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DENTURE BASE RESINS
Dr. Shiva
Introduction
•ADA specification number :- 12
REQUIREMENTS OF DENTURE BASE
MATERIALS
Biological Requirements
Chemical Requirements
Mechanical Requirements
Thermal Requirement
Esthetic Requirements
CLASSIFICATION
Type of
Materials
metallic
nonmetallic
Development
Formerly
used
Vulcanite
Bakelite
cellulose
nitrate,
Most
widely
used
PMMA
Recently
developed
Fiber
reinforced
acrylics
high impact
strength
acrylics
vinyl
acrylics
Method of
Polymerization
Addition
polymers
PMMA
Condensation
polymers
nylon
Bakelite
Method of
Activation
Thermal
Microwave
Catalyst
Visible
light
activated
Dispensing
System
Power and
liquid system
Sheets and
ropes
Gel type
HEAT ACTIVATED DENTURE BASE
ACRYLIC RESINS
•What is PMMA?
•What is Prepolymerized PMMA?
•Why the monomer bottle is dark?
Denture processing
Compression
moulding
technique
Injection
moulding
technique
Digitalized
technique
Steps
• 1. Preliminaries
• 2. Flasking
• 3. Dewaxing
• 4. Separating medium
• 5. Proportioning and mixing
• 6.Trial closure
• 7. Final closure
• 8. Bench curing
• 9. Curing cycle
• 10. Bench cooling
• 11. Deflasking
• 12. Finishing and polishing.
Bench Cooling
• The denture flask should be cooled slowly to
room temperature.
• Rapid cooling may result in warpage or distortion of
the denture base because of differences in thermal
contraction of acrylic resin and investing stone.
• 30 min and subsequently immersed in cold water for
10 min
Deflasking, Finishing and Polishing
CAD-CAM DENTURES
Why idly is one side smooth and other side
porous ?
Denture base resin
Heat
activated
Chemically
activated
Light
activated
Swaging technique
Heat cure Composition
What did you understand from this?
The truth
behind the
story
Physical reaction and chemical reaction
Polymer-monomer interaction
Setting reaction
Physical stages
Wet sandy stage
Sticky / Stringy stage
Dough stage
Rubbery stage
Stiff stage
chemical stages(except initiation all the
stages r same for heat cure & self cure )
Initiation
Propagation
Termination
Chain reaction
Why idly is one side smooth and other side
porous ?
polymer/monomer ratio
• The polymer/monomer ratio is usually 3–3.5:1 by volume or 2.5:1 by wt.
• This amount of monomer in the mix results in about 7% of volumetric
contraction.
If less polymer – more monomer
a. Polymerization
shrinkage will be
greater than 7%
b. Dough forming
time will be
prolonged.
c.There will be a
tendency for
porosity to occur in
the denture.
If more polymer- less monomer
a. Not all the polymer
will wet by monomers
and the cured acrylic
resin will be granular.
b. Dough will be
difficult to manage
Composition of self cure denture base resin
• Powder
• Poly (Methyl methacrylate) or Copolymer beads.
• Benzoyl peroxide (maximum – 2.0%) – Initiator.
• Pigments
• Colored fibers (Nylon/acrylic) – added for esthetic effect
• Liquid
• Monomer – Methyl methacrylate.
• Ethyl glycol dimethacrylate – cross-linking agent.
• Hydroquinone – inhibitor.
• Dibutyl phthalate.
• Tertiary amine (Di Methyl ParaToluidine) – Activator (max. – 0.75%).
Setting Reaction
• When polymer powder and monomer liquid are mixed together
at room temperature, free radicals are produced from benzoyl
peroxide by a reaction with dimethyl para toluidine which
initiates the polymerization reaction. Chain reaction propagates
with the liberation of heat until it is terminated.
Difference between Heat cure and Self cure
Curing Cycle
The curing cycle is the technical name for the
heating process employed to control the initial
propagation of polymerization in the denture
mould.
Normal curing cycle
Slow curing cycle Fast curing cycle
Crazing
MODIFIEDACRYLICS
• Rubber Reinforced Acrylics/High Impact Strength Materials
• Vinyl Acrylics
• Hydrophilic Poly (Acrylates)
• Rapid Heat Polymerized Acrylics/Hybrid Acrylics
• Fiber Reinforced Acrylic
• Light Activated Denture Base Resins
• Radiopaque Denture Base Resins
Radiopaque dentures
What is polymerization shrinkage?
Name physical stages of denture base resins
Name chemical stages of denture base resins
Different types of curing cycles
Crazing?
Which curing cycle is better?
Swagging technique?
Different type of denture base resin
Significance of prepolymerized PMMA
Thank you

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Denture base resins materials and its mechanism of action