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Solid catalysts are of great advantages in alkylation reaction due to heterogenous reaction which makes separation of catalysts very easy and environment friendly. Here, sulfated and borate zirconia catalysts are used to search for ortho-xylene with Toluene & methanol. To find a new path to get o-xylene, catalysts surface was studied and a new mesoporous borate zirconia catalyst was prepared. Mesoporous Borate Zirconia had showed a very efficient path to manufature o-xylene.