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Principles of technological
processes in dairy processing
• Heat treatment
• Centrifugation
• Homogenisation
• Standardisation
• Deaeration
Basic treatments of liquid milk
Heat treatments
Purposes
• Food safety
• Inactivation of enzymes
• Prolonging of shelf life
• Changes of milk compounds (some cases)
Heat treatments
Food safety
• Milk as a source of infection (before heat
treatment)
• Perfect growth medium for microorganisms
• Spread of tuberculosis and typhus by milk
(previously)
Heat treatments
Food safety
• Pasteurisation
– Louis Pasteur – middle of 19th century
– Lethal effect of heat on microorganisms
– Use of heat treatment as a preservative
technique
Heat treatments
Pasteurisation of milk
• special type of heat treatment
• definition: “any heat treatment of milk
which secures the certain destruction of
Tubercle bacillus (Mycobacterium
tuberculosis) without markedly affecting
the physical and chemical properties of the
milk”
Heat treatments
Pasteurisation of milk
• None of the major pathogens in milk form
spores → fortune
• All common pathogenic organisms likely to
occur in milk: killed by relatively mild heat
treatment
– only a very slight effect on the physical and
chemical properties of milk
Heat treatments
Pasteurisation of milk
• Complete safety assured by heating milk
to 63 °C for 30 minutes
• Mycobacterium tuberculosis regarded as
the index organism for pasteurisation
– any heat treatment which destroys
Mycobacterium tuberculosis ensures
devastation of all other pathogens in milk
Heat treatments
Pasteurisation of milk
• Content of other substances and
microorganisms which may
– spoil the taste
– shorten the shelf life of various dairy products
Heat treatments
Secondary purpose of heat treatment
• destruction of as many as possible of these
other organisms and enzymatic systems
• requirement of more intense heat treatment
than is needed to inactivate the pathogens
• heat treatment applied as quickly as
possible after arrival at the dairy plant
Heat treatments
Time/temperature combination
• Very important
• Determination of the heat treatment
intensity
Heat treatment
Time/temperature combination
• Heat treatment: risk of adverse effects on
– appearance
– taste
– nutritional value of milk
Heat treatments
Phosphatase enzyme
• always present in raw milk
• destroyed by the temperature/time
combination necessary for efficient
pasteurization
• presence or absence is easily confirmed
(phosphatase test)
• absence of phosphatase → milk has been
adequately heated
Lethal effect curves and time/temperature
curves for destruction of some enzymes and
microorganims
Heat treatments
The main categories of heat treatment in the
dairy industry
Heat treatments
Indirect heating
• Transfer of heat from heating medium to
cold product on the other side of partition
Heat treatments
Direct heating
• heating medium (water) mixed with product
• heat transfer efficient for rapid heating
• use: sterilisation of milk by direct method
(steam injection or infusion of milk into
steam)
– long life milk production (UHT)
– removal of excess water from the product after
heat treatment
Heat treatments
The heat exchanger
• transfer heat by the indirect method
• heat transfer through the partition
• partition often corrugated to create more
turbulent flow → better heat transfer
Heat treatments
Plate heat exchanger
• pack of stainless
steel plates
clamped in a frame
• different stages of
treatment
– pre-heating, final
heating, cooling
Heat treatments
Heat treatments
• Heat exchanger in dairy industry
Centrifugation
• 4 % of fat in milk
• Lower density of fat globules compared to
water
• After 20–30 minutes from milking (milk
collection) → layer of cream on the surface
• Not proper method of fat collection
• Solution: centrifugation
Centrifugation
Centrifugal separator
• The milk enters the
disc stack through the
distribution holes
• Under the influence of
centrifugal force, the fat
globules begin to settle
in the separation
channels
– according to their
density
Centrifugation
Two products
• Cream with more than 35 % of fat
• Skim milk with less than 0.05 % of fat
• Also separation of sediment (unwanted
solid particles) during centrifugation
Standardisation of fat
Bactofugation
• Specially designed centrifuge (bactofuge)
used to separate microorganisms from
milk
• Improving the quality of milk
– especially when using heat-treatment of lower
temperatures
– e.g. during cheese production
Bactofugation
• Bacteria (esp. heat-
resistant spores):
significantly higher
density than milk
• bactofuge: useful
complement to
thermisation,
pasteurisation and
sterilisation
Homogenisation
• during 30 minutes after milking rise of fat
globules to the surface
• different fat content in the whole volume of
milk
Homogenisation
• Stokes´ Law: rising velocity of a particles
given by formula
Homogenisation
• Primarily: disruption of fat
globules into much smaller
ones
• Subsequently: smaller fat
globules in the whole
volume of milk during
storage
Homogenisation
• Disintegration of the original fat globules
achieved by a combination of contributing
factors such as turbulence and velocity
• Reduction of fat globule size from 3.5 μm
in diameter to below 1 μm
• Four- to six-fold increase in the fat/plasma
interfacial surface area
Homogenisation
• Homogenisation temperatures normally
applied: 55–80 °C
• homogenisation pressure: between 10 and
25 MPa (100–250 bar), depending on the
product
Homogenisation
Homogeniser
• milk forced though a narrow gap where the fat
globules are split
Homogenisation
• Energy demanding process: less than 1 %
of the energy is utilised for homogenisation
– pressure energy is converted into kinetic
energy
– part of energy is converted back to pressure
again after the device
– the other part is released as heat
Homogenisation
• Total homogenisation
– UHT milk and milk for production of fermented
milk product (e.g. yoghurt)
• Partial homogenisation
– only cream is homogenised and main body of
skim milk is not homogenised
– pasteurised (drinking) milk
Deaeration
• Milk contains from 6 to 9 % of gas
• Mainly CO2 and further O2 and N2
• Oxygen causes undesirable oxidation of
fat
Deaeration
Vacuum deaeration in the deaerator
• Pre-heated milk is fed to an expansion
vessel with vacuum
• Boilling point of milk is about 7 °C below
the pre-heated milk
• Water is vapoured and takes down gas
• Gas is taken away but water is condensed
and returns in the milk
Deaeration
• Flow of milk and air in
the vacuum deaerator
with built-in condeser
Pasteurised milk products
Pasteurised milk products
• Shelf-life of pasteurised milk is from 8 to 10
days at 5–7 °C in unopened package
• ESL milk – extend shelf life milk
– typical temperature/time program is 125–130 °C
for 2–4 seconds
– ultrapasteration
– shelf-life of products can be increased to 40
days
Pasteurised milk products
Packaging
• Enable efficient food distribution
• Maintain product hygiene
• Protect nutrients and flavour
• Reduce food spoilage and waste
• Increase food availability
• Convey product information
Long-life milk
In-container sterilisation
• Batch processing in autoclave
• Continuous processing systems such as
– Vertical hydrostatic towers
– Horizontal sterilisers
Long-life milk
UHT treatment
• Milk usually treated at 135–150 °C for a
few seconds
• Shelf-life of product is from months to
years
Long-life milk
UHT treatment
• Direct UHT system
– heating medium (stream) is condensed to milk
– need to be removed from milk by evaporation
in expansive chamber (vacuum, boiling point
of milk about 76 °C)
– homogenisation of milk after heat treatment –
aseptical homogenisators, increase cost
Long-life milk
UHT treatment
• Indirect UHT system
– heating medium is not condensed in milk, only
heat exchange through plate
– homogenisation before heat treatment
Thank you for your attention

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Principle of milk processing in dairy technology

  • 2. • Heat treatment • Centrifugation • Homogenisation • Standardisation • Deaeration Basic treatments of liquid milk
  • 3. Heat treatments Purposes • Food safety • Inactivation of enzymes • Prolonging of shelf life • Changes of milk compounds (some cases)
  • 4. Heat treatments Food safety • Milk as a source of infection (before heat treatment) • Perfect growth medium for microorganisms • Spread of tuberculosis and typhus by milk (previously)
  • 5. Heat treatments Food safety • Pasteurisation – Louis Pasteur – middle of 19th century – Lethal effect of heat on microorganisms – Use of heat treatment as a preservative technique
  • 6. Heat treatments Pasteurisation of milk • special type of heat treatment • definition: “any heat treatment of milk which secures the certain destruction of Tubercle bacillus (Mycobacterium tuberculosis) without markedly affecting the physical and chemical properties of the milk”
  • 7. Heat treatments Pasteurisation of milk • None of the major pathogens in milk form spores → fortune • All common pathogenic organisms likely to occur in milk: killed by relatively mild heat treatment – only a very slight effect on the physical and chemical properties of milk
  • 8. Heat treatments Pasteurisation of milk • Complete safety assured by heating milk to 63 °C for 30 minutes • Mycobacterium tuberculosis regarded as the index organism for pasteurisation – any heat treatment which destroys Mycobacterium tuberculosis ensures devastation of all other pathogens in milk
  • 9. Heat treatments Pasteurisation of milk • Content of other substances and microorganisms which may – spoil the taste – shorten the shelf life of various dairy products
  • 10. Heat treatments Secondary purpose of heat treatment • destruction of as many as possible of these other organisms and enzymatic systems • requirement of more intense heat treatment than is needed to inactivate the pathogens • heat treatment applied as quickly as possible after arrival at the dairy plant
  • 11. Heat treatments Time/temperature combination • Very important • Determination of the heat treatment intensity
  • 12. Heat treatment Time/temperature combination • Heat treatment: risk of adverse effects on – appearance – taste – nutritional value of milk
  • 13. Heat treatments Phosphatase enzyme • always present in raw milk • destroyed by the temperature/time combination necessary for efficient pasteurization • presence or absence is easily confirmed (phosphatase test) • absence of phosphatase → milk has been adequately heated
  • 14. Lethal effect curves and time/temperature curves for destruction of some enzymes and microorganims
  • 15. Heat treatments The main categories of heat treatment in the dairy industry
  • 16. Heat treatments Indirect heating • Transfer of heat from heating medium to cold product on the other side of partition
  • 17. Heat treatments Direct heating • heating medium (water) mixed with product • heat transfer efficient for rapid heating • use: sterilisation of milk by direct method (steam injection or infusion of milk into steam) – long life milk production (UHT) – removal of excess water from the product after heat treatment
  • 18. Heat treatments The heat exchanger • transfer heat by the indirect method • heat transfer through the partition • partition often corrugated to create more turbulent flow → better heat transfer
  • 19. Heat treatments Plate heat exchanger • pack of stainless steel plates clamped in a frame • different stages of treatment – pre-heating, final heating, cooling
  • 21. Heat treatments • Heat exchanger in dairy industry
  • 22. Centrifugation • 4 % of fat in milk • Lower density of fat globules compared to water • After 20–30 minutes from milking (milk collection) → layer of cream on the surface • Not proper method of fat collection • Solution: centrifugation
  • 23. Centrifugation Centrifugal separator • The milk enters the disc stack through the distribution holes • Under the influence of centrifugal force, the fat globules begin to settle in the separation channels – according to their density
  • 24. Centrifugation Two products • Cream with more than 35 % of fat • Skim milk with less than 0.05 % of fat • Also separation of sediment (unwanted solid particles) during centrifugation
  • 26. Bactofugation • Specially designed centrifuge (bactofuge) used to separate microorganisms from milk • Improving the quality of milk – especially when using heat-treatment of lower temperatures – e.g. during cheese production
  • 27. Bactofugation • Bacteria (esp. heat- resistant spores): significantly higher density than milk • bactofuge: useful complement to thermisation, pasteurisation and sterilisation
  • 28. Homogenisation • during 30 minutes after milking rise of fat globules to the surface • different fat content in the whole volume of milk
  • 29. Homogenisation • Stokes´ Law: rising velocity of a particles given by formula
  • 30. Homogenisation • Primarily: disruption of fat globules into much smaller ones • Subsequently: smaller fat globules in the whole volume of milk during storage
  • 31. Homogenisation • Disintegration of the original fat globules achieved by a combination of contributing factors such as turbulence and velocity • Reduction of fat globule size from 3.5 μm in diameter to below 1 μm • Four- to six-fold increase in the fat/plasma interfacial surface area
  • 32. Homogenisation • Homogenisation temperatures normally applied: 55–80 °C • homogenisation pressure: between 10 and 25 MPa (100–250 bar), depending on the product
  • 33. Homogenisation Homogeniser • milk forced though a narrow gap where the fat globules are split
  • 34. Homogenisation • Energy demanding process: less than 1 % of the energy is utilised for homogenisation – pressure energy is converted into kinetic energy – part of energy is converted back to pressure again after the device – the other part is released as heat
  • 35. Homogenisation • Total homogenisation – UHT milk and milk for production of fermented milk product (e.g. yoghurt) • Partial homogenisation – only cream is homogenised and main body of skim milk is not homogenised – pasteurised (drinking) milk
  • 36. Deaeration • Milk contains from 6 to 9 % of gas • Mainly CO2 and further O2 and N2 • Oxygen causes undesirable oxidation of fat
  • 37. Deaeration Vacuum deaeration in the deaerator • Pre-heated milk is fed to an expansion vessel with vacuum • Boilling point of milk is about 7 °C below the pre-heated milk • Water is vapoured and takes down gas • Gas is taken away but water is condensed and returns in the milk
  • 38. Deaeration • Flow of milk and air in the vacuum deaerator with built-in condeser
  • 40. Pasteurised milk products • Shelf-life of pasteurised milk is from 8 to 10 days at 5–7 °C in unopened package • ESL milk – extend shelf life milk – typical temperature/time program is 125–130 °C for 2–4 seconds – ultrapasteration – shelf-life of products can be increased to 40 days
  • 41. Pasteurised milk products Packaging • Enable efficient food distribution • Maintain product hygiene • Protect nutrients and flavour • Reduce food spoilage and waste • Increase food availability • Convey product information
  • 42. Long-life milk In-container sterilisation • Batch processing in autoclave • Continuous processing systems such as – Vertical hydrostatic towers – Horizontal sterilisers
  • 43. Long-life milk UHT treatment • Milk usually treated at 135–150 °C for a few seconds • Shelf-life of product is from months to years
  • 44. Long-life milk UHT treatment • Direct UHT system – heating medium (stream) is condensed to milk – need to be removed from milk by evaporation in expansive chamber (vacuum, boiling point of milk about 76 °C) – homogenisation of milk after heat treatment – aseptical homogenisators, increase cost
  • 45. Long-life milk UHT treatment • Indirect UHT system – heating medium is not condensed in milk, only heat exchange through plate – homogenisation before heat treatment
  • 46. Thank you for your attention