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08.12.2014Report date
Polska
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
AR-14-ST-061473-01
ĚAR-14-ST-Ç&.iČ-01Î
Analytical report
{01ACBDB7-9D01-4A1D-8B44-4D031AAFE724}
Sample Code 720-2014-00110505
Type of sample Vegetable-fat mix "Tulchynka 82.5%" 200g
Sample sender Eurofins Agro Testing Ukraine LLC
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
Reception date time 18.11.2014
Transport by Courier company
Sample condition no proper
Date of sampling 17.11.2014
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Partie-no. 241014 026
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Number of tested samples 1
18.11.2014Start analysis
End Analysis 03.12.2014
Test results
ST0J3 Estrogenes (LC-MS/MS (A)
LC-MS/MS, LC- MS/MSMethod
Subcontracted to an external laboratory accredited for this test Tiergesundheitsdienst Bayern e.V., accreditation nr. DIN EN ISO/IEC
17025:2005 DAkkS D-PL-18094-01-00
Diethylstilbestrol (Stilben) <LOQ µg/kg
Dienestrol (Stilben) <LOQ µg/kg
Estradiol (17- beta) <LOQ µg/kg
Estradiol (17-alpha) <LOQ µg/kg
Ethinyl-Estradiole <LOQ µg/kg
Hexestrol (Stilben) <LOQ µg/kg
Estrone <LOQ µg/kg
Zeranol <LOQ µg/kg
Taleranol <LOQ µg/kg
Estriol <LOQ µg/kg
J7012 Butyric acid (A)
§64 LFGB L 17.00-13, mod., GC-FIDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Butyric acid 0.35 g/100 g fat
JJV14 Milk fat (A)
calculationMethod
Analytical report AR-14-ST-061473-01
720-2014-00110505Sample Code
2/4Page
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Milk fat calculated 3,2% butyric acid 9.1 %
Milk fat calculated 3,5% butyric acid 8.3 %
J5003 Aflatoxin M1 (milk products) (A)
internal method based on EN ISO 14501, IAC, HPLC-FLDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Aflatoxin M1 <0.01 * µg/kg
ST00T Water content (A)
EN ISO 3727-1:2004, weightMethod
Moisture 15.94 ± 0.96%
ST05L Peroxide value. Animal and vegetable oils and fats (A)
ISO 3960:2012, titrationMethod
Peroxide value 0.34 ± 0.05meqO2/kg
ST08J The acid number and the acidity calc.as oleic acid (A)
EN ISO 660:2010, tritimetryMethod
Acidity number 0.062 st Turner
Acidity number 0.12 st
Koettstorfer
a
ST0EX Melting point (#)
ISO 6321, open capillary (flowing point)Method
Subcontracted to an external laboratory
Melting Point 28.30 °C
FGM02 Inhibition test (A)
In-House method, Kundrat AgarMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 DAkkS PL-14268-01
Inhibitory substances Not Detected
JCAF2 Aflatoxins B1, B2, G1, G2 (fats, oils, lecithin) (A)
internal method based on EN 14123, IAC, HPLC-FLDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Aflatoxin B1 <0.1 * µg/kg
Aflatoxin B2 <0.1 * µg/kg
Aflatoxin G1 <0.1 * µg/kg
Aflatoxin G2 <0.1 * µg/kg
Sum of all positive identified Aflatoxins <0.4 * µg/kg
JJF02 Fat total (A)
§64 LFGB L 06.00-6, mod., GravimetryMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Fat, total 83.4 ± 2.5g/100 g
SP421 Organochlorine Pesticides, Pyrethroides (A)
ASU L00.00-34, GC-ECDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14198-01-00
Screened pesticides Not Detected
SP424 Organophosphorus Pesticides (A)
ASU L00.00-34, GC-FPDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14198-01-00
Screened pesticides Not Detected
ST0J0 Contents of total sugars (A)
PN-85/A-82100, tritimetryMethod
Total sugars 1.0 ± 0.2%
ST0QQ Dry mass, without fat (A)
PN-EN ISO 3727-2: 2004, weightMethod
Dry matter, free of fat 1.81 ± 0.29%
SZFB0 Fatty acids profile (A)
Internal Method, GC/FIDMethod
Analytical report AR-14-ST-061473-01
720-2014-00110505Sample Code
3/4Page
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Trans fatty acids total/sample 2.21 g/100 g fat
mono-unsaturated fatty acids total/sample 31.15 g/100 g fat
poly-unsaturated fatty acids total/sample 21.01 g/100 g fat
saturated fatty acids total/sample 47.85 g/100 g fat
C10:0 Capric acid (Methyl decanoate) 0.61 g/100 g fat
C11:0 Undecanoic acid (Methyl undecanoate) <0.5 g/100 g fat
C12:0 Lauric acid (Methyl dodecanoate) 3.96 g/100 g fat
C13:0 Tridecanoic acid (Methyl tridecanoate) <0.5 g/100 g fat
C14:0 Myristic acid (Methyl myristate) 2.72 g/100 g fat
C14:1 Myristoleic acid (Methyl myristoleate) <0.5 g/100 g fat
C15:0 Pentadecanoic acid (Methyl pentadecanoate) <0.5 g/100 g fat
C15:1 Pentadecenoic acid (cis-10) <0.5 g/100 g fat
C16:0 Palmitic acid (Methyl palmitate) 34 g/100 g fat
C16:1 Palmitoleic acid (Methyl palmitoleate) <0.5 g/100 g fat
C17:0 Heptadecanoic acid (Methyl heptadecanoate) <0.5 g/100 g fat
C17:1 Heptadecenoic acid (cis-10-heptadecenoate) <0.5 g/100 g fat
C18:0 Stearic acid (Methyl stearate) 5.62 g/100 g fat
C18:1n11c cis-Vaccen acid (cis-Methyl vaccenate) 21 g/100 g fat
C18:1n11t Vaccen acid (trans-Methyl vaccenate) 1.09 g/100 g fat
C18:1n6 Petroselin acid (Methyl petroselaidate) <0.5 g/100 g fat
C18:1n9 Oleic acid (Methyl oleate) 28.4 g/100 g fat
C18:1n9t Elaidic acid (Methyl elaidate) 1.12 g/100 g fat
C18:2n6 Linoleic acid (Methyl linoleate) 21 g/100 g fat
C18:2n6t Linoleaidic acid (Methyl linolelaidate) <0.5 g/100 g fat
C18:3n3 Apha-Linolenic acid (Methyl linolenate) <0.5 g/100 g fat
C18:3n6 γ-linolenic acid (Methyl γ-linolenate) <0.5 g/100 g fat
C20:0 Arachidic acid (Methyl arachidate) <0.5 g/100 g fat
C20:1 Eicosenoic acid (Methyl cis-11-eicosenoate) <0.5 g/100 g fat
C20:2n6 Eicosadienoic acid (cis-11,14) <0.5 g/100 g fat
C20:3n3 Eicosatrienoic acid (cis-11,14,17) <0.5 g/100 g fat
C20:3n6 Dihomo-γ-linolenic acid (cis-8,11,14) <0.5 g/100 g fat
C20:4n6 Arachidonic acid (Methyl arachidonate) <0.5 g/100 g fat
C20:5n3 Eicosapentaenoic acid (cis-5,8,11,14,17) <0.5 g/100 g fat
C21:0 Heneicosanoic acid (Methyl heneicosanote) <0.5 g/100 g fat
C22:0 Behenic acid (Methyl behenate) <0.5 g/100 g fat
C22:1n9 Erucic acid (Methyl cis-13-docosenoate) <0.5 g/100 g fat
C22:2 Docosadienoic acid (cis-13,16) <0.5 g/100 g fat
C22:5 Docosapentaenic acid <0.5 g/100 g fat
C22:6n-3 Docosahexaenoic (DHA) <0.5 g/100 g fat
C23:0 Tricosanoic acid (Methyl tricosanoate) <0.5 g/100 g fat
C24:0 Lignoceric acid (Methyl tetracosanoate) <0.5 g/100 g fat
C24:1n9 Nervonic acid (cis-15-tetracosenoate) <0.5 g/100 g fat
C4:0 Butyric acid (Methyl butyrate) <0.5 g/100 g fat
C6:0 Caproic acid (Methyl hexanoate) <0.5 g/100 g fat
C8:0 Caprylic acid (Methyl octanoate) 0.56 g/100 g fat
SZQA1 Arsenic (As) (A)
LS-PP-CH-2/2, AAS-HG method (hydride technique)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Arsenic (As) <0.030 mg/kg
SZQA2 Cadmium (Cd) (A)
LS-PP-CH-2/4, AAS-ETA method (electrothermic atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Analytical report AR-14-ST-061473-01
720-2014-00110505Sample Code
4/4Page
Cadmium (Cd) <0.010 mg/kg
SZQA4 Copper (Cu) (A)
LS-PP-CH-2/8, AAS-F method (flame atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Copper (Cu) 0.84 mg/kg
SZQA6 Iron (Fe) (A)
LS-PP-CH-2/20, AES-ICPMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Iron (Fe) <0.50 mg/kg
SZQA7 Lead (Pb) (A)
LS-PP-CH-2/25, AAS-ETA method (electrothermic atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Lead (Pb) <0.050 mg/kg
SZQAA Mercury (Hg) (A)
LS-PP-CH-30, AAS-AMA methodMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Mercury (Hg) <0.004 mg/kg
SZQAG Zinc (Zn) (A)
LS-PP-CH-2/12, AAS-F method (flame atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Zinc (Zn) 0.99 mg/kg
Below indicated quantification level* =
# = Not accredited
A = Method accredited
+/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The
result and its uncertainty refer to the analyzed sample.
JUDGEMENT
LOQ- Below indicated quantification level
List of analyzed pesticides is attached to the report.
Estrogenes: LOQ- 1 µg/kg
Approved by:Authorized by:Elżbieta Szyszkowska
Team Leader Analytical Service Manager
Joanna Brzoza
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in
writing, by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
1/2Page
08.12.2014Report date
Polska
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
AR-14-ST-061472-01
ĚAR-14-ST-Ç&.hČ-01OÎ
Analytical report
{F06DD157-7FAC-456B-A32C-6722A4752E65}
Sample Code 720-2014-00110506
Type of sample Vegetable-fat mix "Tulchynka 72.5%" 200g
Sample sender Eurofins Agro Testing Ukraine LLC
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
Reception date time 18.11.2014
Transport by Courier company
Sample condition no proper
Date of sampling 17.11.2014
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Partie-no. 191014084
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Number of tested samples 1
18.11.2014Start analysis
End Analysis 03.12.2014
Test results
J7012 Butyric acid (A)
§64 LFGB L 17.00-13, mod., GC-FIDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Butyric acid 0.35 g/100 g fat
JJV14 Milk fat (A)
calculationMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Milk fat calculated 3,2% butyric acid 7.9 %
Milk fat calculated 3,5% butyric acid 7.2 %
ST00T Water content (A)
EN ISO 3727-1:2004, weightMethod
Moisture 24.40 ± 1.46%
ST08J The acid number and the acidity calc.as oleic acid (A)
EN ISO 660:2010, tritimetryMethod
Acidity number 0.05 ± 0.01st Turnera
Acidity number 0.11 ± 0.02st
Koettstorfer
a
FGM02 Inhibition test (A)
In-House method, Kundrat AgarMethod
Analytical report AR-14-ST-061472-01
720-2014-00110506Sample Code
2/2Page
Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 DAkkS PL-14268-01
Inhibitory substances Not Detected
JJF02 Fat total (A)
§64 LFGB L 06.00-6, mod., GravimetryMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Fat, total 71.9 ± 2.2g/100 g
ST0QQ Dry mass, without fat (A)
PN-EN ISO 3727-2: 2004, weightMethod
Dry matter, free of fat 3.92 ± 0.63%
A = Method accredited
+/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The
result and its uncertainty refer to the analyzed sample.
Approved by:Authorized by:Elżbieta Szyszkowska
Team Leader Analytical Service Manager
Joanna Brzoza
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in
writing, by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
1/2Page
08.12.2014Report date
Polska
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
AR-14-ST-061469-01
ĚAR-14-ST-Ç&.eČ-01(Î
Analytical report
{EAB9E494-3C4E-4CC4-94BD-117BB5CE5079}
Sample Code 720-2014-00110507
Type of sample Vegetable- fat mix "Tulchynka 62.5%" 200g
Sample sender Eurofins Agro Testing Ukraine LLC
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
Reception date time 18.11.2014
Transport by Courier company
Sample condition no proper
Date of sampling 17.11.2014
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Partie-no. 201014068
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Number of tested samples 1
18.11.2014Start analysis
End Analysis 03.12.2014
Test results
J7012 Butyric acid (A)
§64 LFGB L 17.00-13, mod., GC-FIDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Butyric acid 0.40 g/100 g fat
JJV14 Milk fat (A)
calculationMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Milk fat calculated 3,2% butyric acid 8.1 %
Milk fat calculated 3,5% butyric acid 7.4 %
ST00T Water content (A)
EN ISO 3727-1:2004, weightMethod
Moisture 32.75 ± 1.97%
ST08J The acid number and the acidity calc.as oleic acid (A)
EN ISO 660:2010, tritimetryMethod
Acidity number 0.066 Turnera
Acidity number 0.131 st
Koettstorfer
a
FGM02 Inhibition test (A)
In-House method, Kundrat AgarMethod
Analytical report AR-14-ST-061469-01
720-2014-00110507Sample Code
2/2Page
Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 DAkkS PL-14268-01
Inhibitory substances Not Detected
JJF02 Fat total (A)
§64 LFGB L 06.00-6, mod., GravimetryMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Fat, total 64.8 ± 1.9g/100 g
ST0QQ Dry mass, without fat (A)
PN-EN ISO 3727-2: 2004, weightMethod
Dry matter, free of fat 3.84 ± 0.61%
A = Method accredited
+/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The
result and its uncertainty refer to the analyzed sample.
Approved by:Authorized by:Elżbieta Szyszkowska
Team Leader Analytical Service Manager
Joanna Brzoza
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in
writing, by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
1/4Page
10.12.2014Report date
Polska
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
AR-14-ST-061474-01
ĚAR-14-ST-Ç&.jČ-01iÎ
Analytical report
{78BD63EE-5BD0-44E5-BCB1-30B0A8C618D7}
Sample Code 720-2014-00110508
Type of sample Vegetable- fat mix "Chocolate Tulchynka 62%"
Sample sender Eurofins Agro Testing Ukraine LLC
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
Reception date time 18.11.2014
Transport by Courier company
Sample condition no proper
Date of sampling 17.11.2014
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Partie-no. 061014 008
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Number of tested samples 1
18.11.2014Start analysis
End Analysis 02.12.2014
Test results
J7012 Butyric acid (A)
§64 LFGB L 17.00-13, mod., GC-FIDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Butyric acid 0.45 g/100 g fat
JJV14 Milk fat (A)
calculationMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Milk fat calculated 3,2% butyric acid 8.5 %
Milk fat calculated 3,5% butyric acid 7.7 %
JJ006 Aflatoxins B1, B2, G1, G2 (nuts, cocoa, cereals) (A)
internal method based on EN 14123, IAC, HPLC-FLDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Aflatoxin B1 <0.1 * µg/kg
Aflatoxin B2 <0.1 * µg/kg
Aflatoxin G1 <0.1 * µg/kg
Aflatoxin G2 <0.1 * µg/kg
J5003 Aflatoxin M1 (milk products) (A)
internal method based on EN ISO 14501, IAC, HPLC-FLDMethod
Analytical report AR-14-ST-061474-01
720-2014-00110508Sample Code
2/4Page
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Aflatoxin M1 <0.01 * µg/kg
JJF02 Fat total (A)
§64 LFGB L 06.00-6, mod., GravimetryMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14251-01-00
Fat, total 60.2 ± 1.8g/100 g
ST00T Water content (A)
EN ISO 3727-1:2004, , weightMethod
Moisture 16.15 ± 0.97%
ST05L Peroxide value. Animal and vegetable oils and fats (A)
ISO 3960:2012, titrationMethod
Peroxide value 0.27 ± 0.04meqO2/kg
ST08J The acid number and the acidity calc.as oleic acid (A)
EN ISO 660:2010, tritimetryMethod
Acidity number 0,054 st Turnera
Acidity number 0,108 st
Koettstorfer
a
ST0EX Melting point (#)
ISO 6321, open capillary (flowing point)Method
Subcontracted to an external laboratory
Melting Point 33.20 °C
FGM02 Inhibition test (A)
In-House method, Kundrat AgarMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 DAkkS PL-14268-01
Inhibitory substances not detected
JCAF2 Aflatoxins B1, B2, G1, G2 (fats, oils, lecithin) (A)
internal method based on EN 14123, IAC, HPLC-FLDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Sum of all positive identified Aflatoxins
Sum of all positive identified Aflatoxins
JJ006 Aflatoxins B1, B2, G1, G2 (nuts, cocoa, cereals) (A)
internal method based on EN 14123, IAC, HPLC-FLDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC
17025:2005 DAKKS D-PL-14602-01-00
Sum of all positive identified Aflatoxins
Sum of all positive identified Aflatoxins <0.4 * µg/kg
SP421 Organochlorine Pesticides, Pyrethroides (A)
ASU L00.00-34, GC-ECDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14198-01-00
Screened pesticides Not Detected
SP424 Organophosphorus Pesticides (A)
ASU L00.00-34, GC-FPDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC
17025:2005 D-PL-14198-01-00
Screened pesticides Not Detected
ST0J0 Contents of total sugars (A)
PN-85/A-82100, tritimetryMethod
Total sugars 21.9 ± 4.4%
ST0QQ Dry mass, without fat (A)
PN-EN ISO 3727-2: 2004, , weightMethod
Dry matter, free of fat 24.41 ± 3.91%
SZFB0 Fatty acids profile (A)
Internal Method, GC/FIDMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Trans fatty acids total/sample 2.17 g/100 g fat
Analytical report AR-14-ST-061474-01
720-2014-00110508Sample Code
3/4Page
poly-unsaturated fatty acids total/sample 14.17 g/100 g fat
saturated fatty acids total/sample 53.19 g/100 g fat
mono-unsaturated fatty acids total/sample 32.64 g/100 g fat
C10:0 Capric acid (Methyl decanoate) 1.15 g/100 g fat
C11:0 Undecanoic acid (Methyl undecanoate) <0.5 g/100 g fat
C12:0 Lauric acid (Methyl dodecanoate) 6.83 g/100 g fat
C13:0 Tridecanoic acid (Methyl tridecanoate) <0.5 g/100 g fat
C14:0 Myristic acid (Methyl myristate) 4.33 g/100 g fat
C14:1 Myristoleic acid (Methyl myristoleate) <0.5 g/100 g fat
C15:0 Pentadecanoic acid (Methyl pentadecanoate) <0.5 g/100 g fat
C15:1 Pentadecenoic acid (cis-10) <0.5 g/100 g fat
C16:0 Palmitic acid (Methyl palmitate) 33 g/100 g fat
C16:1 Palmitoleic acid (Methyl palmitoleate) <0.5 g/100 g fat
C17:0 Heptadecanoic acid (Methyl heptadecanoate) <0.5 g/100 g fat
C17:1 Heptadecenoic acid (cis-10-heptadecenoate) <0.5 g/100 g fat
C18:0 Stearic acid (Methyl stearate) 6.25 g/100 g fat
C18:1n11c cis-Vaccen acid (cis-Methyl vaccenate) 14.2 g/100 g fat
C18:1n11t Vaccen acid (trans-Methyl vaccenate) 0.84 g/100 g fat
C18:1n6 Petroselin acid (Methyl petroselaidate) <0.5 g/100 g fat
C18:1n9 Oleic acid (Methyl oleate) 29.8 g/100 g fat
C18:1n9t Elaidic acid (Methyl elaidate) 1.33 g/100 g fat
C18:2n6 Linoleic acid (Methyl linoleate) 14.2 g/100 g fat
C18:2n6t Linoleaidic acid (Methyl linolelaidate) <0.5 g/100 g fat
C18:3n3 Apha-Linolenic acid (Methyl linolenate) <0.5 g/100 g fat
C18:3n6 γ-linolenic acid (Methyl γ-linolenate) <0.5 g/100 g fat
C20:0 Arachidic acid (Methyl arachidate) <0.5 g/100 g fat
C20:1 Eicosenoic acid (Methyl cis-11-eicosenoate) <0.5 g/100 g fat
C20:2n6 Eicosadienoic acid (cis-11,14) <0.5 g/100 g fat
C20:3n3 Eicosatrienoic acid (cis-11,14,17) <0.5 g/100 g fat
C20:3n6 Dihomo-γ-linolenic acid (cis-8,11,14) <0.5 g/100 g fat
C20:4n6 Arachidonic acid (Methyl arachidonate) <0.5 g/100 g fat
C20:5n3 Eicosapentaenoic acid (cis-5,8,11,14,17) <0.5 g/100 g fat
C21:0 Heneicosanoic acid (Methyl heneicosanote) <0.5 g/100 g fat
C22:0 Behenic acid (Methyl behenate) <0.5 g/100 g fat
C22:1n9 Erucic acid (Methyl cis-13-docosenoate) <0.5 g/100 g fat
C22:2 Docosadienoic acid (cis-13,16) <0.5 g/100 g fat
C22:5 Docosapentaenic acid <0.5 g/100 g fat
C22:6n-3 Docosahexaenoic (DHA) <0.5 g/100 g fat
C23:0 Tricosanoic acid (Methyl tricosanoate) <0.5 g/100 g fat
C24:0 Lignoceric acid (Methyl tetracosanoate) <0.5 g/100 g fat
C24:1n9 Nervonic acid (cis-15-tetracosenoate) <0.5 g/100 g fat
C4:0 Butyric acid (Methyl butyrate) <0.5 g/100 g fat
C6:0 Caproic acid (Methyl hexanoate) <0.5 g/100 g fat
C8:0 Caprylic acid (Methyl octanoate) 1.26 g/100 g fat
SZQA1 Arsenic (As) (A)
LS-PP-CH-2/2, AAS-HG method (hydride technique)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Arsenic (As) <0.030 mg/kg
SZQA2 Cadmium (Cd) (A)
LS-PP-CH-2/4, AAS-ETA method (electrothermic atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Cadmium (Cd) <0.010 mg/kg
SZQA4 Copper (Cu) (A)
LS-PP-CH-2/8, AAS-F method (flame atomization)Method
Analytical report AR-14-ST-061474-01
720-2014-00110508Sample Code
4/4Page
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Copper (Cu) 1.1 mg/kg
SZQA6 Iron (Fe) (A)
LS-PP-CH-2/20, AES-ICPMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Iron (Fe) 20.7 mg/kg
SZQA7 Lead (Pb) (A)
LS-PP-CH-2/25, AAS-ETA method (electrothermic atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Lead (Pb) <0.050 mg/kg
SZQAA Mercury (Hg) (A)
LS-PP-CH-30, AAS-AMA methodMethod
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Mercury (Hg) <0.004 mg/kg
SZQAG Zinc (Zn) (A)
LS-PP-CH-2/12, AAS-F method (flame atomization)Method
Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005
SNAS No. S-106
Zinc (Zn) 2.5 mg/kg
Below indicated quantification level* =
# = Not accredited
A = Method accredited
+/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The
result and its uncertainty refer to the analyzed sample.
Approved by:Authorized by:Elżbieta Szyszkowska
Team Leader Analytical Service Manager
Joanna Brzoza
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in
writing, by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
1/2Page
Polska
{09635A0A-28FC-4B0E-92B2-ED8D23D47D7F}
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
ĚAR-14-ST-Ç%Ç{Č-01cÎ
AR-14-ST-059991-01
02.12.2014Report date
Analytical report
Eurofins Agro Testing Ukraine LLCSample sender
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
18.11.2014Reception date time
CourierTransport by
Sample condition unreservedly
17.11.2014Date of sampling
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Number of tested samples 1
Start analysis
End Analysis 24.11.2014
19.11.2014
720-2014-00110516 Vegetable- fat mix "Tulchynka 82.5%"Type of sample
241014026Partie-no.
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Test results
720-2014-00110516
Vegetable- fat mix
"Tulchynka 82.5%"
Not Detected /25 g
(A)UM2PF: Salmonella
Method: ISO 6579
< 10 cfu/g
(A)UMJPR: Anaerobic Sulphite Reducing Bacteria
Method: ISO 15213
Not Detected /1 g
(A)UMIMW: Coagulase positive Staphylococcus
Method: ISO 6888-3
< 10 cfu/g
(A)UMARE: Coliforms 30°C
Method: ISO 4832
Not Detected /25 g
(A)UM7CU: Listeria monocytogenes
Method: ISO 11290-1 A1
< 10 cfu/g
(A)UMFZ4: Moulds
Method: ISO 21527-1
< 10 cfu/g
(A)UMMJ5: Yeast
Method: ISO 21527-1
Report date
AR-14-ST-059991-012/2
02.12.2014
Page Analytical report
720-2014-00110516
Vegetable- fat mix
"Tulchynka 82.5%"
5800 cfu/g
(A)UM274: Aerobic Plate Count 30°C
Method: ISO 4833-1
A = Method accredited
Approved by:Authorized by:Magdalena Duszynska
Analytical Service Manager
Rafal Sawaniewski
Older Assistant
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing,
by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
1/2Page
Polska
{C9E62175-DF2A-43A7-9E65-DC6237D4824D}
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
ĚAR-14-ST-Ç%Ç}Č-01}Î
AR-14-ST-059993-01
02.12.2014Report date
Analytical report
Eurofins Agro Testing Ukraine LLCSample sender
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
18.11.2014Reception date time
CourierTransport by
Sample condition unreservedly
17.11.2014Date of sampling
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Number of tested samples 1
Start analysis
End Analysis 24.11.2014
19.11.2014
720-2014-00110518 Vegetable- fat mix " Tulchynka 62.5%"Type of sample
201014068Partie-no.
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Test results
720-2014-00110518
Vegetable- fat mix "
Tulchynka 62.5%"
Not Detected /25 g
(A)UM2PF: Salmonella
Method: ISO 6579
< 10 cfu/g
(A)UMJPR: Anaerobic Sulphite Reducing Bacteria
Method: ISO 15213
Not Detected /1 g
(A)UMIMW: Coagulase positive Staphylococcus
Method: ISO 6888-3
< 10 cfu/g
(A)UMARE: Coliforms 30°C
Method: ISO 4832
Not Detected /25 g
(A)UM7CU: Listeria monocytogenes
Method: ISO 11290-1 A1
< 10 cfu/g
(A)UMFZ4: Moulds
Method: ISO 21527-1
< 10 cfu/g
(A)UMMJ5: Yeast
Method: ISO 21527-1
Report date
AR-14-ST-059993-012/2
02.12.2014
Page Analytical report
720-2014-00110518
Vegetable- fat mix "
Tulchynka 62.5%"
200000 cfu/g
(A)UM274: Aerobic Plate Count 30°C
Method: ISO 4833-1
A = Method accredited
Approved by:Authorized by:Magdalena Duszynska
Analytical Service Manager
Rafal Sawaniewski
Older Assistant
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing,
by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
1/2Page
Polska
{8B9F2DA8-DADF-4E17-8B0F-3074C8EBEE19}
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
ĚAR-14-ST-Ç%Ç~Č-01#Î
AR-14-ST-059994-01
02.12.2014Report date
Analytical report
Eurofins Agro Testing Ukraine LLCSample sender
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
18.11.2014Reception date time
CourierTransport by
Sample condition unreservedly
17.11.2014Date of sampling
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Number of tested samples 1
Start analysis
End Analysis 24.11.2014
19.11.2014
720-2014-00110519 Vegetable- fat mix "Chocolate Tulchynka 62%"Type of sample
0610140008Partie-no.
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Test results
720-2014-00110519
Vegetable- fat mix
"Chocolate Tulchynka 62%"
Not Detected /25 g
(A)UM2PF: Salmonella
Method: ISO 6579
< 10 cfu/g
(A)UMJPR: Anaerobic Sulphite Reducing Bacteria
Method: ISO 15213
Not Detected /1 g
(A)UMIMW: Coagulase positive Staphylococcus
Method: ISO 6888-3
< 10 cfu/g
(A)UMARE: Coliforms 30°C
Method: ISO 4832
Not Detected /25 g
(A)UM7CU: Listeria monocytogenes
Method: ISO 11290-1 A1
< 10 cfu/g
(A)UMFZ4: Moulds
Method: ISO 21527-1
< 10 cfu/g
(A)UMMJ5: Yeast
Method: ISO 21527-1
Report date
AR-14-ST-059994-012/2
02.12.2014
Page Analytical report
720-2014-00110519
Vegetable- fat mix
"Chocolate Tulchynka 62%"
32000 cfu/g
(A)UM274: Aerobic Plate Count 30°C
Method: ISO 4833-1
A = Method accredited
Approved by:Authorized by:Magdalena Duszynska
Analytical Service Manager
Rafal Sawaniewski
Older Assistant
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing,
by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
technical information
Tests and packages
Pesticides OC/OP/Py (fats & oils)PSP46
LOQ
- Organochlorine Pesticides, Pyrethroides [SP421-4]
2.3.4.6-Tetrachloranisol 0.005 mg/kg
Aclonifen 0.01 mg/kg
Acrinathrin 0.05 mg/kg
Aldrin 0.005 mg/kg
Aldrin/ Dieldrin (Sum)
Benfluralin 0.005 mg/kg
Benzoylprop-ethyl 0.01 mg/kg
Bifenox 0.02 mg/kg
Bifenthrin 0.05 mg/kg
Binapacryl 0.02 mg/kg
Bromocyclen 0.01 mg/kg
Bromoxynil-octanoate 0.01 mg/kg
Butralin 0.02 mg/kg
Chlordane (total)
Chlordane, cis- 0.005 mg/kg
Chlordane, oxy- 0.005 mg/kg
Chlordane, trans- 0.005 mg/kg
Chlorfenapyr 0.01 mg/kg
Chlorfenprop-methyl 0.02 mg/kg
Chlorfenson 0.01 mg/kg
Chloroneb 0.02 mg/kg
Chlorothalonil 0.01 mg/kg
Chlorthal-dimethyl 0.005 mg/kg
Cyfluthrin 0.05 mg/kg
Cyhalothrin, lambda- 0.05 mg/kg
Cypermethrin 0.05 mg/kg
Cyphenothrin 0.05 mg/kg
DDD, o,p- 0.005 mg/kg
DDD, p,p'- 0.005 mg/kg
DDE, o,p- 0.005 mg/kg
DDE, p,p'- 0.005 mg/kg
DDT (total)
DDT, o,p'- 0.005 mg/kg
DDT, p,p'- 0.005 mg/kg
Deltamethrin 0.05 mg/kg
Dibromobenzophenone, p,p- 0.02 mg/kg
Dichlobenil 0.01 mg/kg
Dichlone 0.02 mg/kg
Dichlorobenzophenone, o,p- 0.02 mg/kg
Dichlorobenzophenone, p,p- 0.02 mg/kg
Dicloran 0.005 mg/kg
Dicofol (sum)
Dicofol, o,p- 0.02 mg/kg
Dicofol, p,p- 0.02 mg/kg
Dieldrin 0.005 mg/kg
Page 1 of 514-November-2014 TM4TP
technical information
Dienochlor 0.01 mg/kg
Dinitramine 0.01 mg/kg
Dinobuton 0.02 mg/kg
Endosulfan (total)
Endosulfan sulphate 0.01 mg/kg
Endosulfan, alpha- 0.005 mg/kg
Endosulfan, beta- 0.005 mg/kg
Endrin 0.005 mg/kg
Endrin ketone 0.01 mg/kg
Ethalfluralin 0.01 mg/kg
Etridiazole 0.01 mg/kg
Fenfluthrin 0.05 mg/kg
Fenpropathrin 0.05 mg/kg
Fenson 0.01 mg/kg
Fenvalerate (RR-/SS-Isomers) 0.05 mg/kg
Fenvalerate (RS-/SR-Isomers) 0.05 mg/kg
Flubenzimine 0.01 mg/kg
Fluchloralin 0.01 mg/kg
Flucythrinate 0.05 mg/kg
Flumetralin 0.01 mg/kg
Fluorodifen 0.01 mg/kg
Fluoroimide 0.02 mg/kg
Genite 0.01 mg/kg
Halfenprox 0.05 mg/kg
HCH isomers (without lindane)
HCH, alpha- 0.005 mg/kg
HCH, beta- 0.005 mg/kg
HCH, delta- 0.005 mg/kg
HCH, epsilon- 0.005 mg/kg
Heptachlor 0.005 mg/kg
Heptachlor (sum)
Heptachlor epoxide, cis- 0.005 mg/kg
Heptachlor epoxide, trans- 0.005 mg/kg
Hexachlorobenzene (HCB) 0.005 mg/kg
Ioxynil-Octanoate 0.01 mg/kg
Isobenzan 0.005 mg/kg
Isodrin 0.005 mg/kg
Isopropalin 0.01 mg/kg
Lindane (gamma-HCH) 0.005 mg/kg
Methoxychlor 0.01 mg/kg
Mirex 0.005 mg/kg
Nitrapyrin 0.01 mg/kg
Nitrofen 0.01 mg/kg
Nonachlor, trans- 0.005 mg/kg
Octachlorstyrene 0.005 mg/kg
Other screened pesticides
Oxyfluorfen 0.01 mg/kg
Pendimethalin 0.01 mg/kg
Pentachloranisole 0.005 mg/kg
Pentachloroaniline 0.005 mg/kg
Pentachlorobenzene 0.01 mg/kg
Pentachlorothioanisole 0.005 mg/kg
Permethrin 0.05 mg/kg
Plifenate 0.02 mg/kg
Polychloroterpene (Camphechlor) 0.5 mg/kg
Profluralin 0.005 mg/kg
Page 2 of 514-November-2014 TM4TP
technical information
Quintozene 0.005 mg/kg
Quintozene (sum)
S 421 0.01 mg/kg
Screened pesticides
tau-Fluvalinate 0.05 mg/kg
Tecnazene 0.005 mg/kg
Tefluthrin 0.05 mg/kg
Tetradifon 0.01 mg/kg
Tetrasul 0.01 mg/kg
Tralomethrin 0.05 mg/kg
Transfluthrin 0.05 mg/kg
Triallate 0.02 mg/kg
Trichloronat 0.01 mg/kg
Trifluralin 0.005 mg/kg
- Organophosphorus Pesticides [SP424-3]
Acephate 0.02 mg/kg
Azinphos-ethyl 0.05 mg/kg
Azinphos-methyl 0.05 mg/kg
Bromfenvinphos 0.02 mg/kg
Bromophos-ethyl 0.02 mg/kg
Bromophos-methyl 0.02 mg/kg
Butamifos 0.02 mg/kg
Cadusaphos 0.02 mg/kg
Carbophenothion 0.02 mg/kg
Carbophenothion-methyl 0.02 mg/kg
Chlorfenvinphos 0.02 mg/kg
Chlormephos 0.02 mg/kg
Chlorpyrifos (-ethyl) 0.02 mg/kg
Chlorpyrifos-methyl 0.02 mg/kg
Chlorthion 0.02 mg/kg
Chlorthiophos 0.02 mg/kg
Coumaphos 0.1 mg/kg
Crotoxyphos 0.02 mg/kg
Crufomate 0.02 mg/kg
Cyanofenphos 0.05 mg/kg
Cyanophos 0.02 mg/kg
Demeton-S-methyl 0.05 mg/kg
Demeton-S-methyl-sulfone 0.1 mg/kg
Dialifos 0.02 mg/kg
Diazinon 0.02 mg/kg
Dicapthon 0.02 mg/kg
Dichlofenthion 0.02 mg/kg
Dichlorvos 0.02 mg/kg
Dicrotophos 0.02 mg/kg
Dimefox 0.02 mg/kg
Dimethoate 0.02 mg/kg
Dimethylvinphos 0.02 mg/kg
Dioxabenzofos 0.02 mg/kg
Dioxathion 0.05 mg/kg
Disulfoton 0.05 mg/kg
Disulfoton-sulfon 0.05 mg/kg
Disulfoton-sulfoxide 0.05 mg/kg
Ditalimfos 0.02 mg/kg
Edifenphos 0.05 mg/kg
Ethion 0.02 mg/kg
Page 3 of 514-November-2014 TM4TP
technical information
Ethoprophos 0.02 mg/kg
Etrimfos 0.02 mg/kg
Fenamiphos 0.02 mg/kg
Fenamiphos-sulfone 0.05 mg/kg
Fenamiphos-sulfoxide 0.05 mg/kg
Fenchlorphos 0.02 mg/kg
Fenchlorphos oxon 0.05 mg/kg
Fenitrothion 0.02 mg/kg
Fensulfothion 0.02 mg/kg
Fensulfothion-oxon-sulfone 0.05 mg/kg
Fensulfothion-oxon-sulfoxide 0.05 mg/kg
Fensulfothion-sulfone 0.05 mg/kg
Fenthion 0.02 mg/kg
Fenthion-oxon-sulfone 0.05 mg/kg
Fenthion-oxon-sulfoxide 0.05 mg/kg
Fenthion-sulfone 0.05 mg/kg
Fenthion-sulfoxide 0.05 mg/kg
Fonofos 0.02 mg/kg
Formothion 0.02 mg/kg
Fosthiazate 0.05 mg/kg
Fosthietan 0.02 mg/kg
Heptenophos 0.02 mg/kg
Iodofenphos 0.05 mg/kg
Iprobenfos 0.02 mg/kg
Isazophos 0.02 mg/kg
Isocarbofos 0.02 mg/kg
Isofenphos 0.02 mg/kg
Isofenphos-methyl 0.02 mg/kg
Isoxathion 0.05 mg/kg
Leptophos 0.05 mg/kg
Malaoxon 0.02 mg/kg
Malathion 0.02 mg/kg
Mecarbam 0.02 mg/kg
Mephosfolan 0.02 mg/kg
Merphos 0.05 mg/kg
Methacriphos 0.02 mg/kg
Methamidophos 0.02 mg/kg
Methidathion 0.02 mg/kg
Mevinphos 0.02 mg/kg
Monocrotophos 0.02 mg/kg
Morphothion 0.05 mg/kg
Omethoate 0.02 mg/kg
Other screened pesticides
Oxydemeton-methyl 0.1 mg/kg
Paraoxon-ethyl 0.02 mg/kg
Paraoxon-methyl 0.02 mg/kg
Parathion 0.02 mg/kg
Parathion-methyl 0.02 mg/kg
Phenkapton 0.05 mg/kg
Phenthoate 0.02 mg/kg
Phorate 0.02 mg/kg
Phorate-sulfone 0.05 mg/kg
Phorate-sulfoxide 0.05 mg/kg
Phosalone 0.05 mg/kg
Phosmet 0.05 mg/kg
Phosphamidon 0.02 mg/kg
Page 4 of 514-November-2014 TM4TP
technical information
Pirimiphos-ethyl 0.02 mg/kg
Pirimiphos-methyl 0.02 mg/kg
Profenofos 0.02 mg/kg
Propaphos 0.02 mg/kg
Propetamphos 0.02 mg/kg
Prothiofos 0.02 mg/kg
Prothoate 0.02 mg/kg
Pyraclofos 0.05 mg/kg
Pyrazophos 0.05 mg/kg
Pyridaphenthion 0.02 mg/kg
Quinalphos 0.02 mg/kg
Quintiofos 0.02 mg/kg
Sulfotep 0.02 mg/kg
Sulprofos 0.05 mg/kg
TEPP 0.02 mg/kg
Terbufos 0.02 mg/kg
Terbufos-sulfone 0.05 mg/kg
Tetrachlorvinphos 0.02 mg/kg
Thiometon 0.02 mg/kg
Tolclofos-methyl 0.02 mg/kg
Triamiphos 0.05 mg/kg
Triazophos 0.02 mg/kg
Trichlorfon 0.1 mg/kg
Vamidothion 0.05 mg/kg
- Extraction DFG S19 fats and oils [SPP03-1]
LOD: Limit of detectionLOQ: Limit of Quantification
Page 5 of 514-November-2014 TM4TP
Eurofins Polska Sp. z.o.o.
Aleja Wojska Polskiego 90 A
PL-82 200 Malbork
POLAND
Tel: +48 552 720 473, Fax: +48 552 720 475
www.eurofins.pl
1/2Page
Polska
{9DE5FF1B-B627-479E-95D7-A3E9988AB778}
Eurofins Agro Testing Ukraine LLC
BC "Forum Victoria Park"
office 2-202, Okhtyrskiy Lane, post box 22
03680 Kyiv
UKRAINA
ĚAR-14-ST-Ç%Ç|Č-01pÎ
AR-14-ST-059992-01
02.12.2014Report date
Analytical report
Eurofins Agro Testing Ukraine LLCSample sender
Prescriber Eurofins Agro Testing Ukraine LLC
Purchase order date 17.11.2014
18.11.2014Reception date time
CourierTransport by
Sample condition unreservedly
17.11.2014Date of sampling
Sample taken by client
Type of sampling another way of sampling guarantee its representativeness
Purpose of the testing other
Number of tested samples 1
Start analysis
End Analysis 24.11.2014
19.11.2014
720-2014-00110517 Vegetable- fat mix "Tulchynka 72.5%"Type of sample
191014084Partie-no.
Supplier name Customer (name and address) JSC International Media Center-
CTV 03113, Ukraine, Kiev, 1 Shevtsova Str.
Test results
720-2014-00110517
Vegetable- fat mix
"Tulchynka 72.5%"
Not Detected /25 g
(A)UM2PF: Salmonella
Method: ISO 6579
< 10 cfu/g
(A)UMJPR: Anaerobic Sulphite Reducing Bacteria
Method: ISO 15213
Not Detected /1 g
(A)UMIMW: Coagulase positive Staphylococcus
Method: ISO 6888-3
< 10 cfu/g
(A)UMARE: Coliforms 30°C
Method: ISO 4832
Not Detected /25 g
(A)UM7CU: Listeria monocytogenes
Method: ISO 11290-1 A1
< 10 cfu/g
(A)UMFZ4: Moulds
Method: ISO 21527-1
< 10 cfu/g
(A)UMMJ5: Yeast
Method: ISO 21527-1
Report date
AR-14-ST-059992-012/2
02.12.2014
Page Analytical report
720-2014-00110517
Vegetable- fat mix
"Tulchynka 72.5%"
4700 cfu/g
(A)UM274: Aerobic Plate Count 30°C
Method: ISO 4833-1
A = Method accredited
Approved by:Authorized by:Magdalena Duszynska
Analytical Service Manager
Rafal Sawaniewski
Older Assistant
1. The results refer only to the tested samples.
2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o.
3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the
customer’s wish.
4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing,
by mail or fax.
NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179

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Tulchinka

  • 1. 1/4Page 08.12.2014Report date Polska Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl AR-14-ST-061473-01 ĚAR-14-ST-Ç&.iČ-01Î Analytical report {01ACBDB7-9D01-4A1D-8B44-4D031AAFE724} Sample Code 720-2014-00110505 Type of sample Vegetable-fat mix "Tulchynka 82.5%" 200g Sample sender Eurofins Agro Testing Ukraine LLC Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 Reception date time 18.11.2014 Transport by Courier company Sample condition no proper Date of sampling 17.11.2014 Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Partie-no. 241014 026 Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Number of tested samples 1 18.11.2014Start analysis End Analysis 03.12.2014 Test results ST0J3 Estrogenes (LC-MS/MS (A) LC-MS/MS, LC- MS/MSMethod Subcontracted to an external laboratory accredited for this test Tiergesundheitsdienst Bayern e.V., accreditation nr. DIN EN ISO/IEC 17025:2005 DAkkS D-PL-18094-01-00 Diethylstilbestrol (Stilben) <LOQ µg/kg Dienestrol (Stilben) <LOQ µg/kg Estradiol (17- beta) <LOQ µg/kg Estradiol (17-alpha) <LOQ µg/kg Ethinyl-Estradiole <LOQ µg/kg Hexestrol (Stilben) <LOQ µg/kg Estrone <LOQ µg/kg Zeranol <LOQ µg/kg Taleranol <LOQ µg/kg Estriol <LOQ µg/kg J7012 Butyric acid (A) §64 LFGB L 17.00-13, mod., GC-FIDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Butyric acid 0.35 g/100 g fat JJV14 Milk fat (A) calculationMethod
  • 2. Analytical report AR-14-ST-061473-01 720-2014-00110505Sample Code 2/4Page Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Milk fat calculated 3,2% butyric acid 9.1 % Milk fat calculated 3,5% butyric acid 8.3 % J5003 Aflatoxin M1 (milk products) (A) internal method based on EN ISO 14501, IAC, HPLC-FLDMethod Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Aflatoxin M1 <0.01 * µg/kg ST00T Water content (A) EN ISO 3727-1:2004, weightMethod Moisture 15.94 ± 0.96% ST05L Peroxide value. Animal and vegetable oils and fats (A) ISO 3960:2012, titrationMethod Peroxide value 0.34 ± 0.05meqO2/kg ST08J The acid number and the acidity calc.as oleic acid (A) EN ISO 660:2010, tritimetryMethod Acidity number 0.062 st Turner Acidity number 0.12 st Koettstorfer a ST0EX Melting point (#) ISO 6321, open capillary (flowing point)Method Subcontracted to an external laboratory Melting Point 28.30 °C FGM02 Inhibition test (A) In-House method, Kundrat AgarMethod Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 DAkkS PL-14268-01 Inhibitory substances Not Detected JCAF2 Aflatoxins B1, B2, G1, G2 (fats, oils, lecithin) (A) internal method based on EN 14123, IAC, HPLC-FLDMethod Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Aflatoxin B1 <0.1 * µg/kg Aflatoxin B2 <0.1 * µg/kg Aflatoxin G1 <0.1 * µg/kg Aflatoxin G2 <0.1 * µg/kg Sum of all positive identified Aflatoxins <0.4 * µg/kg JJF02 Fat total (A) §64 LFGB L 06.00-6, mod., GravimetryMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Fat, total 83.4 ± 2.5g/100 g SP421 Organochlorine Pesticides, Pyrethroides (A) ASU L00.00-34, GC-ECDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14198-01-00 Screened pesticides Not Detected SP424 Organophosphorus Pesticides (A) ASU L00.00-34, GC-FPDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14198-01-00 Screened pesticides Not Detected ST0J0 Contents of total sugars (A) PN-85/A-82100, tritimetryMethod Total sugars 1.0 ± 0.2% ST0QQ Dry mass, without fat (A) PN-EN ISO 3727-2: 2004, weightMethod Dry matter, free of fat 1.81 ± 0.29% SZFB0 Fatty acids profile (A) Internal Method, GC/FIDMethod
  • 3. Analytical report AR-14-ST-061473-01 720-2014-00110505Sample Code 3/4Page Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Trans fatty acids total/sample 2.21 g/100 g fat mono-unsaturated fatty acids total/sample 31.15 g/100 g fat poly-unsaturated fatty acids total/sample 21.01 g/100 g fat saturated fatty acids total/sample 47.85 g/100 g fat C10:0 Capric acid (Methyl decanoate) 0.61 g/100 g fat C11:0 Undecanoic acid (Methyl undecanoate) <0.5 g/100 g fat C12:0 Lauric acid (Methyl dodecanoate) 3.96 g/100 g fat C13:0 Tridecanoic acid (Methyl tridecanoate) <0.5 g/100 g fat C14:0 Myristic acid (Methyl myristate) 2.72 g/100 g fat C14:1 Myristoleic acid (Methyl myristoleate) <0.5 g/100 g fat C15:0 Pentadecanoic acid (Methyl pentadecanoate) <0.5 g/100 g fat C15:1 Pentadecenoic acid (cis-10) <0.5 g/100 g fat C16:0 Palmitic acid (Methyl palmitate) 34 g/100 g fat C16:1 Palmitoleic acid (Methyl palmitoleate) <0.5 g/100 g fat C17:0 Heptadecanoic acid (Methyl heptadecanoate) <0.5 g/100 g fat C17:1 Heptadecenoic acid (cis-10-heptadecenoate) <0.5 g/100 g fat C18:0 Stearic acid (Methyl stearate) 5.62 g/100 g fat C18:1n11c cis-Vaccen acid (cis-Methyl vaccenate) 21 g/100 g fat C18:1n11t Vaccen acid (trans-Methyl vaccenate) 1.09 g/100 g fat C18:1n6 Petroselin acid (Methyl petroselaidate) <0.5 g/100 g fat C18:1n9 Oleic acid (Methyl oleate) 28.4 g/100 g fat C18:1n9t Elaidic acid (Methyl elaidate) 1.12 g/100 g fat C18:2n6 Linoleic acid (Methyl linoleate) 21 g/100 g fat C18:2n6t Linoleaidic acid (Methyl linolelaidate) <0.5 g/100 g fat C18:3n3 Apha-Linolenic acid (Methyl linolenate) <0.5 g/100 g fat C18:3n6 γ-linolenic acid (Methyl γ-linolenate) <0.5 g/100 g fat C20:0 Arachidic acid (Methyl arachidate) <0.5 g/100 g fat C20:1 Eicosenoic acid (Methyl cis-11-eicosenoate) <0.5 g/100 g fat C20:2n6 Eicosadienoic acid (cis-11,14) <0.5 g/100 g fat C20:3n3 Eicosatrienoic acid (cis-11,14,17) <0.5 g/100 g fat C20:3n6 Dihomo-γ-linolenic acid (cis-8,11,14) <0.5 g/100 g fat C20:4n6 Arachidonic acid (Methyl arachidonate) <0.5 g/100 g fat C20:5n3 Eicosapentaenoic acid (cis-5,8,11,14,17) <0.5 g/100 g fat C21:0 Heneicosanoic acid (Methyl heneicosanote) <0.5 g/100 g fat C22:0 Behenic acid (Methyl behenate) <0.5 g/100 g fat C22:1n9 Erucic acid (Methyl cis-13-docosenoate) <0.5 g/100 g fat C22:2 Docosadienoic acid (cis-13,16) <0.5 g/100 g fat C22:5 Docosapentaenic acid <0.5 g/100 g fat C22:6n-3 Docosahexaenoic (DHA) <0.5 g/100 g fat C23:0 Tricosanoic acid (Methyl tricosanoate) <0.5 g/100 g fat C24:0 Lignoceric acid (Methyl tetracosanoate) <0.5 g/100 g fat C24:1n9 Nervonic acid (cis-15-tetracosenoate) <0.5 g/100 g fat C4:0 Butyric acid (Methyl butyrate) <0.5 g/100 g fat C6:0 Caproic acid (Methyl hexanoate) <0.5 g/100 g fat C8:0 Caprylic acid (Methyl octanoate) 0.56 g/100 g fat SZQA1 Arsenic (As) (A) LS-PP-CH-2/2, AAS-HG method (hydride technique)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Arsenic (As) <0.030 mg/kg SZQA2 Cadmium (Cd) (A) LS-PP-CH-2/4, AAS-ETA method (electrothermic atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106
  • 4. Analytical report AR-14-ST-061473-01 720-2014-00110505Sample Code 4/4Page Cadmium (Cd) <0.010 mg/kg SZQA4 Copper (Cu) (A) LS-PP-CH-2/8, AAS-F method (flame atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Copper (Cu) 0.84 mg/kg SZQA6 Iron (Fe) (A) LS-PP-CH-2/20, AES-ICPMethod Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Iron (Fe) <0.50 mg/kg SZQA7 Lead (Pb) (A) LS-PP-CH-2/25, AAS-ETA method (electrothermic atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Lead (Pb) <0.050 mg/kg SZQAA Mercury (Hg) (A) LS-PP-CH-30, AAS-AMA methodMethod Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Mercury (Hg) <0.004 mg/kg SZQAG Zinc (Zn) (A) LS-PP-CH-2/12, AAS-F method (flame atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Zinc (Zn) 0.99 mg/kg Below indicated quantification level* = # = Not accredited A = Method accredited +/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The result and its uncertainty refer to the analyzed sample. JUDGEMENT LOQ- Below indicated quantification level List of analyzed pesticides is attached to the report. Estrogenes: LOQ- 1 µg/kg Approved by:Authorized by:Elżbieta Szyszkowska Team Leader Analytical Service Manager Joanna Brzoza 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 5. 1/2Page 08.12.2014Report date Polska Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl AR-14-ST-061472-01 ĚAR-14-ST-Ç&.hČ-01OÎ Analytical report {F06DD157-7FAC-456B-A32C-6722A4752E65} Sample Code 720-2014-00110506 Type of sample Vegetable-fat mix "Tulchynka 72.5%" 200g Sample sender Eurofins Agro Testing Ukraine LLC Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 Reception date time 18.11.2014 Transport by Courier company Sample condition no proper Date of sampling 17.11.2014 Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Partie-no. 191014084 Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Number of tested samples 1 18.11.2014Start analysis End Analysis 03.12.2014 Test results J7012 Butyric acid (A) §64 LFGB L 17.00-13, mod., GC-FIDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Butyric acid 0.35 g/100 g fat JJV14 Milk fat (A) calculationMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Milk fat calculated 3,2% butyric acid 7.9 % Milk fat calculated 3,5% butyric acid 7.2 % ST00T Water content (A) EN ISO 3727-1:2004, weightMethod Moisture 24.40 ± 1.46% ST08J The acid number and the acidity calc.as oleic acid (A) EN ISO 660:2010, tritimetryMethod Acidity number 0.05 ± 0.01st Turnera Acidity number 0.11 ± 0.02st Koettstorfer a FGM02 Inhibition test (A) In-House method, Kundrat AgarMethod
  • 6. Analytical report AR-14-ST-061472-01 720-2014-00110506Sample Code 2/2Page Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 DAkkS PL-14268-01 Inhibitory substances Not Detected JJF02 Fat total (A) §64 LFGB L 06.00-6, mod., GravimetryMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Fat, total 71.9 ± 2.2g/100 g ST0QQ Dry mass, without fat (A) PN-EN ISO 3727-2: 2004, weightMethod Dry matter, free of fat 3.92 ± 0.63% A = Method accredited +/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The result and its uncertainty refer to the analyzed sample. Approved by:Authorized by:Elżbieta Szyszkowska Team Leader Analytical Service Manager Joanna Brzoza 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 7. 1/2Page 08.12.2014Report date Polska Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl AR-14-ST-061469-01 ĚAR-14-ST-Ç&.eČ-01(Î Analytical report {EAB9E494-3C4E-4CC4-94BD-117BB5CE5079} Sample Code 720-2014-00110507 Type of sample Vegetable- fat mix "Tulchynka 62.5%" 200g Sample sender Eurofins Agro Testing Ukraine LLC Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 Reception date time 18.11.2014 Transport by Courier company Sample condition no proper Date of sampling 17.11.2014 Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Partie-no. 201014068 Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Number of tested samples 1 18.11.2014Start analysis End Analysis 03.12.2014 Test results J7012 Butyric acid (A) §64 LFGB L 17.00-13, mod., GC-FIDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Butyric acid 0.40 g/100 g fat JJV14 Milk fat (A) calculationMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Milk fat calculated 3,2% butyric acid 8.1 % Milk fat calculated 3,5% butyric acid 7.4 % ST00T Water content (A) EN ISO 3727-1:2004, weightMethod Moisture 32.75 ± 1.97% ST08J The acid number and the acidity calc.as oleic acid (A) EN ISO 660:2010, tritimetryMethod Acidity number 0.066 Turnera Acidity number 0.131 st Koettstorfer a FGM02 Inhibition test (A) In-House method, Kundrat AgarMethod
  • 8. Analytical report AR-14-ST-061469-01 720-2014-00110507Sample Code 2/2Page Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 DAkkS PL-14268-01 Inhibitory substances Not Detected JJF02 Fat total (A) §64 LFGB L 06.00-6, mod., GravimetryMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Fat, total 64.8 ± 1.9g/100 g ST0QQ Dry mass, without fat (A) PN-EN ISO 3727-2: 2004, weightMethod Dry matter, free of fat 3.84 ± 0.61% A = Method accredited +/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The result and its uncertainty refer to the analyzed sample. Approved by:Authorized by:Elżbieta Szyszkowska Team Leader Analytical Service Manager Joanna Brzoza 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 9. 1/4Page 10.12.2014Report date Polska Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl AR-14-ST-061474-01 ĚAR-14-ST-Ç&.jČ-01iÎ Analytical report {78BD63EE-5BD0-44E5-BCB1-30B0A8C618D7} Sample Code 720-2014-00110508 Type of sample Vegetable- fat mix "Chocolate Tulchynka 62%" Sample sender Eurofins Agro Testing Ukraine LLC Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 Reception date time 18.11.2014 Transport by Courier company Sample condition no proper Date of sampling 17.11.2014 Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Partie-no. 061014 008 Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Number of tested samples 1 18.11.2014Start analysis End Analysis 02.12.2014 Test results J7012 Butyric acid (A) §64 LFGB L 17.00-13, mod., GC-FIDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Butyric acid 0.45 g/100 g fat JJV14 Milk fat (A) calculationMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Milk fat calculated 3,2% butyric acid 8.5 % Milk fat calculated 3,5% butyric acid 7.7 % JJ006 Aflatoxins B1, B2, G1, G2 (nuts, cocoa, cereals) (A) internal method based on EN 14123, IAC, HPLC-FLDMethod Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Aflatoxin B1 <0.1 * µg/kg Aflatoxin B2 <0.1 * µg/kg Aflatoxin G1 <0.1 * µg/kg Aflatoxin G2 <0.1 * µg/kg J5003 Aflatoxin M1 (milk products) (A) internal method based on EN ISO 14501, IAC, HPLC-FLDMethod
  • 10. Analytical report AR-14-ST-061474-01 720-2014-00110508Sample Code 2/4Page Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Aflatoxin M1 <0.01 * µg/kg JJF02 Fat total (A) §64 LFGB L 06.00-6, mod., GravimetryMethod Subcontracted to the accredited Eurofins laboratory Eurofins Analytik GmbH, Wiertz-Eggert-Jörissen, accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14251-01-00 Fat, total 60.2 ± 1.8g/100 g ST00T Water content (A) EN ISO 3727-1:2004, , weightMethod Moisture 16.15 ± 0.97% ST05L Peroxide value. Animal and vegetable oils and fats (A) ISO 3960:2012, titrationMethod Peroxide value 0.27 ± 0.04meqO2/kg ST08J The acid number and the acidity calc.as oleic acid (A) EN ISO 660:2010, tritimetryMethod Acidity number 0,054 st Turnera Acidity number 0,108 st Koettstorfer a ST0EX Melting point (#) ISO 6321, open capillary (flowing point)Method Subcontracted to an external laboratory Melting Point 33.20 °C FGM02 Inhibition test (A) In-House method, Kundrat AgarMethod Subcontracted to the accredited Eurofins laboratory Eurofins Fintelmann und Meyer GMP (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 DAkkS PL-14268-01 Inhibitory substances not detected JCAF2 Aflatoxins B1, B2, G1, G2 (fats, oils, lecithin) (A) internal method based on EN 14123, IAC, HPLC-FLDMethod Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Sum of all positive identified Aflatoxins Sum of all positive identified Aflatoxins JJ006 Aflatoxins B1, B2, G1, G2 (nuts, cocoa, cereals) (A) internal method based on EN 14123, IAC, HPLC-FLDMethod Subcontracted to the accredited Eurofins laboratory Eurofins WEJ Contaminants GmbH (Hamburg), accreditation nr. EN ISO/IEC 17025:2005 DAKKS D-PL-14602-01-00 Sum of all positive identified Aflatoxins Sum of all positive identified Aflatoxins <0.4 * µg/kg SP421 Organochlorine Pesticides, Pyrethroides (A) ASU L00.00-34, GC-ECDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14198-01-00 Screened pesticides Not Detected SP424 Organophosphorus Pesticides (A) ASU L00.00-34, GC-FPDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Dr. Specht Laboratorien (Hamburg), accreditation nr. DIN EN ISO/IEC 17025:2005 D-PL-14198-01-00 Screened pesticides Not Detected ST0J0 Contents of total sugars (A) PN-85/A-82100, tritimetryMethod Total sugars 21.9 ± 4.4% ST0QQ Dry mass, without fat (A) PN-EN ISO 3727-2: 2004, , weightMethod Dry matter, free of fat 24.41 ± 3.91% SZFB0 Fatty acids profile (A) Internal Method, GC/FIDMethod Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Trans fatty acids total/sample 2.17 g/100 g fat
  • 11. Analytical report AR-14-ST-061474-01 720-2014-00110508Sample Code 3/4Page poly-unsaturated fatty acids total/sample 14.17 g/100 g fat saturated fatty acids total/sample 53.19 g/100 g fat mono-unsaturated fatty acids total/sample 32.64 g/100 g fat C10:0 Capric acid (Methyl decanoate) 1.15 g/100 g fat C11:0 Undecanoic acid (Methyl undecanoate) <0.5 g/100 g fat C12:0 Lauric acid (Methyl dodecanoate) 6.83 g/100 g fat C13:0 Tridecanoic acid (Methyl tridecanoate) <0.5 g/100 g fat C14:0 Myristic acid (Methyl myristate) 4.33 g/100 g fat C14:1 Myristoleic acid (Methyl myristoleate) <0.5 g/100 g fat C15:0 Pentadecanoic acid (Methyl pentadecanoate) <0.5 g/100 g fat C15:1 Pentadecenoic acid (cis-10) <0.5 g/100 g fat C16:0 Palmitic acid (Methyl palmitate) 33 g/100 g fat C16:1 Palmitoleic acid (Methyl palmitoleate) <0.5 g/100 g fat C17:0 Heptadecanoic acid (Methyl heptadecanoate) <0.5 g/100 g fat C17:1 Heptadecenoic acid (cis-10-heptadecenoate) <0.5 g/100 g fat C18:0 Stearic acid (Methyl stearate) 6.25 g/100 g fat C18:1n11c cis-Vaccen acid (cis-Methyl vaccenate) 14.2 g/100 g fat C18:1n11t Vaccen acid (trans-Methyl vaccenate) 0.84 g/100 g fat C18:1n6 Petroselin acid (Methyl petroselaidate) <0.5 g/100 g fat C18:1n9 Oleic acid (Methyl oleate) 29.8 g/100 g fat C18:1n9t Elaidic acid (Methyl elaidate) 1.33 g/100 g fat C18:2n6 Linoleic acid (Methyl linoleate) 14.2 g/100 g fat C18:2n6t Linoleaidic acid (Methyl linolelaidate) <0.5 g/100 g fat C18:3n3 Apha-Linolenic acid (Methyl linolenate) <0.5 g/100 g fat C18:3n6 γ-linolenic acid (Methyl γ-linolenate) <0.5 g/100 g fat C20:0 Arachidic acid (Methyl arachidate) <0.5 g/100 g fat C20:1 Eicosenoic acid (Methyl cis-11-eicosenoate) <0.5 g/100 g fat C20:2n6 Eicosadienoic acid (cis-11,14) <0.5 g/100 g fat C20:3n3 Eicosatrienoic acid (cis-11,14,17) <0.5 g/100 g fat C20:3n6 Dihomo-γ-linolenic acid (cis-8,11,14) <0.5 g/100 g fat C20:4n6 Arachidonic acid (Methyl arachidonate) <0.5 g/100 g fat C20:5n3 Eicosapentaenoic acid (cis-5,8,11,14,17) <0.5 g/100 g fat C21:0 Heneicosanoic acid (Methyl heneicosanote) <0.5 g/100 g fat C22:0 Behenic acid (Methyl behenate) <0.5 g/100 g fat C22:1n9 Erucic acid (Methyl cis-13-docosenoate) <0.5 g/100 g fat C22:2 Docosadienoic acid (cis-13,16) <0.5 g/100 g fat C22:5 Docosapentaenic acid <0.5 g/100 g fat C22:6n-3 Docosahexaenoic (DHA) <0.5 g/100 g fat C23:0 Tricosanoic acid (Methyl tricosanoate) <0.5 g/100 g fat C24:0 Lignoceric acid (Methyl tetracosanoate) <0.5 g/100 g fat C24:1n9 Nervonic acid (cis-15-tetracosenoate) <0.5 g/100 g fat C4:0 Butyric acid (Methyl butyrate) <0.5 g/100 g fat C6:0 Caproic acid (Methyl hexanoate) <0.5 g/100 g fat C8:0 Caprylic acid (Methyl octanoate) 1.26 g/100 g fat SZQA1 Arsenic (As) (A) LS-PP-CH-2/2, AAS-HG method (hydride technique)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Arsenic (As) <0.030 mg/kg SZQA2 Cadmium (Cd) (A) LS-PP-CH-2/4, AAS-ETA method (electrothermic atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Cadmium (Cd) <0.010 mg/kg SZQA4 Copper (Cu) (A) LS-PP-CH-2/8, AAS-F method (flame atomization)Method
  • 12. Analytical report AR-14-ST-061474-01 720-2014-00110508Sample Code 4/4Page Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Copper (Cu) 1.1 mg/kg SZQA6 Iron (Fe) (A) LS-PP-CH-2/20, AES-ICPMethod Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Iron (Fe) 20.7 mg/kg SZQA7 Lead (Pb) (A) LS-PP-CH-2/25, AAS-ETA method (electrothermic atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Lead (Pb) <0.050 mg/kg SZQAA Mercury (Hg) (A) LS-PP-CH-30, AAS-AMA methodMethod Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Mercury (Hg) <0.004 mg/kg SZQAG Zinc (Zn) (A) LS-PP-CH-2/12, AAS-F method (flame atomization)Method Subcontracted to the accredited Eurofins laboratory Eurofins Bel/Novamann (Nové Zámky), accreditation nr. ISO/IEC 17025:2005 SNAS No. S-106 Zinc (Zn) 2.5 mg/kg Below indicated quantification level* = # = Not accredited A = Method accredited +/- Uncertainty of result presented as expanded uncertainty of measurement (95%; k=2). The uncertainty does not include the sampling. The result and its uncertainty refer to the analyzed sample. Approved by:Authorized by:Elżbieta Szyszkowska Team Leader Analytical Service Manager Joanna Brzoza 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 13. Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl 1/2Page Polska {09635A0A-28FC-4B0E-92B2-ED8D23D47D7F} Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA ĚAR-14-ST-Ç%Ç{Č-01cÎ AR-14-ST-059991-01 02.12.2014Report date Analytical report Eurofins Agro Testing Ukraine LLCSample sender Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 18.11.2014Reception date time CourierTransport by Sample condition unreservedly 17.11.2014Date of sampling Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Number of tested samples 1 Start analysis End Analysis 24.11.2014 19.11.2014 720-2014-00110516 Vegetable- fat mix "Tulchynka 82.5%"Type of sample 241014026Partie-no. Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Test results 720-2014-00110516 Vegetable- fat mix "Tulchynka 82.5%" Not Detected /25 g (A)UM2PF: Salmonella Method: ISO 6579 < 10 cfu/g (A)UMJPR: Anaerobic Sulphite Reducing Bacteria Method: ISO 15213 Not Detected /1 g (A)UMIMW: Coagulase positive Staphylococcus Method: ISO 6888-3 < 10 cfu/g (A)UMARE: Coliforms 30°C Method: ISO 4832 Not Detected /25 g (A)UM7CU: Listeria monocytogenes Method: ISO 11290-1 A1 < 10 cfu/g (A)UMFZ4: Moulds Method: ISO 21527-1 < 10 cfu/g (A)UMMJ5: Yeast Method: ISO 21527-1
  • 14. Report date AR-14-ST-059991-012/2 02.12.2014 Page Analytical report 720-2014-00110516 Vegetable- fat mix "Tulchynka 82.5%" 5800 cfu/g (A)UM274: Aerobic Plate Count 30°C Method: ISO 4833-1 A = Method accredited Approved by:Authorized by:Magdalena Duszynska Analytical Service Manager Rafal Sawaniewski Older Assistant 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 15. Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl 1/2Page Polska {C9E62175-DF2A-43A7-9E65-DC6237D4824D} Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA ĚAR-14-ST-Ç%Ç}Č-01}Î AR-14-ST-059993-01 02.12.2014Report date Analytical report Eurofins Agro Testing Ukraine LLCSample sender Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 18.11.2014Reception date time CourierTransport by Sample condition unreservedly 17.11.2014Date of sampling Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Number of tested samples 1 Start analysis End Analysis 24.11.2014 19.11.2014 720-2014-00110518 Vegetable- fat mix " Tulchynka 62.5%"Type of sample 201014068Partie-no. Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Test results 720-2014-00110518 Vegetable- fat mix " Tulchynka 62.5%" Not Detected /25 g (A)UM2PF: Salmonella Method: ISO 6579 < 10 cfu/g (A)UMJPR: Anaerobic Sulphite Reducing Bacteria Method: ISO 15213 Not Detected /1 g (A)UMIMW: Coagulase positive Staphylococcus Method: ISO 6888-3 < 10 cfu/g (A)UMARE: Coliforms 30°C Method: ISO 4832 Not Detected /25 g (A)UM7CU: Listeria monocytogenes Method: ISO 11290-1 A1 < 10 cfu/g (A)UMFZ4: Moulds Method: ISO 21527-1 < 10 cfu/g (A)UMMJ5: Yeast Method: ISO 21527-1
  • 16. Report date AR-14-ST-059993-012/2 02.12.2014 Page Analytical report 720-2014-00110518 Vegetable- fat mix " Tulchynka 62.5%" 200000 cfu/g (A)UM274: Aerobic Plate Count 30°C Method: ISO 4833-1 A = Method accredited Approved by:Authorized by:Magdalena Duszynska Analytical Service Manager Rafal Sawaniewski Older Assistant 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 17. Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl 1/2Page Polska {8B9F2DA8-DADF-4E17-8B0F-3074C8EBEE19} Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA ĚAR-14-ST-Ç%Ç~Č-01#Î AR-14-ST-059994-01 02.12.2014Report date Analytical report Eurofins Agro Testing Ukraine LLCSample sender Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 18.11.2014Reception date time CourierTransport by Sample condition unreservedly 17.11.2014Date of sampling Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Number of tested samples 1 Start analysis End Analysis 24.11.2014 19.11.2014 720-2014-00110519 Vegetable- fat mix "Chocolate Tulchynka 62%"Type of sample 0610140008Partie-no. Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Test results 720-2014-00110519 Vegetable- fat mix "Chocolate Tulchynka 62%" Not Detected /25 g (A)UM2PF: Salmonella Method: ISO 6579 < 10 cfu/g (A)UMJPR: Anaerobic Sulphite Reducing Bacteria Method: ISO 15213 Not Detected /1 g (A)UMIMW: Coagulase positive Staphylococcus Method: ISO 6888-3 < 10 cfu/g (A)UMARE: Coliforms 30°C Method: ISO 4832 Not Detected /25 g (A)UM7CU: Listeria monocytogenes Method: ISO 11290-1 A1 < 10 cfu/g (A)UMFZ4: Moulds Method: ISO 21527-1 < 10 cfu/g (A)UMMJ5: Yeast Method: ISO 21527-1
  • 18. Report date AR-14-ST-059994-012/2 02.12.2014 Page Analytical report 720-2014-00110519 Vegetable- fat mix "Chocolate Tulchynka 62%" 32000 cfu/g (A)UM274: Aerobic Plate Count 30°C Method: ISO 4833-1 A = Method accredited Approved by:Authorized by:Magdalena Duszynska Analytical Service Manager Rafal Sawaniewski Older Assistant 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179
  • 19. technical information Tests and packages Pesticides OC/OP/Py (fats & oils)PSP46 LOQ - Organochlorine Pesticides, Pyrethroides [SP421-4] 2.3.4.6-Tetrachloranisol 0.005 mg/kg Aclonifen 0.01 mg/kg Acrinathrin 0.05 mg/kg Aldrin 0.005 mg/kg Aldrin/ Dieldrin (Sum) Benfluralin 0.005 mg/kg Benzoylprop-ethyl 0.01 mg/kg Bifenox 0.02 mg/kg Bifenthrin 0.05 mg/kg Binapacryl 0.02 mg/kg Bromocyclen 0.01 mg/kg Bromoxynil-octanoate 0.01 mg/kg Butralin 0.02 mg/kg Chlordane (total) Chlordane, cis- 0.005 mg/kg Chlordane, oxy- 0.005 mg/kg Chlordane, trans- 0.005 mg/kg Chlorfenapyr 0.01 mg/kg Chlorfenprop-methyl 0.02 mg/kg Chlorfenson 0.01 mg/kg Chloroneb 0.02 mg/kg Chlorothalonil 0.01 mg/kg Chlorthal-dimethyl 0.005 mg/kg Cyfluthrin 0.05 mg/kg Cyhalothrin, lambda- 0.05 mg/kg Cypermethrin 0.05 mg/kg Cyphenothrin 0.05 mg/kg DDD, o,p- 0.005 mg/kg DDD, p,p'- 0.005 mg/kg DDE, o,p- 0.005 mg/kg DDE, p,p'- 0.005 mg/kg DDT (total) DDT, o,p'- 0.005 mg/kg DDT, p,p'- 0.005 mg/kg Deltamethrin 0.05 mg/kg Dibromobenzophenone, p,p- 0.02 mg/kg Dichlobenil 0.01 mg/kg Dichlone 0.02 mg/kg Dichlorobenzophenone, o,p- 0.02 mg/kg Dichlorobenzophenone, p,p- 0.02 mg/kg Dicloran 0.005 mg/kg Dicofol (sum) Dicofol, o,p- 0.02 mg/kg Dicofol, p,p- 0.02 mg/kg Dieldrin 0.005 mg/kg Page 1 of 514-November-2014 TM4TP
  • 20. technical information Dienochlor 0.01 mg/kg Dinitramine 0.01 mg/kg Dinobuton 0.02 mg/kg Endosulfan (total) Endosulfan sulphate 0.01 mg/kg Endosulfan, alpha- 0.005 mg/kg Endosulfan, beta- 0.005 mg/kg Endrin 0.005 mg/kg Endrin ketone 0.01 mg/kg Ethalfluralin 0.01 mg/kg Etridiazole 0.01 mg/kg Fenfluthrin 0.05 mg/kg Fenpropathrin 0.05 mg/kg Fenson 0.01 mg/kg Fenvalerate (RR-/SS-Isomers) 0.05 mg/kg Fenvalerate (RS-/SR-Isomers) 0.05 mg/kg Flubenzimine 0.01 mg/kg Fluchloralin 0.01 mg/kg Flucythrinate 0.05 mg/kg Flumetralin 0.01 mg/kg Fluorodifen 0.01 mg/kg Fluoroimide 0.02 mg/kg Genite 0.01 mg/kg Halfenprox 0.05 mg/kg HCH isomers (without lindane) HCH, alpha- 0.005 mg/kg HCH, beta- 0.005 mg/kg HCH, delta- 0.005 mg/kg HCH, epsilon- 0.005 mg/kg Heptachlor 0.005 mg/kg Heptachlor (sum) Heptachlor epoxide, cis- 0.005 mg/kg Heptachlor epoxide, trans- 0.005 mg/kg Hexachlorobenzene (HCB) 0.005 mg/kg Ioxynil-Octanoate 0.01 mg/kg Isobenzan 0.005 mg/kg Isodrin 0.005 mg/kg Isopropalin 0.01 mg/kg Lindane (gamma-HCH) 0.005 mg/kg Methoxychlor 0.01 mg/kg Mirex 0.005 mg/kg Nitrapyrin 0.01 mg/kg Nitrofen 0.01 mg/kg Nonachlor, trans- 0.005 mg/kg Octachlorstyrene 0.005 mg/kg Other screened pesticides Oxyfluorfen 0.01 mg/kg Pendimethalin 0.01 mg/kg Pentachloranisole 0.005 mg/kg Pentachloroaniline 0.005 mg/kg Pentachlorobenzene 0.01 mg/kg Pentachlorothioanisole 0.005 mg/kg Permethrin 0.05 mg/kg Plifenate 0.02 mg/kg Polychloroterpene (Camphechlor) 0.5 mg/kg Profluralin 0.005 mg/kg Page 2 of 514-November-2014 TM4TP
  • 21. technical information Quintozene 0.005 mg/kg Quintozene (sum) S 421 0.01 mg/kg Screened pesticides tau-Fluvalinate 0.05 mg/kg Tecnazene 0.005 mg/kg Tefluthrin 0.05 mg/kg Tetradifon 0.01 mg/kg Tetrasul 0.01 mg/kg Tralomethrin 0.05 mg/kg Transfluthrin 0.05 mg/kg Triallate 0.02 mg/kg Trichloronat 0.01 mg/kg Trifluralin 0.005 mg/kg - Organophosphorus Pesticides [SP424-3] Acephate 0.02 mg/kg Azinphos-ethyl 0.05 mg/kg Azinphos-methyl 0.05 mg/kg Bromfenvinphos 0.02 mg/kg Bromophos-ethyl 0.02 mg/kg Bromophos-methyl 0.02 mg/kg Butamifos 0.02 mg/kg Cadusaphos 0.02 mg/kg Carbophenothion 0.02 mg/kg Carbophenothion-methyl 0.02 mg/kg Chlorfenvinphos 0.02 mg/kg Chlormephos 0.02 mg/kg Chlorpyrifos (-ethyl) 0.02 mg/kg Chlorpyrifos-methyl 0.02 mg/kg Chlorthion 0.02 mg/kg Chlorthiophos 0.02 mg/kg Coumaphos 0.1 mg/kg Crotoxyphos 0.02 mg/kg Crufomate 0.02 mg/kg Cyanofenphos 0.05 mg/kg Cyanophos 0.02 mg/kg Demeton-S-methyl 0.05 mg/kg Demeton-S-methyl-sulfone 0.1 mg/kg Dialifos 0.02 mg/kg Diazinon 0.02 mg/kg Dicapthon 0.02 mg/kg Dichlofenthion 0.02 mg/kg Dichlorvos 0.02 mg/kg Dicrotophos 0.02 mg/kg Dimefox 0.02 mg/kg Dimethoate 0.02 mg/kg Dimethylvinphos 0.02 mg/kg Dioxabenzofos 0.02 mg/kg Dioxathion 0.05 mg/kg Disulfoton 0.05 mg/kg Disulfoton-sulfon 0.05 mg/kg Disulfoton-sulfoxide 0.05 mg/kg Ditalimfos 0.02 mg/kg Edifenphos 0.05 mg/kg Ethion 0.02 mg/kg Page 3 of 514-November-2014 TM4TP
  • 22. technical information Ethoprophos 0.02 mg/kg Etrimfos 0.02 mg/kg Fenamiphos 0.02 mg/kg Fenamiphos-sulfone 0.05 mg/kg Fenamiphos-sulfoxide 0.05 mg/kg Fenchlorphos 0.02 mg/kg Fenchlorphos oxon 0.05 mg/kg Fenitrothion 0.02 mg/kg Fensulfothion 0.02 mg/kg Fensulfothion-oxon-sulfone 0.05 mg/kg Fensulfothion-oxon-sulfoxide 0.05 mg/kg Fensulfothion-sulfone 0.05 mg/kg Fenthion 0.02 mg/kg Fenthion-oxon-sulfone 0.05 mg/kg Fenthion-oxon-sulfoxide 0.05 mg/kg Fenthion-sulfone 0.05 mg/kg Fenthion-sulfoxide 0.05 mg/kg Fonofos 0.02 mg/kg Formothion 0.02 mg/kg Fosthiazate 0.05 mg/kg Fosthietan 0.02 mg/kg Heptenophos 0.02 mg/kg Iodofenphos 0.05 mg/kg Iprobenfos 0.02 mg/kg Isazophos 0.02 mg/kg Isocarbofos 0.02 mg/kg Isofenphos 0.02 mg/kg Isofenphos-methyl 0.02 mg/kg Isoxathion 0.05 mg/kg Leptophos 0.05 mg/kg Malaoxon 0.02 mg/kg Malathion 0.02 mg/kg Mecarbam 0.02 mg/kg Mephosfolan 0.02 mg/kg Merphos 0.05 mg/kg Methacriphos 0.02 mg/kg Methamidophos 0.02 mg/kg Methidathion 0.02 mg/kg Mevinphos 0.02 mg/kg Monocrotophos 0.02 mg/kg Morphothion 0.05 mg/kg Omethoate 0.02 mg/kg Other screened pesticides Oxydemeton-methyl 0.1 mg/kg Paraoxon-ethyl 0.02 mg/kg Paraoxon-methyl 0.02 mg/kg Parathion 0.02 mg/kg Parathion-methyl 0.02 mg/kg Phenkapton 0.05 mg/kg Phenthoate 0.02 mg/kg Phorate 0.02 mg/kg Phorate-sulfone 0.05 mg/kg Phorate-sulfoxide 0.05 mg/kg Phosalone 0.05 mg/kg Phosmet 0.05 mg/kg Phosphamidon 0.02 mg/kg Page 4 of 514-November-2014 TM4TP
  • 23. technical information Pirimiphos-ethyl 0.02 mg/kg Pirimiphos-methyl 0.02 mg/kg Profenofos 0.02 mg/kg Propaphos 0.02 mg/kg Propetamphos 0.02 mg/kg Prothiofos 0.02 mg/kg Prothoate 0.02 mg/kg Pyraclofos 0.05 mg/kg Pyrazophos 0.05 mg/kg Pyridaphenthion 0.02 mg/kg Quinalphos 0.02 mg/kg Quintiofos 0.02 mg/kg Sulfotep 0.02 mg/kg Sulprofos 0.05 mg/kg TEPP 0.02 mg/kg Terbufos 0.02 mg/kg Terbufos-sulfone 0.05 mg/kg Tetrachlorvinphos 0.02 mg/kg Thiometon 0.02 mg/kg Tolclofos-methyl 0.02 mg/kg Triamiphos 0.05 mg/kg Triazophos 0.02 mg/kg Trichlorfon 0.1 mg/kg Vamidothion 0.05 mg/kg - Extraction DFG S19 fats and oils [SPP03-1] LOD: Limit of detectionLOQ: Limit of Quantification Page 5 of 514-November-2014 TM4TP
  • 24. Eurofins Polska Sp. z.o.o. Aleja Wojska Polskiego 90 A PL-82 200 Malbork POLAND Tel: +48 552 720 473, Fax: +48 552 720 475 www.eurofins.pl 1/2Page Polska {9DE5FF1B-B627-479E-95D7-A3E9988AB778} Eurofins Agro Testing Ukraine LLC BC "Forum Victoria Park" office 2-202, Okhtyrskiy Lane, post box 22 03680 Kyiv UKRAINA ĚAR-14-ST-Ç%Ç|Č-01pÎ AR-14-ST-059992-01 02.12.2014Report date Analytical report Eurofins Agro Testing Ukraine LLCSample sender Prescriber Eurofins Agro Testing Ukraine LLC Purchase order date 17.11.2014 18.11.2014Reception date time CourierTransport by Sample condition unreservedly 17.11.2014Date of sampling Sample taken by client Type of sampling another way of sampling guarantee its representativeness Purpose of the testing other Number of tested samples 1 Start analysis End Analysis 24.11.2014 19.11.2014 720-2014-00110517 Vegetable- fat mix "Tulchynka 72.5%"Type of sample 191014084Partie-no. Supplier name Customer (name and address) JSC International Media Center- CTV 03113, Ukraine, Kiev, 1 Shevtsova Str. Test results 720-2014-00110517 Vegetable- fat mix "Tulchynka 72.5%" Not Detected /25 g (A)UM2PF: Salmonella Method: ISO 6579 < 10 cfu/g (A)UMJPR: Anaerobic Sulphite Reducing Bacteria Method: ISO 15213 Not Detected /1 g (A)UMIMW: Coagulase positive Staphylococcus Method: ISO 6888-3 < 10 cfu/g (A)UMARE: Coliforms 30°C Method: ISO 4832 Not Detected /25 g (A)UM7CU: Listeria monocytogenes Method: ISO 11290-1 A1 < 10 cfu/g (A)UMFZ4: Moulds Method: ISO 21527-1 < 10 cfu/g (A)UMMJ5: Yeast Method: ISO 21527-1
  • 25. Report date AR-14-ST-059992-012/2 02.12.2014 Page Analytical report 720-2014-00110517 Vegetable- fat mix "Tulchynka 72.5%" 4700 cfu/g (A)UM274: Aerobic Plate Count 30°C Method: ISO 4833-1 A = Method accredited Approved by:Authorized by:Magdalena Duszynska Analytical Service Manager Rafal Sawaniewski Older Assistant 1. The results refer only to the tested samples. 2. The test results shall not be reproduced except in full without the written permission of Eurofins Polska Sp. z o.o. 3. Laboratory measurement uncertainty is given when it is relevant to the validity of the test result, or for compliance with specified limits and the customer’s wish. 4. The client has the right to file a complaint in a written from within 14 days of receipt of the analytical report. May be admitted only complaint in writing, by mail or fax. NIP: PL5792000046 Regon: 192897343 Nordea Bank Polska SA SWIFT-BIC NDEAPLP2 Account PL74 1440 1101 0000 0000 0161 9179