Trilostane 13647 35-3 coa

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SHANDONG OCTAGON CHEMICALS LIMITED

Trilostane certificate of analysis

Health & Medicine

SHANDONG OCTAGON CHEMICALS LIMITED
CERTIFICATE OF ANALYSIS
TEL:0086-15589503653 FAX:0086-0535-6715688
Address: Rm 528, Building 2, No. 300-2, Changjiang Rd, YEDA, YanTai City,
ShanDong Province, China sales@octagonchem.com
Page 1 of 1
Product name Trilostane (Cas 13647-35-3)
Batch No. 20200301 Mfg. date 2020.03.15
Rep. Date 2020.03.20 Exp. date 2022.03.14
Packaging 20kg/Drum Batch Size 350.6kg
Test Items Standards: Enterprise Results
Appearance White to off-white powder Off-white powder
Solubility
Soluble in dimethyl sulfoxide, soluble in
pyridine, slightly soluble in ethanol and water
Conforms
Identification IHPLC Conforms
Melting point 257~270°C 265~268.1°C
Specific optical
rotation
+137°~+139° +138.5°
Loss on drying NMT0.5% 0.11%
Heavy metals NMT20ppm <20ppm
Residue on ignition NMT0.1% 0.06%
Solvent residues NMT0.5% 0.12%
Related substances
Total Impurities: NMT1.0%
Single impurity: NMT0.5%
0.1%
0.03%
Assay(HPLC) NLT99% 99.87%
Conclusion It meets the requirements of Enterprise Standards
Storage Store in a well-closed container at ambient temperature
Prepared by: LI Reviewed by: WEI Released by:Zhang

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Trilostane 13647 35-3 coa

1. SHANDONG OCTAGON CHEMICALS LIMITED CERTIFICATE OF ANALYSIS TEL:0086-15589503653 FAX:0086-0535-6715688 Address: Rm 528, Building 2, No. 300-2, Changjiang Rd, YEDA, YanTai City, ShanDong Province, China sales@octagonchem.com Page 1 of 1 Product name Trilostane (Cas 13647-35-3) Batch No. 20200301 Mfg. date 2020.03.15 Rep. Date 2020.03.20 Exp. date 2022.03.14 Packaging 20kg/Drum Batch Size 350.6kg Test Items Standards: Enterprise Results Appearance White to off-white powder Off-white powder Solubility Soluble in dimethyl sulfoxide, soluble in pyridine, slightly soluble in ethanol and water Conforms Identification IHPLC Conforms Melting point 257~270°C 265~268.1°C Specific optical rotation +137°~+139° +138.5° Loss on drying NMT0.5% 0.11% Heavy metals NMT20ppm <20ppm Residue on ignition NMT0.1% 0.06% Solvent residues NMT0.5% 0.12% Related substances Total Impurities: NMT1.0% Single impurity: NMT0.5% 0.1% 0.03% Assay(HPLC) NLT99% 99.87% Conclusion It meets the requirements of Enterprise Standards Storage Store in a well-closed container at ambient temperature Prepared by: LI Reviewed by: WEI Released by:Zhang

Trilostane 13647 35-3 coa

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