Calibration and validation , ph meter and weigh balance calibration SOPs procedure with difference and frequency of doing this hope this will be helpful for you... also comment if needed
2. .
Calibration
In measurement technology and
metrology, calibration is the comparison
of measurement values delivered by a
device under test with those of a
calibration standard of known accuracy.
3. VALIDATION
Validation is the process of establishing
documentary evidence demonstrating that a
procedure, process, or activity carried out in
testing and then production maintains the desired
level of compliance at all stages
4. DIFFERENCE BETWEEN BOTH
Calibration ensures that instrument or measuring
devices producing accurate results.Validation provides
documented evidence that a process, equipment,
method or system produces consistent results (in
other words, it ensures that uniforms batches are
produced)
5. PH METER CALIBRATION
pH meter calibration is a necessary step of using a pH meter
because of how the electrode changes over time.Your pH
electrode is designed to measure pH based off of slope and
offset (the Nernst Equation)
All pH meters require calibration and should be calibrated
anywhere from before every use to at least once a month.
6. PROCEDURE
CalibratingYour pH Meter. Place your electrode in the buffer
with a pH value of 7 and begin reading. Press the “measure”
or calibrate button to begin reading the pH once your
electrode is placed in the buffer. Allow the pH reading to
stabilize before letting it sit for approximately 1-2 minutes.
7. CALIBRATION OF WEIGHING BALANCE
Calibration is crucial to increasing a weighing scale or
balance's longevity. It is also a necessary process to
ensure valid data during rigorous testing.
Calibration of the reference weights is performed
every two years by an ISO 17025 accredited vendor.
Internal calibration daily , and predcision once a
month
8. PROCEDURE
Place 5 gm of weighing pan
Note the weight
Calculate the weight difference
Repeat the above steps using 50 gm and 100 gm
Record the weight by noting down in form
And for precision place 5 gm pan and repeat this 9 times
And note the results.