two merging worlds: A report from 11th ICPIC Congress in Berlin, 2004. Cement and Concrete Composites Wendehorst, R. (1992) Baustoffkunde. Weinheim, Germany. Huang Cheng-yi and R.F. Feldman. (1985) Influence of silica fume on the micro structural development in cement mortars. Science direct [online]. Available at: https://www.sciencedirect.com (Accessed: 8 January 2010) http://www.instron.co.uk/wa/application /flexure (2010) (Accessed 22 March 2010) Johansson, J. (2005) ‘End peeling of mineral based CFRP strengthened concrete structures- a parametric study.’ Proceedings of the international symposium on bond behaviour of FRP in structures. BBFF 2005. Kadri, E., Duval, R., (2009) ‘Hydration heat kinetics of concrete with silica fume Construction’. Building Materials. Volume 23, Issue 11, November 2009. Miller, R. H., and Collins, R. J., (1975) “Waste Materials as Potential Replacements for Highway Aggregates,” NCHRP Report No. 166. Naik, T.R. (2002) ‘Greener concrete using recycled materials’ Concrete international. July 2002.
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