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CASTING
PROCEDURE FOR
FIXED PARTIAL
DENTURE
CONTENTS
 INTRODUCTION
 HISTORY
 BASIC STEPS OF CASTING
PROCEDURE
 SPRUE FORMER AND ITS ATTACHMENT
 CRUCIBLE FORMERS
 CASTING RINGS AND LINERS
 INVESTING PROCEDURE
 WAX BURNOUT
CASITNG OF ALLOY INTO MOLD
 CASTING ALLOYS
 HEAT SOURCE
 MACHINES TO INDUCE CASTING
FORCE
 RECOVERY AND CLEANING OF
CASTING
History
 11th Century Theophilus Described
lost wax technique, which was a common
practice jewelry in 11th century
1558 - Benvenuto Cellini - claimed to have
attempted use of wax and clay for preparation
of castings
1884 - Agulihon de saran used 24K gold to
form Inlay
 . 1897 - Phillibrook described a method
of casting metal filling
 1907 -Taggart -devised a practically
useful casting machine.
 Apart from this various studies
conducted on the properties of
investment materials and casting alloys
have lead a path for a better, practical
and useful processing methods.
 CASTING:- Is defined as something that
has been cast in a mold, an object
formed by the solidification of a fluid that
has been poured or injected into a
mold.(GPT-8)
CASTING PROCEDURES
FOR FIXED PARTIAL
DENTURE
 The basic steps involved in the casting
of fixed partial denture are
 1. Tooth preparation.
 2. Impression and die preparation.
 3. Wax pattern preparation.
 4. Spruing.
 5. Investing.
 6. Burnout.
 7. Casting of molten alloy.
 8. Recovery of casting, cleaning.
 9. Finishing and polishing
Objectives of casting
 1) To heat the alloy as quickly as possible to a
completely molten condition.
 2) To prevent oxidation by heating the metal
with a well adjusted torch.
 3) To produce a casting with sharp details by
having adequate pressure to the well melted
metal to force into the mold
Wax Pattern
Spruing
 The process of attaching a sprue
former/sprue pin to the wax pattern is
called as spruing
Purpose:-
 To provide a channel through which
molten alloy can reach the mold in an
invested ring after the wax has been
eliminated..
3 Basic requirements of sprue:-
 1) Must allow the molten wax to escape
from the mould.
 2) Sprue must enable the molten metal
to flow into the mould with as little
turbulence as possible.
 3) Metal must remain molten slightly
longer than the alloy that has filled the
mould
Principles of selecting an
appropriate sprue
Type of sprue
Sprues made of different materials
 1. Wax - used for casting of small and
large casting, which use single stage
burnout.
2.Plastic/Resin -
 used for castings of alloys which use 2
stage
burn out with Po4 bonded investment.
 Their main disadvantage is its softening
temperature, which is higher than wax
pattern. And may block escape of wax.
 They may be used for casting FPD‘s
because of their high rigidity, which
minimizes distortion. Plastic sprues may be
completely solid (or) hallow plastic help in
wax elimination.
3. Metal sprues
should be a non-rust metal to avoid
contamination of wax.
Hallow metallic sprue increase contact surface area
and strengthen the attachment between the sprue
and pattern.
They are removed from the investment at the same
time as the crucible former.
Care should be taken to examine for any fractured
investment material after metal sprue removal
2.Sprue gauge/size (diameter)
 Large diameter sprue:this improves the flow
of molten metal into the mould. The
diameter of sprue should be equal to the
thickest portion the wax pattern.
 less diameter sprue:causes localized
shrinkage porosity
 A narrow sprue may be useful in air
pressure casting procedure where the metal
is melted on crucible former and narrow
sprue prevent the premature metal flow into
mold.
C) Sprue length
Very short sprue : porosity in casting at
the junction of sprue and pattern.
Very long sprue : sprue solidifies first
leading to casting shrinkage and incomplete
casting
D) Sprue shape
 The sprue former should be straight to
reduce chances of creating turbulence in
molten metal entering the mold.
 High turbulence of alloy cause porosity
E) Number of sprue:
Usually a single sprue is used for
small castings.
When two thick sections of a pattern are
connected by thin part of wax, 2 separate
sprues should be attached to each thick
portion.
 The double sprue design is more
effective than the single sprue design in
decreasing the internal porosity
(jpd vol 78 no 4 oct 1997)
Attachment of sprue former and
wax pattern
 Patterns may be sprued either directly or
indirectly.
 For direct spruing ;-
 the sprue former provides a direct
connection between the pattern area
and sprue base.
 In indirect spruing -
a connector or reservoir bar is
positioned between the pattern and
crucible former.
 It is common to use indirect spruing for
multiple single units and fixed partial
dentures, although several single units
can be sprued with multiple direct sprue
formers.
Principles of spruing
a) Location of attachment
b) Angulation of sprue
c) Attachment morphology
a) Location of attachment
 The ideal location for attachment of sprue
is the thickest portion of wax pattern
 The sprue should not be located where it
can obliterate centric occulsal contacts and
centric cusp tips and margins
 Full veneer crown - sprue is attached to
Maxillary buccal and mandibular lingual
cusp.
 Partial veneer crown - sprue is attached to
cusp that encompasses the preparation.
 If attached to cusp tips near margins of wax
pattern, distortion and restriction of flow of
molten metal into mold occurs.
b) Angle of sprue attachment
 The sprue should be attached to pattern
such that it makes 45⁰ to the walls of
mold, which decreases the turbulence of
molten alloy.
 If the sprue is placed perpendicular to
the mold wall, it induces high turbulence
in molten alloy, leading to creation of a
hot spot on mold wall.
 This results in localized shrinkage
porosity
c) Attachment morphology
 The attachment of sprue former to the
wax pattern should be such that the
transition is smooth and do not posses
pits / irregularities into which investment
can flow.
 Irregularities produces tags of
investment which is prone for fracture by
molten alloy leading to casting failure.
 Usually it is flared for high density gold alloys
but restricted for low density alloys. Flaring
acts as reservoir and facilitates the entry of
molted alloy into the mold area.
 Tuccillo and Nielsen - flaring minimize
investment debris and aspirated air; allow
smooth flow of molten metal.
 Nielsen and Shalita - flaring cause the spread
of heat over an increased region.
Indirect spruing:
Indirect spruing uses the same basic
principles of spruing
But the only difference lies in attachment
of 3 running horizontal bars. The whole
indirect sprue complex consist of 3 parts.
 The need for indirect spruing
as the ambient air is colder than molten alloy
the button solidifies earlier than molten alloy. So,
it can no longer serve as a reservoir to prevent
shrink spot porosity.
The use of horizontal runner bar will act as
reservoirs of molten alloy, which equalizes the
flow to all parts of F.P.D and stabilizes the pattern
against distortion during investment.
Reservoir :
 Reservoir is a small amount of additional
wax which is added to the sprue former
near the junction of wax pattern
 It prevents localized shrinkage porosity as
the alloy in this part solidifies last after the
solidification of metal in mold
 It is used in direct spruing.
 The horizontal running bar of indirect
spacing provides the same function;
they are used when the distance
between the crucible and pattern is high.
 The reservoir is present in prefabricated
plastic sprues also.
Venting
 Small auxiliary sprues/vents are applied
to thin wax pattern to improve the quality
of casting. Usually 18- gauges sprues
are used. It is indicated with extremely
thin/thick casting to produce nonporous
castings.
They help in escape of gases during casting
and ensure beginning of solidification in critical
areas by acting as a heat sink.
It is attached to the wax pattern directly
opposite to larger sprue former. It terminates
either in investment attached to reservoir. As its
termination is near the outer wall of investment,
it solidifies first and induce solidification in main
mold.
Crucible former
 The sprue is attached to crucible former
which constitutes the base of casting
relation with casting ring during
investing.
 It also helps by holding sprue in desired
ring.
 Crucible formers are basically of 2 types---
a) Steep-sided core: used with metal when
casted using centrifugal casting force. The tall
crucible formers allow the use of short sprue.
b) Shallow cone: used to cast metal using
stream/air pressure
 They are available as----
 Rubber crucible former
 Metallic Crucible former
 Plastic crucible former
 They form a conical depression in
investment, which guides flow of molten
metal.
 It should be clean and petroleum is applied
to prevent formation of rough investment
tag.
 Molten sticky wax is applied on the apex of
cone portion of crucible former, which
contains a hole (for passing the sprue
former)
 Then the end of sprue former is passed
into the hole and held in position till the
molten wax sets.
 The attachment area should be smooth
and without irregularities to prevent
creation of investment tags which are
prone to fracture when alloy is forced
into mold.
Casting ring
 Casting rings are used to confine the
fluid investment around the wax pattern
while the investment sets.
 It also allow the hardened investment to
be safely handled during burnout and
casting
 They are available as---
1) Shapes - Round
- Oval
2)
I) Complete rings - Rigid
- Metal (stainless steel)
- Plastic
- Flexible - Rubber
II) Split rings - Metal
- Plastic
3)
I) Cylindrical
II) Conical
 Considerations in selection of castings rings: -
1) The internal diameter of casting ring should
be 5-10mm greater than the widest
measurement of the pattern and about 6 mm
higher.
2) For single crown/inlay - small rings as
used. Diameter - 32 mm
3) For large fixed partial denture – 63mm
round/oval shaped casting ring are used
Ringless casting system
Plastic ring with rubber crucible formers are
used. The ring is conical in shape with tapering
walls. As the investment sets the investment is
tapped out of ring. Then burnout is done with out
casting ring, this causes greater expansion
 Usually casting rings are rigid in nature.
Because of this the mold may become
smaller rather than larger due to the reverse
pressure resulting from confinement of the
setting expansion. To overcome this flexible
rings/ split rings are used.
 But the most commonly used technique is to
provide expansion by lining the ring with a
ring liner.
Casting ring liner
 They are commonly used to produce
expansion of mold. Various materials
used as ring liners ----
1. Asbestos liner
2. Cellulose (blotting paper) liner
3. Ceramic ring liner
4. Combination of ceramic and cellulose
ring liner
5. Wax crinkled paper
Functions of Ring liner
1. Allow uniform setting expansion of
investment by decreasing the confinement of
rigid casting ring.
2. In case of wet liner technique ---The
absorbed water help in hygroscopic expansion.
 The water in the setting investment and the
liner form a continuous phase.
 The water in liner influences expansion of
mold at a distance of at least 25mm. Wetting
of the liner prevents absorption of water by
liner (if dry) from the setting investment.
3. Thickness of the liner should be < 1mm
4. The amount of expansion depends on the
number of liners used. The expansion seen with
2 liners is greater than one liner
1. Asbestos liner: Asbestos is refractory to
high temperature, they show a sufficient amount
of water absorption. There are 3 types of
asbestos---
 White asbestos (least toxic) – this type is used
in dentistry
 Blue asbestos (most toxic)
 Brown asbestos (Intermediately toxic)
 Asbestos is this no longer used in
dentistry. As produces 3 types of
diseases
1) Asbestosis
2) Bronchogenic lung cancer
3) Mesothelioma – fatal tumour
 The carcinogenicity is due to the
dimensions and durability of asbestos
fibres.
 which are longer than 4mm and
diameter less than 1.5mm & is known to
induce Mesothelioma.
(JPD 1987; 57, 362-369)
2. Cellulose liner
 This material shows adequate water
absorption.
 It is burnt during burnout procedure. So to
keep the investment in contact with ring after
burnout
 The liner is kept 3mm short of ring ends.
 This also restricts the longitudinal setting and
hygroscopic expansion.
Procedure
9.5 cm long cellulose liner is carefully adopted on
the walls of casting ring and is tucked in position
with sticky wax.
If wet liner technique is used, the lined ring is
immersed in water for some time. Then excess
water is shaken away.
squeezing of liner should be avoided.
The liner should end 3mm short of the casting ring
end.
Ceramic ring liner
They are basically alumino-silicate fibrous
material.
 They do not absorb water to, but its network
of fibres can retain small amount of water on
its surface/wetting agents can be used to
increase the water sorption on surface.
 They are refractory to high temperature. The
binders used in ceramic liner (Ex – neoprene-
latex) can contribute to toxicity (stimulate
fibrosis/ act as adsorbent surface for
carcinogenesis).
 They show potential for development of
Mesothelioma .They posses fibers of ---
Length 5.3-17.8 mm.
Diameter 0.2- 0.97 mm
Wax crinkled paper
They were used previously.
They are waxed to internal wall of
cylinder/held in position by paper clips
INVESTING PROCEDURE
 The wax pattern should be cleaned of
any debris, grease or oils.
 For this we can use either:-
- A commercial wax pattern cleaner, or,
- A diluted synthetic detergent.
 The pattern is left to air dry while the
investment is being prepared.
 The thin film of cleanser left on the
pattern reduces the surface tension of
the wax & permits better ‗wetting‘ of the
investment to ensure complete
coverage.
 Wetting agent reduces the contact angle
of a liquid with wax surface.
 Lower contact angle indicates that
treated wax surface has an affinity for
water, which results in investment being
able to spread more easily over wax.
MIXING
Mixing of investment may be done
either by ----
i) Vacuum mixing
ii) Hand mixing
The incidence of bubble free casting
with different investing technique
– Open investing - 17%
– Vacuum investing - 95%
 The incidence of nodules on casting is
more in hand mixing then vacuum
mixing. Application of surface tension
reducing agent decreased the nodules
(Johnston, IJP, 1992, 5; 424-433).
 The best method is vacuum mix and
vacuum pour technique. But most
popular method vacuum mix and open
pour.
I) Vacuum investing
technique
1. First, hand spatulate the mix
2. With the crucible former and pattern in
place attach the ring to the mixing bowl
3. Attach the vacuum hose and mix
according to the manufacturer‘s
recommendations
4. Invert the bowl and fill the ring under
vibration
5. Remove the vacuum hose before setting
of the mixer
6. Remove the filled ring and crucible
former from the bowl
7. Immediately clean the bowl and mixing
blade under running water.
 This technique is suited for Gypsum-bonded
investment because of their fluidity after
mixing. But with phosphate-bonded
investments because of greater viscosity it
can trap air in sharp corners of the pattern
II) Vacuum mixing and hand
investing (Brushing technique)
 This technique is used in case of phosphate -
bonded investment to prevent air entrapment
and casting defects.
 In this technique mixing is done on vac-u-
vester (vacuum mixing) then before filling the
ring, the wax pattern is painted with
investment material using brush.
 Then pouring carefully around the
pattern fills the ring.
 Brush technique: In this technique,
pattern is first painted with surface
tension reducer; the surface must be
wet completely
 A finger positioned under the crucible
former on the table of the vibrator
minimizes the risk of excessive vibration
and possible breaking of the pattern
from the sprue.
 After the pattern has been completely
coated, the ring is immediately filled by
vibrating the remaining investment out of
the bowl.
 When the investment reaches the level
of the pattern, tilt the ring several times
to cover and uncover the pattern,
thereby minimizing the possible
entrapment of air.
 Investing must be performed quickly
within the working time of the
investment.
 If the investment begins to set too soon,
rinse it off quickly with cold water.
 After the ring is filled to the rim, allow the
investment to set.
 If the hygroscopic technique is used, the
ring is placed in a 37⁰C (100⁰F) water
bath for 1 hour
Advantages of vacuum mixing-----
1) Remove air bubbles
2) Produce smooth castings
3) Increase tensile strength of investment
4) 95% of castings free of nodules.
5) Removes all the gaseous by products of
chemical reaction of investment material
 Small ring: 1 package
 Large ring: 2 packages
 Hand mix for 15 seconds
 Vacuum mix for 60 seconds
 Working time: 2-3 minutes
Mixing Ratios
General ---
• More investment liquid, less water =more
expansion
• Less investment liquid, more water =less
expansion
• Begin with a dry bowl Use a maximum of 27ml of
liquid
Using more liquid results in a weak
mold
• For 100gms of investment:-Crowns/veneers:
22ml liquid,
5ml distilled water
 • Inlays/Onlays: 16ml liquid, 11ml
distilled water
 • Follow instructions on investment
packet
INVESTING OF GYPSUM BONDED
INVESTMENTS
 Require very specific W:P ratio‘s .
 A variation of only 1ml of H2O can significantly alter
the setting expansion & the character of the casting
surface.
 increasing W:P ratio makes investing process easier
but investment will lose strength,
cause cracks to occur during heating
surface of casting inferiors.
After the casting ring has been filled with investment
material, any excess should be removed before the
material sets.
 The filled ring is now set aside to allow
the investment material to complete its
setting reaction & the accompanying
setting expansion.
 Setting is complete in 30-40min.
 Hygroscopic technique is used.
- Freshly filled investment ring is
immediately placed into water bath for
30min. & kept at 100ºF(38ºC).
INVESTING OF PHOSPHATE
BONDED INVESTMENTS
Expansion of the mold cavity can be increased
by--
1) increasing the no. of layers of asbestos or
fibrous ceramic lining the casting ring.
2) increasing the special liquid : water ratio.
3) increasing the total L:P ratio.
4) Placing the investment in contact with
water during setting.
5) Burning out the mold at a higher temp.
3mm on each end is left as it serves to
lock the investment within the ring &
equalize radial & axial expansion.
 Residual, hardened investment in an unclean
mixing bowl will greatly accelerate the set of
newly mixed investment
 Phosphate investment should not be mixed in
an apparatus that has been used for gypsum
investment. Residual gypsum will also
accelerate the set & will break down at temp.
above 2400ºF(1300ºC) liberating sulfurous
gases that can be detrimental to the casting
 Ammonia gas is given off during mixing,
& it is important to hold the mixed
investment under the vacuum after
mixing ceases to dissipate some of this
gas & thereby reduce the incidence of
bubbles adhering to the wax pattern (
this additional holding time will vary from
15-45sec).
 Initial set of the phosphate bonded
investment is generally rapid with the
liberation of heat.
 If burnout is not carried within 1-2hrs,
the ring should be stored in a humidor at
100% humidity, not soaked in water
since excessive hygroscopic expansion
may result
 Rapid steam release from a water
saturated ring can fracture the investment.
 Carefully grinding or scraping the shiny
―skin‖ off the end of investment just prior to
burnout is advisable. This removes a
relatively impervious layer, opening the
pores of the investment & facilitating gas
release as the alloy is cast into the mold.
BURNOUT PROCEDURE
 Once the investment has set for an appropriate
period 45min. it is ready for burnout.
 A crucible former or any metal sprue former are
carefully removed.
 It is advisable to begin the burnout procedure
while the mold is still wet, because water trapped
in the pores of investment reduces the absorption
of wax & as water vaporizes, it flushes wax from
mold.
 This burnout after 45min. determines with a
gradual increase in temp. with wax elimination
& phenomena of crystalline inversion that
accounts for volume increase on thermal
expansion.
 Temp. of investment must be increased in
successive stages & be well defined in terms
of time.
 These time intervals bet. various successive
burnout temp. levels must be followed
Purpose of wax elimination. :-
1) To create a mold space – By wax elimination
2) To provide thermal expansion of investment.
3) To remove residual water in investment.
4) Heat soaking of investment - raises the
temperature of investment and eliminates the
temperature difference between the molten alloy
and investment
 temp difference causes incomplete casting.
 For expansion phenomena to take place
in the best possible conditions, it is
necessary that internal temp. of casting
ring gradually reach prescribed level.
 The interval between successive temp.
level is in dispersible to permit the
external heat to reach the internal areas
of casting ring
 Final burnout temp. of casting ring must
satisfy fundamental principles:-
1) Give a degree of expansion that is in
harmony with the shrinkage of alloy.
2) Maintain the viscosity of alloy at a level
necessary for complete filling of thinnest
area in mold.
3) Permit controlled cooling.
Gypsum Investments:-
 These investments are relatively fragile
& require the use of metal ring for
protection during heating.
 So, the mould are usually placed in a
furnace at room temp. & slowly heated
to 650ºC-700ºC for 60min. & held for
15-30min. at the upper temp.
 At 468⁰C for hygroscopic technique the
investment obtains its compensation
expansion from 3 sources:-
1) 37ºC water bath expands the wax pattern
2) Warm water entering the investment mould
from top adds some hygroscopic expansion.
3) Thermal expansion at this temp. provides the
needed expansion.
Advantages -----
1) Less mold degradation.
2) Cooler surface for smoother castings
3) Convenience of placing molds directly
at 468ºC
 Rate of heating has some influence on
the smoothness & in some instances on
overall dimensions.
 Rapid heating can generate steam that
can cause flaking of the mould walls.
 Too many patterns in the same plane
within the investment often cause
separation of a whole section of
investment because, expanding wax
creates excessive pressure over a large
area.
 Too rapid heating may also cause cracking
of the investment. In such case, outside
layer of the investment becomes heated
before the centre sections.
 Outside layer starts to expand thermally,
resulting in compressive stress in the
outside layer that counteracts tensile
stresses in the middle regions of the mold.
Decomposition & alloy contamination is related to
a chemical reaction between residual carbon &
CaSO4 binder.
 CaSO4 does not decompose unless it is heated
above 1000ºC.
CaSO4 + 4C CaS + 4CO
3 CaSO4 + CaS 4CaO + 4SO2
 This reaction takes place whenever gypsum
investments are heated above 700ºC in the
presence of carbon
 reduction of CaSO4 by carbon takes place
rapidly above 700ºC.
 Sulfur dioxide as a product of this reaction
contaminates gold castings & makes them
extremely brittle.
 After casting temp. has reached, the casting
should be made immediately.
 Maintaining a high temp. for a considerable
length of time may result in sulfur
contamination, rough surface
 Methods for rapid burnout procedure are
-----
- Placing the mold in a furnace at
315ºC for 30min. & then rapid heating.
Or
- Directly place into a furnace at the final
burnout temp. held for 30min. & cast.
Burnout Procedure For
Phosphate bonded Investments
PBI require:-
1) Higher burnout temp. for total elimination of
wax patterns.
2) Completion of chemical & physical changes.
3) Prevention of premature solidification of
higher melting alloys. Usual burnout temp. range
from 750⁰C-900⁰C.
.
 Total expansion of 2% or more is
required for porcelain bonding alloys,
since gold & base metal alloys require
higher melting & solidification temp.
 These investments- harder & stronger
than GBI.
 Heating rate is usually slow to 315ºC &
is quite rapid thereafter, reaching
completion after a hold at upper temp.
for 30min.
Disadvantage:-
 - Quite brittle & are subject to the same
unequal expansion of adjacent sections
as phase changes occur during heating.
TIME ALLOWABLE FOR CASTING---
 The investment contracts thermally as it cools.
 When high heat technique is used, the
investment loses heat after the heated ring is
removed from the furnace & the mould
contracts.
 Because of the liner & low thermal conductivity
of the investment, a short period can elapse
before the temp. of the mould is appreciably
affected.
Under average condition approx. 1min. can
pass without a noticeable loss in dimensions.
In low- heat casting technique, temp. gradient
between the investment mould & the room is not
as great as that employed with high- heat
technique.
Casting
 Casting of an alloy into the mold space
uses 2 basic requirements.
A) Heat source – to melt the alloy
B) Casting force – to force molten alloy into
mould casting force > surface tension of
alloy
+ resistance offered by gas in the mold
 A) Heat Source: Different types of materials and
method are used as heat source to melt alloy. Two
basic modes are by using
1)Torch flame--
Gas air
Gas oxygen
Air acetylene
Oxygen acetylene.
Hydrogen oxygen generator
2) Electricity --
Electrical resistance melting
Electrical melting
Electrical induction melting
 Crucibles : The Melting of alloy requires
a crucible to act as a platform on which
the heat can be applied to the metal.
There are three types of casting
crucibles available---
Clay
Carbon
Quartz
 Clay crucibles are used with high noble
and noble metal alloys used for crown
and bridge alloy.
 Quartz crucibles are recommended for
high-fusing alloys of any type of base
metal alloys and palladium alloys
 Carbon crucibles –
for high noble crown and bridge and also
for higher fusing gold-based metal ceramic
alloys.
 Carbon crucibles should not be used in
melting of high palladium palladium
silver alloys (to be melted above 1504⁰c)
and also with nickel-chromium/cobalt
chromium base metal alloys
 The crucibles used with noble metal
alloys should not be used for melting
base metal alloy
 Copper –containing gold alloys and non-
copper gold alloys for use with porcelain
should not be melted in the same
crucible
 Crucible should be discarded if it
contains large amount of oxides and
contaminants from previous metals
CLASSIFICATION OF DENTAL
CASTING ALLOYS
 1. ALLOY TYPES BY FUNCTIONS:
In 1927, the Bureau of Standard established
gold casting alloys, type I to type IV according
to dental function with hardness increasing from
type I to type IV.
 Type I (Soft):
 It is used for fabrication of small inlays,
class III and class V restorations which
are not subjected to great stress . These
alloys are easily burnishable
 Type -II (Medium):
 These are used for fabrication of inlays
subjected to moderate stress,
 thick 3/4 crowns, abutments, pontics,
full crowns and soft saddles.
 Type I and II are usually referred to as
inlay gold
Type -III (Hard):
 It is used for fabrication of inlays subjected to
high stress,
 thin 3/4 crowns, thin cast backing abutments,
pontics, full crowns, denture bases and short
span FPDs .
 Type III alloys can be age hardened.
 Type-IV (Extra hard):
 It is used for fabrication of inlays subjected to
high stress, denture bases, bars and clasps,
partial denture frameworks and long span
FPDs.
 These alloys can be age hardened by heat
treatment
 Type III and Type IV gold alloys are
generally called "Crown and Bridge
Alloys", although type IV alloy is used for
high stress applications such as RPD
framework
 Later, in 1960, metal ceramic alloys were
introduced and removable partial denture
alloys were added in this classification.
 Metal ceramic alloys (hard and extra hard)---
It is suitable for veneering with dental
porcelain, copings, thin walled crowns, short
span FPDs and long span FPDs. These alloy
vary greatly in composition and may be gold,
palladium, nickel or cobalt based.
 Removable partial denture alloys --
It is used for removable partial denture
frameworks. Now a days, light weight,
strong and less expensive nickel or cobalt
based have replaced type IV alloys
 2. ALLOY TYPES BY DESCRIPTION:
By description, these alloys are classified into---
A)CROWN AND BRIDGE ALLOYS
This category of alloys include both noble and base
metal alloys that have been or potentially could be
used in the fabrication of full metal or partial
veneers.
1. Noble metal alloys:
i) Gold based alloy - type III and type IV gold
alloys , low gold alloys
ii) Non-gold based alloy-Silver -palladium alloy
 2. Base metal alloys:
i) Nickel-based alloys
ii)Cobalt based alloys
 3. Other alloys:
i) Copper-zinc with Indium and nickel
ii)Silver-indium with palladium
B) METAL CERAMIC ALLOY
1.Noble metal alloys for porcelain
bonding:
 i) Gold-platinum -palladium alloy
 ii) Gold-palladium-silver alloy
 iii) Gold-palladium alloy
 iv) Palladium silver alloy
 v) High palladium alloy
2. Base metal alloys for porcelain
bonding:
 i) Nickel -chromium alloy
 ii) Cobalt-chromium alloy
C) REMOVABLE PARTIAL DENTURE ALLOY
Although type-IV noble metal alloy may be used,
majority of removable partial framework are
made from base metal alloys---
 1. Cobalt-chromium alloy
 2. Nickel-chromium alloy
 3. Cobalt-chromium-nickel alloy
 4. Silver-palladium alloy
 5. Aluminum -bronze alloy
3.ALLOY TYPE BY NOBILITY
 High noble, noble, and predominantly base metal.
 Alloy Classification of the American Dental Association
(1984)
ALLOY TYPE TOTAL NOBLE METAL CONTENT
High noble metal > 60 wt% of the noble
metal elements
Noble metal > 25 wt % of the noble metal
elements
Predominantly base metal < 25 wt % of the noble metal
elements
 Amount of metal needed: -
Usually new gold alloys should be
used for castings in case of gold alloys and
other alloys if the remounts of castings are
used.
 They should be cleaned and at least
1/3rd of a new gold pellet by weight
must be used for each melting..
Sufficient mass of alloy must be present to
sustain adequate casting pressure---
 High-density noble metal alloys.
 For premolar and anterior castings- 6
grams
 For molor castings - 9 grams
 For pontics - 12 grams
MELTING OF ALLOY
Different types of materials and method are used
as heat source to melt alloy. Two basic modes
are by using
1)Torch flame–
 Gas air
 Gas oxygen
 Air acetylene
 Oxygen acetylene.
 Hydrogen oxygen generator
 2) Electricity --
 Electrical resistance melting
 Electrical melting
 Electrical induction melting
 Expansion aids in enlarging the mold to
compensate for the casting shrinkage-
 For gold alloy-
 3 type of expansion may be seen
 1)normal setting expansion
 2)hygroscopic setting expansion
 3)thermal expansion
Hygroscopic low-heat technique
 used with gypsum bonded investment
which are allowed to set under water.
 They are used in casting gold alloys.
 The temperature used in this technique
is 482⁰c for 60-90 mins
 0.55% of expansion
High heat thermal expansion
technique
 . Gypsum bonded Investment : The
investment is slowly heated to 650⁰c -
700⁰c in 60mins. Then maintained for
15-30 mins.
 For phosphate bonded:
 This technique is used when investment
is allowed to set in open.
 The temperature of 2nd stage in this
technique depends on type of
investment material used
 After initial slow raise of temp to 315⁰c,
the temperature is rapidly raised to 750-
900⁰c and maintained for 30 mins.
 The technique cause 1.33-1.58 % of
Thermal expansion
 Normal setting expansion
-0.5%
 Hygroscopic setting expansion
-minimal-1.2%
- maximum-2.2%
Thermal expansion
-if Hygroscopic setting
expansion is used then thermal expansion
will be 0.5-0.6%
 If normal setting expansion then thermal
expansion should be 1-2%
 For Phosphate bonded
 1)wax pattern expansion;-the heat
during setting allows a significant
expansion of the wax pattern
 Setting expansion-around 0.7 to 1%
 Thermal expansion-around 1.33-1.58%
 Casting shrinkage occurs in 3 stages
 1)thermal contraction of the liquid metal
 2)contraction of metal while changing
from liquid to solid state
 3)thermal contraction of solid metal as it
cools to room temp.
 Casting shrinkage—
 Type 1- 1.56%
 Type 2-1.37%
 Type 3-1.42%
 Type 4-(ni-cr based)-2.30%
 Type4-(co-cr based)-2.30%
 Melting temp of pure gold –1063⁰c
 Melting temp of gold alloy-924-960⁰c
 Melting temp of base metal alloy-1155-
1304⁰c
 Fuel gas characteristics
 flame temp heat content
 Hydrogen: 2660⁰c 2362kcal/m3
 Natural gas:2680⁰c 8898
 Propane: 2850⁰c 21221
 Acetylene: 3140⁰c 12884
Melting of metal
 Gas air torch: -Gas-air torch is used
to melt conventional noble metal alloys
(used for inlays, crown and bridge)
whose melting points less than 1000⁰c
Gas–oxygen torch:
 Used to melt metal ceramic alloys of
higher temperature up to 1200⁰c
 The tip of torch is available as single
orifice/multiorifice.
the oxygen pressure is adjusted to
10-15 psi
 The flame is directed onto metal with
the nozzle of the torch about 1.5 cm away
from the metal.
 Complete fluid should be obtained within
30 second at which point the
metal is poured into the
mould.
Oxy-acetylene torch :
The actual production of flame can be
done by adjusting the pressure and flow of
individual gases .
commonly advised pressure for acetylene
nozzle is 3.5 N/cm2 and oxygen nozzle 7-
10 n/cm2
 The best results are obtained when
flame is used with a distance of 10cm
between the face of blow torch nozzle
and the base of crucible.
 If distance is reduced to - 7.5 mm -slight
porosity
 - 5 mm -increased porosity due to
occluded H2 gas
 When the reducing zone is in contact,
the surface of the gold alloy is bright and
mirror like.
 When the oxidizing portion of the flame
is in contact with alloy there is a dull film
of ―dross‖ developed over the surface
 II Electrical source :-
 A) Electrical resistance heated casting
machine :-
 It is used to melt ceramic alloys. Here
the alloy is automatically melted in
graphite crucible.
 provides best means of temperature
control. It is quite convenient as
compared to blow torch.
 B) Electrical arc melting:
 is used to melt higher fusing alloys.
 which is used to create a electrical arc at
the end of two electrodes
 The apparatus requires a high electrical
input (30A)
 A current is selected according to which
alloy is being melted
 One electrode is attached to the
negative terminal and the other to the
positive terminal. Both electrodes are
placed about 5cm apart
 A brilliant arc is produced around the
end of electrodes.
 The arc is directed on to the alloy , the
end of electrodes being about 12mm
away from the alloy.
High fusing alloys show rounding off of
corners and signs of collapsing, at which
point they are thrust into the mould.
C) Induction casting :
 - It is used to melt base metal alloys of
high melting temperature
 . The centrifugal casting machine is
controlled by electricity.
 Principle :- Induction casting is based on
electric currents in a metal core caused
by induction from a magnetic field.
 When high density alternating current
(high frequency 1500 KHz) is passed
through the copper coil then it will
produce electric resistance
 Because of electric resistance of coil
energy is transferred to thermal energy.
 Magnetic field is produced by current
oscillating in that particular area.induces
an oscillating current in crucible.
 Because crucible has some resistance
to the current,electric energy of current
is continuously transferd to thermal
energy
 alloy with the capability to have its
polarity changed, is placed inside the
crucible
 the rapid change of polarity produced
causes the molecules of the alloy to
oscillate and their molecular bonds to
break down.
 This high intensity of molecular activity
produces heat. The effect is that the
alloy becomes molten.
 1) Water is circulated into the machine
under pressure of 20 psi. This travels
through the copper coil to keep it cool
during the melting process.
 The metal is melted by an induction field
that develops within a crucible
surrounded by water cooled metal
tubing
 In casting machines an electronic eye is
present above the crucible.
 The starter switch is activated until the
metal becomes red in color.
 In about 30 seconds the metal will begin
to sag and a circular shadow appears to
hour over the metal.
 Eventually, the shadow will diminish in
size towards the center of crucible and
then disappear
As the shadow disappears in the
direction the induction coil is lowered and
the casting machine is activated which
usually rotate at a speed of 600 RPM. This
causes the flow of molten alloy into the
mold.
 the electricity supply to the machine
switched off and the water supply turned
off.
 If carbon crucible is used (for gold
alloys) the crucible itself becomes hot
and transfers heat to the alloy.
CASTING MACHINES
 Device for forcing the molten alloy into
the mould under pressure after wax has
been eliminated
CASTING MACHINES
 Type I
Alloy melted in crucible , followed by
application of air pressure (10-15 psi) to
force the material into the mould
 Type II
Common
Alloy is melted in separate crucible and the
metal is cast into the mould by centrifugal
force
 Type III
 Alloy melted electrically by resistance or
induction furnace & cast into the mould
by centrifugal force ( INDUCTION
CASTING)
 Type IV
 Alloy melted electrically by resistance or
induction furnace, metal cast into mould
by air pressure or vaccum
CASTING FORCE
positive force has to be applied..for molten
metal
1) Vacuum force
2) Pneumatic (steam/Gas) Pressure
3) Centrifugal force
 The casting of alloy is affected by 2
main factors :-
 1) Amount of force
 2) Time duration within which force is
applied
 The amount of force can be increased
by increasing the speed of rotation /
amount of pressure applied. The time
need to fill mold with pneumatic force is
greater than centrifugal force.
Casting by vacuum :-
Vacuum is applied to the external
surface of the investment mass, drawing
out the investment and mold gases,
allowing the melt to ingress.
 It cannot work alone in filling the mold.
So, machines are used in combination
centifugal and gas pressure.
 B) Gas pressure :-
 The metal is melted in the investment
crucible. Then gas pressure is applied
on the molten metal.
 different gases used are carbon
dioxide, carbon monoxide / nitrogen.
 They apply a pressure of 10-15 Psi
by centrifugal force :-
 This is the most feasible and commonly
used mode, for casting
 . This machine utilize the centrifugal
force which is defined as a radical force
radiating outward from the center of
rotation of a body.
 There are various types of machines which
use this principle and may be categorized
as :-
 i) a) Spring operated
 b) electrically operated
 ii) a) Horizontally rotating
 b) Vertically rotating

 ADVANTAGE: Both small and large casting
on the same machine
a) Spring operated
electrically operated
Horizontally rotating
Vertically rotating
Spring operated centrifugal
mechine
 It consists two arms
one contains the casting assembly.
 1) Cradle to seat the casting ring.
 2) Bracket to place the crucible against
the ring.
 3) Head plate to prevent
displacement of casting
ring.
 The other arm consists of appropriate
counter weight for proper rotation.
Loading pin prevents the rotation of arm.
Both arms pivot on this central spindle
Base consists of spring which rotates
central
 As the metal fills the mould a hydrostatic
pressure gradient develops along the
length of casting
 Ordinarily the pressure gradient at the
moment before solidification begins
reaches about 0.21 – 0.28 Mpa (30.40
Psi) at the tip of casting.
 Because of this pressure gradient, there
is also a gradient in the heat transfer
rate such that the greatest rate of heat
transfer to the mold is at the high
pressure end of the gradient (i.e. tip of
the casting). Because this end also is
frequently the sharp edge of the margin
of a crown,
Recovery of a casting
quenched in water as soon as the button
exhibits a dull red glow.
 Advantages of quenching:-
 1) The noble metal alloy is left in an
annealed condition for burnishing,
polishing & similar procedures.
 2) When water contact with hot
investment, a violent reaction ensues.
The investment becomes soft & granular
& the casting is more easily cleaned
 A, Trimming is done from the button end
of the ring.
B, Investment is being pushed out of the
casting ring
 C, The mold is broken open.
 D, Investment is removed from the
casting. Care must be taken to avoid
damaging the margin
sandblasting
 The casting is held in a sandblasting
machine to clean the remaining
investment from its surface.
pickling
 Surface of casting appears dark with
oxides & tarnish. Such surface film can
be removed by a process known as
pickling
 Best method for Pickling is to place the
casting in a test tube or dish & pour the
acid over it.
 May be necessary to heat the acid, but
boiling is avoided, because of
considerable amount of acid fumes
involved.
 Pickling solution should be renewed
frequently, since it is likely to become
contaminated
 Precious alloys(Gold-Platinum-
Palladium) can be soaked with
hydroflouric acid
 Nickel Chromium should never be
placed in acid because of high reactivity
TRIMMING
 The casting is trimmed , shaped and
smooth with a suitable burs or stones.
 The sprue is sectioned off with a cutting
disc.
POLISHING
 Minimum polishing is required if all the
procedures from the wax pattern to
casting are followed meticulously.
 White stone ,rubber wheels, rubber
disks, and fine grit are included in the
finishing and polishing agents
CASTING DEFECTS
Error in the procedure often results in
defective casting
 Dimensional inaccuracies &Distortion
Due to distortion of wax
Due to hygroscopic and setting
expansion
Surface roughness and
irregularites
 Surface roughness –
Cause :silica particle in investment
Inaccurate powder liquid ratio ,too rapid
heating
 Surface irregularities –nodules or fins
Cause :air bubble attached to pattern
,water film on pattern ,careless removal of
pattern
 Prevention: correct powder liquid ratio,use
of mechanical mixer , use of wetting agent
 High W/P ratio .
 Prolonged heating of the mold cavity .
 Overheating of the gold alloy .
 Too high or too low casting pressure .
 Composition of the investment .
 Foreign body inclusion
 POROSITY
 May be internal or external .
 External porosity causes discolouration .
 Internal porosity weakens the restoration
.
Classification of porosity .
 I .Those caused by solidification
shrinkage :
 a) Localised shrinkage porosity .
 b) Suck back porosity .
 c) Microporosity .
 They are usually irregular in shape
 .
 II ) Those caused by gas :
 a) Pin hole porosity .
 b) Gas inclusions .
 c) Subsurface porosity .
 Usually they are spherical in shape
 III ) Those caused by air trapped in the
mold :
 Back pressure porosity .
 Localised shrinkage porosity
 Large irregular voids found near sprue
casting junction.
 Suck back porosity
 It is an external void seen in the inside
of a crown opposite the sprue .
 Hot spot is created which freezes last .
 It is avoided by :
 Reducing the temp difference between
the mold & molten alloy
 Microporosity :
 Fine irregular voids within the casting .
 Occurs when casting freezes rapidly .
 Also when mold or casting temp is too
low .
 Pin hole porosity :
 Upon solidification the dissolved gases
are expelled from the metal causing tiny
voids .
 Pt & Pd absorb Hydrogen .
 Cu & Ag absorb oxygen
 Gas inclusion porosities
 Larger than pin hole porosities .
 May be due to dissolved gases or due to
gases Carried in or trapped by molten
metal .
 A poorly adjusted blow torech can also
occlude gases
 Back pressure porosity
 This is caused by inadequate venting of
the mold .
 This can be prevented by :
 - using adequate casting force .
 -use investment of adequate porosity .
 -place the pattern not more than 6-8 mm
away from tne end of the casting
 Incomplete casting
 This is due to :
 - insufficient alloy .
 -Alloy not able to enter thin parts of the
mold .
 -When the mold is not heated to the
casting temp .
 -Premature solidification of the alloy .
 -sprues blocked with foreign bodies .
 -Back pressure of gases .
 -low casting pressure .
 -Alloy not sufficiently molten
 Small casting :
 occurs when proper expansion is not
obtained & due to the shrinkage of the
impression
 Contamination of the casting
 1) Due to overheating there is oxidation
of metal .
 2) Use of oxidising zone of the flame .
 3) Failure to use a flux .
 4) Due to formation sulfur compounds .
 Black casting
 It is due to :
 1) Overheating of the investment .
 2) Incomplete elimination of the wax
SUMMARY &
CONCLUSION
REVIEW OF LITERATURE
 Thomas E.M (1952) conducted studies on
hygroscopic and setting expansion of
investment and find out that a confined
compensating expansion of at least 1.5 %
is necessary to compensate for the casting
shrinkage of the available inlay gold alloys.
Hygroscopic expansion when taking place
at 1000º F will compensate for the casting
shrinkage and shape of the wax pattern
has no influence on the amount of
expansion required
 Delgado et al (1953) studied hygroscopic
expansion of investment and
 Stated that:
 The use of mechanical spatulation or hand
spatulation does not affect the amount of
hygroscopic setting expansion, when a
water bath at mouth temperature is used.
 Mechanical spatulation gives higher
expansion values for thick mixes than hand
spatulation when a water bath at room
temperature is used.
 David (1963): investigated the influence of
factors on setting expansion and stated that:
 Expansion of investment away from the wax
pattern is relatively small than the expansion
of the investment surrounded by the wax
pattern.
 Greased and dry asbestos liners tend to
decrease effective setting expansion whereas
loose and double asbestos tend to increase it.
 Use of soft wax results in greater effective
setting expansion and Over spatulation and
thick mix increase setting expansion.
 Robert Neiman and Atul Sarma in 1980
studied the setting and thermal reaction of
phosphate investment. They concluded that
 The sequence of reaction based on
experimental findings were interpreted in
terms of chemical and structural presentation.
 The simple chemical reaction has been shown
to be MgO + NH4 + H2PO4 =
NH4MgPO4.6H2O. However the setting
reaction is in reality a complex system of multi
molecular structure as described.
 Alton M. lacy, Hisao Fukui et al in 1983 studied
factors affecting investment setting expansion
they studied the related effect of mixing rate,
ring liner position and storage. Their studies
reveled that
 -The rate and magnitude of of setting
expansion varied directly to the rate of mixing.
Although after 24 hrs the rapid mix investment
showed reversal of expansion. This was seen
with Gypsum bonded investment. No such
shrinkage was observed with phosphate
bonded investment
 Lacy et al (1985) stated that machine
mixing under vaccum is more effective than
hand mixing in reducing the number of
bubbles from investment. They also stated
that increasing the mixing time had a little
effect on reducing the air bubbles but
decrease liquid powder ratio favors
reduction of incidence of air bubbles.
Debubblizer is effective in reducing air
bubble adhering to the surface
 Papadopoulos T and Margrette in 1990
studied the heat rate in thermal expansion
of phosphate bonded investment. In their
study three heating rates were used one
too high (15c/min), too low (4c/min), and
one in middle (9c/min) from the results it
was concluded that rates that were too fast
must be avoided in heating procedure.
Optimum thermal expansion was found
when the heating rate was around 9c per
minute
 J.E Hutton and G.Marshel in 1995 studied
expansion of phosphate bonded
investment. The investment were mixed
with either distilled water or special liquid
and allowed a setting time of 1 or 24 hrs,
their study revealed that
 1)1 hr is optimum time for achieving
complete expansion of investment material
after mixing
 2) Mixing the material with special liquid
increases the setting expansion
REFERENCES
 ASGAR. K - Further Investigation into the nature of
hygroscopic expansion of dental Casting Investment.
J. Prosthet. Dent 1958: 8;678.
 DAVID B.M., BRUCEADY - Influence of factors on
setting expansion J.Prosthet.Dent 1963; 13:365.
 DELGADO V.P. PYTOM F.A. - The hygroscopic
Setting Expansion of dental casting Investment. J.
Prosthet. Dent 1953; 3-423.
 LACY. M. A and MORA. A. incidence of bubbles on
sample cast in phosphate bonded investment. J.
Prosthet. Dent 1985; 44, 367-369.
 THOMAS E.M. - Resume of the
expansion required to compensation for
casting gold shrinkage. J. Prosthet. Dent
1952; 550-56.
 Stephen F. Rosenstiel. Contemporary
fixed prosthodontics III Ed. 1995.
 Kenneth J. Anusavice. Phillips Science
of Dental materials. 11 th Ed. 2003.

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casting defects

  • 2. CONTENTS  INTRODUCTION  HISTORY  BASIC STEPS OF CASTING PROCEDURE  SPRUE FORMER AND ITS ATTACHMENT  CRUCIBLE FORMERS  CASTING RINGS AND LINERS  INVESTING PROCEDURE
  • 3.  WAX BURNOUT CASITNG OF ALLOY INTO MOLD  CASTING ALLOYS  HEAT SOURCE  MACHINES TO INDUCE CASTING FORCE  RECOVERY AND CLEANING OF CASTING
  • 4. History  11th Century Theophilus Described lost wax technique, which was a common practice jewelry in 11th century 1558 - Benvenuto Cellini - claimed to have attempted use of wax and clay for preparation of castings 1884 - Agulihon de saran used 24K gold to form Inlay
  • 5.  . 1897 - Phillibrook described a method of casting metal filling  1907 -Taggart -devised a practically useful casting machine.  Apart from this various studies conducted on the properties of investment materials and casting alloys have lead a path for a better, practical and useful processing methods.
  • 6.  CASTING:- Is defined as something that has been cast in a mold, an object formed by the solidification of a fluid that has been poured or injected into a mold.(GPT-8)
  • 7. CASTING PROCEDURES FOR FIXED PARTIAL DENTURE  The basic steps involved in the casting of fixed partial denture are  1. Tooth preparation.  2. Impression and die preparation.  3. Wax pattern preparation.  4. Spruing.
  • 8.  5. Investing.  6. Burnout.  7. Casting of molten alloy.  8. Recovery of casting, cleaning.  9. Finishing and polishing
  • 9. Objectives of casting  1) To heat the alloy as quickly as possible to a completely molten condition.  2) To prevent oxidation by heating the metal with a well adjusted torch.  3) To produce a casting with sharp details by having adequate pressure to the well melted metal to force into the mold
  • 11. Spruing  The process of attaching a sprue former/sprue pin to the wax pattern is called as spruing Purpose:-  To provide a channel through which molten alloy can reach the mold in an invested ring after the wax has been eliminated..
  • 12. 3 Basic requirements of sprue:-  1) Must allow the molten wax to escape from the mould.  2) Sprue must enable the molten metal to flow into the mould with as little turbulence as possible.  3) Metal must remain molten slightly longer than the alloy that has filled the mould
  • 13. Principles of selecting an appropriate sprue
  • 14. Type of sprue Sprues made of different materials  1. Wax - used for casting of small and large casting, which use single stage burnout.
  • 15. 2.Plastic/Resin -  used for castings of alloys which use 2 stage burn out with Po4 bonded investment.  Their main disadvantage is its softening temperature, which is higher than wax pattern. And may block escape of wax.  They may be used for casting FPD‘s because of their high rigidity, which minimizes distortion. Plastic sprues may be completely solid (or) hallow plastic help in wax elimination.
  • 16. 3. Metal sprues should be a non-rust metal to avoid contamination of wax. Hallow metallic sprue increase contact surface area and strengthen the attachment between the sprue and pattern. They are removed from the investment at the same time as the crucible former. Care should be taken to examine for any fractured investment material after metal sprue removal
  • 18.  Large diameter sprue:this improves the flow of molten metal into the mould. The diameter of sprue should be equal to the thickest portion the wax pattern.  less diameter sprue:causes localized shrinkage porosity  A narrow sprue may be useful in air pressure casting procedure where the metal is melted on crucible former and narrow sprue prevent the premature metal flow into mold.
  • 19. C) Sprue length Very short sprue : porosity in casting at the junction of sprue and pattern. Very long sprue : sprue solidifies first leading to casting shrinkage and incomplete casting
  • 20. D) Sprue shape  The sprue former should be straight to reduce chances of creating turbulence in molten metal entering the mold.  High turbulence of alloy cause porosity
  • 21. E) Number of sprue: Usually a single sprue is used for small castings. When two thick sections of a pattern are connected by thin part of wax, 2 separate sprues should be attached to each thick portion.
  • 22.  The double sprue design is more effective than the single sprue design in decreasing the internal porosity (jpd vol 78 no 4 oct 1997)
  • 23. Attachment of sprue former and wax pattern  Patterns may be sprued either directly or indirectly.  For direct spruing ;-  the sprue former provides a direct connection between the pattern area and sprue base.
  • 24.  In indirect spruing - a connector or reservoir bar is positioned between the pattern and crucible former.  It is common to use indirect spruing for multiple single units and fixed partial dentures, although several single units can be sprued with multiple direct sprue formers.
  • 25. Principles of spruing a) Location of attachment b) Angulation of sprue c) Attachment morphology
  • 26. a) Location of attachment  The ideal location for attachment of sprue is the thickest portion of wax pattern  The sprue should not be located where it can obliterate centric occulsal contacts and centric cusp tips and margins
  • 27.  Full veneer crown - sprue is attached to Maxillary buccal and mandibular lingual cusp.  Partial veneer crown - sprue is attached to cusp that encompasses the preparation.  If attached to cusp tips near margins of wax pattern, distortion and restriction of flow of molten metal into mold occurs.
  • 28. b) Angle of sprue attachment  The sprue should be attached to pattern such that it makes 45⁰ to the walls of mold, which decreases the turbulence of molten alloy.
  • 29.  If the sprue is placed perpendicular to the mold wall, it induces high turbulence in molten alloy, leading to creation of a hot spot on mold wall.  This results in localized shrinkage porosity
  • 30. c) Attachment morphology  The attachment of sprue former to the wax pattern should be such that the transition is smooth and do not posses pits / irregularities into which investment can flow.  Irregularities produces tags of investment which is prone for fracture by molten alloy leading to casting failure.
  • 31.  Usually it is flared for high density gold alloys but restricted for low density alloys. Flaring acts as reservoir and facilitates the entry of molted alloy into the mold area.  Tuccillo and Nielsen - flaring minimize investment debris and aspirated air; allow smooth flow of molten metal.  Nielsen and Shalita - flaring cause the spread of heat over an increased region.
  • 32. Indirect spruing: Indirect spruing uses the same basic principles of spruing But the only difference lies in attachment of 3 running horizontal bars. The whole indirect sprue complex consist of 3 parts.
  • 33.  The need for indirect spruing as the ambient air is colder than molten alloy the button solidifies earlier than molten alloy. So, it can no longer serve as a reservoir to prevent shrink spot porosity. The use of horizontal runner bar will act as reservoirs of molten alloy, which equalizes the flow to all parts of F.P.D and stabilizes the pattern against distortion during investment.
  • 34. Reservoir :  Reservoir is a small amount of additional wax which is added to the sprue former near the junction of wax pattern  It prevents localized shrinkage porosity as the alloy in this part solidifies last after the solidification of metal in mold
  • 35.  It is used in direct spruing.  The horizontal running bar of indirect spacing provides the same function; they are used when the distance between the crucible and pattern is high.  The reservoir is present in prefabricated plastic sprues also.
  • 36. Venting  Small auxiliary sprues/vents are applied to thin wax pattern to improve the quality of casting. Usually 18- gauges sprues are used. It is indicated with extremely thin/thick casting to produce nonporous castings.
  • 37. They help in escape of gases during casting and ensure beginning of solidification in critical areas by acting as a heat sink. It is attached to the wax pattern directly opposite to larger sprue former. It terminates either in investment attached to reservoir. As its termination is near the outer wall of investment, it solidifies first and induce solidification in main mold.
  • 38. Crucible former  The sprue is attached to crucible former which constitutes the base of casting relation with casting ring during investing.  It also helps by holding sprue in desired ring.
  • 39.  Crucible formers are basically of 2 types--- a) Steep-sided core: used with metal when casted using centrifugal casting force. The tall crucible formers allow the use of short sprue. b) Shallow cone: used to cast metal using stream/air pressure
  • 40.  They are available as----  Rubber crucible former  Metallic Crucible former  Plastic crucible former
  • 41.  They form a conical depression in investment, which guides flow of molten metal.  It should be clean and petroleum is applied to prevent formation of rough investment tag.  Molten sticky wax is applied on the apex of cone portion of crucible former, which contains a hole (for passing the sprue former)
  • 42.  Then the end of sprue former is passed into the hole and held in position till the molten wax sets.  The attachment area should be smooth and without irregularities to prevent creation of investment tags which are prone to fracture when alloy is forced into mold.
  • 43. Casting ring  Casting rings are used to confine the fluid investment around the wax pattern while the investment sets.  It also allow the hardened investment to be safely handled during burnout and casting
  • 44.  They are available as--- 1) Shapes - Round - Oval 2) I) Complete rings - Rigid - Metal (stainless steel) - Plastic - Flexible - Rubber II) Split rings - Metal - Plastic 3) I) Cylindrical II) Conical
  • 45.  Considerations in selection of castings rings: - 1) The internal diameter of casting ring should be 5-10mm greater than the widest measurement of the pattern and about 6 mm higher. 2) For single crown/inlay - small rings as used. Diameter - 32 mm 3) For large fixed partial denture – 63mm round/oval shaped casting ring are used
  • 46. Ringless casting system Plastic ring with rubber crucible formers are used. The ring is conical in shape with tapering walls. As the investment sets the investment is tapped out of ring. Then burnout is done with out casting ring, this causes greater expansion
  • 47.  Usually casting rings are rigid in nature. Because of this the mold may become smaller rather than larger due to the reverse pressure resulting from confinement of the setting expansion. To overcome this flexible rings/ split rings are used.  But the most commonly used technique is to provide expansion by lining the ring with a ring liner.
  • 48. Casting ring liner  They are commonly used to produce expansion of mold. Various materials used as ring liners ---- 1. Asbestos liner 2. Cellulose (blotting paper) liner 3. Ceramic ring liner 4. Combination of ceramic and cellulose ring liner 5. Wax crinkled paper
  • 49. Functions of Ring liner 1. Allow uniform setting expansion of investment by decreasing the confinement of rigid casting ring. 2. In case of wet liner technique ---The absorbed water help in hygroscopic expansion.  The water in the setting investment and the liner form a continuous phase.
  • 50.  The water in liner influences expansion of mold at a distance of at least 25mm. Wetting of the liner prevents absorption of water by liner (if dry) from the setting investment. 3. Thickness of the liner should be < 1mm 4. The amount of expansion depends on the number of liners used. The expansion seen with 2 liners is greater than one liner
  • 51. 1. Asbestos liner: Asbestos is refractory to high temperature, they show a sufficient amount of water absorption. There are 3 types of asbestos---  White asbestos (least toxic) – this type is used in dentistry  Blue asbestos (most toxic)  Brown asbestos (Intermediately toxic)
  • 52.  Asbestos is this no longer used in dentistry. As produces 3 types of diseases 1) Asbestosis 2) Bronchogenic lung cancer 3) Mesothelioma – fatal tumour
  • 53.  The carcinogenicity is due to the dimensions and durability of asbestos fibres.  which are longer than 4mm and diameter less than 1.5mm & is known to induce Mesothelioma. (JPD 1987; 57, 362-369)
  • 54. 2. Cellulose liner  This material shows adequate water absorption.  It is burnt during burnout procedure. So to keep the investment in contact with ring after burnout  The liner is kept 3mm short of ring ends.  This also restricts the longitudinal setting and hygroscopic expansion.
  • 55. Procedure 9.5 cm long cellulose liner is carefully adopted on the walls of casting ring and is tucked in position with sticky wax. If wet liner technique is used, the lined ring is immersed in water for some time. Then excess water is shaken away. squeezing of liner should be avoided. The liner should end 3mm short of the casting ring end.
  • 56. Ceramic ring liner They are basically alumino-silicate fibrous material.  They do not absorb water to, but its network of fibres can retain small amount of water on its surface/wetting agents can be used to increase the water sorption on surface.
  • 57.  They are refractory to high temperature. The binders used in ceramic liner (Ex – neoprene- latex) can contribute to toxicity (stimulate fibrosis/ act as adsorbent surface for carcinogenesis).  They show potential for development of Mesothelioma .They posses fibers of --- Length 5.3-17.8 mm. Diameter 0.2- 0.97 mm
  • 58. Wax crinkled paper They were used previously. They are waxed to internal wall of cylinder/held in position by paper clips
  • 59. INVESTING PROCEDURE  The wax pattern should be cleaned of any debris, grease or oils.  For this we can use either:- - A commercial wax pattern cleaner, or, - A diluted synthetic detergent.
  • 60.  The pattern is left to air dry while the investment is being prepared.  The thin film of cleanser left on the pattern reduces the surface tension of the wax & permits better ‗wetting‘ of the investment to ensure complete coverage.
  • 61.  Wetting agent reduces the contact angle of a liquid with wax surface.  Lower contact angle indicates that treated wax surface has an affinity for water, which results in investment being able to spread more easily over wax.
  • 62. MIXING Mixing of investment may be done either by ---- i) Vacuum mixing ii) Hand mixing The incidence of bubble free casting with different investing technique – Open investing - 17% – Vacuum investing - 95%
  • 63.  The incidence of nodules on casting is more in hand mixing then vacuum mixing. Application of surface tension reducing agent decreased the nodules (Johnston, IJP, 1992, 5; 424-433).  The best method is vacuum mix and vacuum pour technique. But most popular method vacuum mix and open pour.
  • 65. 1. First, hand spatulate the mix 2. With the crucible former and pattern in place attach the ring to the mixing bowl 3. Attach the vacuum hose and mix according to the manufacturer‘s recommendations 4. Invert the bowl and fill the ring under vibration 5. Remove the vacuum hose before setting of the mixer
  • 66. 6. Remove the filled ring and crucible former from the bowl 7. Immediately clean the bowl and mixing blade under running water.  This technique is suited for Gypsum-bonded investment because of their fluidity after mixing. But with phosphate-bonded investments because of greater viscosity it can trap air in sharp corners of the pattern
  • 67. II) Vacuum mixing and hand investing (Brushing technique)  This technique is used in case of phosphate - bonded investment to prevent air entrapment and casting defects.  In this technique mixing is done on vac-u- vester (vacuum mixing) then before filling the ring, the wax pattern is painted with investment material using brush.
  • 68.  Then pouring carefully around the pattern fills the ring.  Brush technique: In this technique, pattern is first painted with surface tension reducer; the surface must be wet completely
  • 69.  A finger positioned under the crucible former on the table of the vibrator minimizes the risk of excessive vibration and possible breaking of the pattern from the sprue.
  • 70.  After the pattern has been completely coated, the ring is immediately filled by vibrating the remaining investment out of the bowl.
  • 71.  When the investment reaches the level of the pattern, tilt the ring several times to cover and uncover the pattern, thereby minimizing the possible entrapment of air.  Investing must be performed quickly within the working time of the investment.
  • 72.  If the investment begins to set too soon, rinse it off quickly with cold water.  After the ring is filled to the rim, allow the investment to set.  If the hygroscopic technique is used, the ring is placed in a 37⁰C (100⁰F) water bath for 1 hour
  • 73. Advantages of vacuum mixing----- 1) Remove air bubbles 2) Produce smooth castings 3) Increase tensile strength of investment 4) 95% of castings free of nodules. 5) Removes all the gaseous by products of chemical reaction of investment material
  • 74.  Small ring: 1 package  Large ring: 2 packages  Hand mix for 15 seconds  Vacuum mix for 60 seconds  Working time: 2-3 minutes
  • 75. Mixing Ratios General --- • More investment liquid, less water =more expansion • Less investment liquid, more water =less expansion • Begin with a dry bowl Use a maximum of 27ml of liquid Using more liquid results in a weak mold • For 100gms of investment:-Crowns/veneers: 22ml liquid, 5ml distilled water
  • 76.  • Inlays/Onlays: 16ml liquid, 11ml distilled water  • Follow instructions on investment packet
  • 77. INVESTING OF GYPSUM BONDED INVESTMENTS  Require very specific W:P ratio‘s .  A variation of only 1ml of H2O can significantly alter the setting expansion & the character of the casting surface.  increasing W:P ratio makes investing process easier but investment will lose strength, cause cracks to occur during heating surface of casting inferiors. After the casting ring has been filled with investment material, any excess should be removed before the material sets.
  • 78.  The filled ring is now set aside to allow the investment material to complete its setting reaction & the accompanying setting expansion.  Setting is complete in 30-40min.  Hygroscopic technique is used. - Freshly filled investment ring is immediately placed into water bath for 30min. & kept at 100ºF(38ºC).
  • 79. INVESTING OF PHOSPHATE BONDED INVESTMENTS Expansion of the mold cavity can be increased by-- 1) increasing the no. of layers of asbestos or fibrous ceramic lining the casting ring. 2) increasing the special liquid : water ratio. 3) increasing the total L:P ratio.
  • 80. 4) Placing the investment in contact with water during setting. 5) Burning out the mold at a higher temp. 3mm on each end is left as it serves to lock the investment within the ring & equalize radial & axial expansion.
  • 81.  Residual, hardened investment in an unclean mixing bowl will greatly accelerate the set of newly mixed investment  Phosphate investment should not be mixed in an apparatus that has been used for gypsum investment. Residual gypsum will also accelerate the set & will break down at temp. above 2400ºF(1300ºC) liberating sulfurous gases that can be detrimental to the casting
  • 82.  Ammonia gas is given off during mixing, & it is important to hold the mixed investment under the vacuum after mixing ceases to dissipate some of this gas & thereby reduce the incidence of bubbles adhering to the wax pattern ( this additional holding time will vary from 15-45sec).
  • 83.  Initial set of the phosphate bonded investment is generally rapid with the liberation of heat.  If burnout is not carried within 1-2hrs, the ring should be stored in a humidor at 100% humidity, not soaked in water since excessive hygroscopic expansion may result
  • 84.  Rapid steam release from a water saturated ring can fracture the investment.  Carefully grinding or scraping the shiny ―skin‖ off the end of investment just prior to burnout is advisable. This removes a relatively impervious layer, opening the pores of the investment & facilitating gas release as the alloy is cast into the mold.
  • 85. BURNOUT PROCEDURE  Once the investment has set for an appropriate period 45min. it is ready for burnout.  A crucible former or any metal sprue former are carefully removed.  It is advisable to begin the burnout procedure while the mold is still wet, because water trapped in the pores of investment reduces the absorption of wax & as water vaporizes, it flushes wax from mold.
  • 86.  This burnout after 45min. determines with a gradual increase in temp. with wax elimination & phenomena of crystalline inversion that accounts for volume increase on thermal expansion.  Temp. of investment must be increased in successive stages & be well defined in terms of time.  These time intervals bet. various successive burnout temp. levels must be followed
  • 87. Purpose of wax elimination. :- 1) To create a mold space – By wax elimination 2) To provide thermal expansion of investment. 3) To remove residual water in investment. 4) Heat soaking of investment - raises the temperature of investment and eliminates the temperature difference between the molten alloy and investment  temp difference causes incomplete casting.
  • 88.
  • 89.  For expansion phenomena to take place in the best possible conditions, it is necessary that internal temp. of casting ring gradually reach prescribed level.  The interval between successive temp. level is in dispersible to permit the external heat to reach the internal areas of casting ring
  • 90.  Final burnout temp. of casting ring must satisfy fundamental principles:- 1) Give a degree of expansion that is in harmony with the shrinkage of alloy. 2) Maintain the viscosity of alloy at a level necessary for complete filling of thinnest area in mold. 3) Permit controlled cooling.
  • 91. Gypsum Investments:-  These investments are relatively fragile & require the use of metal ring for protection during heating.  So, the mould are usually placed in a furnace at room temp. & slowly heated to 650ºC-700ºC for 60min. & held for 15-30min. at the upper temp.
  • 92.  At 468⁰C for hygroscopic technique the investment obtains its compensation expansion from 3 sources:- 1) 37ºC water bath expands the wax pattern 2) Warm water entering the investment mould from top adds some hygroscopic expansion. 3) Thermal expansion at this temp. provides the needed expansion.
  • 93. Advantages ----- 1) Less mold degradation. 2) Cooler surface for smoother castings 3) Convenience of placing molds directly at 468ºC
  • 94.  Rate of heating has some influence on the smoothness & in some instances on overall dimensions.  Rapid heating can generate steam that can cause flaking of the mould walls.
  • 95.  Too many patterns in the same plane within the investment often cause separation of a whole section of investment because, expanding wax creates excessive pressure over a large area.
  • 96.  Too rapid heating may also cause cracking of the investment. In such case, outside layer of the investment becomes heated before the centre sections.  Outside layer starts to expand thermally, resulting in compressive stress in the outside layer that counteracts tensile stresses in the middle regions of the mold.
  • 97. Decomposition & alloy contamination is related to a chemical reaction between residual carbon & CaSO4 binder.  CaSO4 does not decompose unless it is heated above 1000ºC. CaSO4 + 4C CaS + 4CO 3 CaSO4 + CaS 4CaO + 4SO2  This reaction takes place whenever gypsum investments are heated above 700ºC in the presence of carbon  reduction of CaSO4 by carbon takes place rapidly above 700ºC.
  • 98.  Sulfur dioxide as a product of this reaction contaminates gold castings & makes them extremely brittle.  After casting temp. has reached, the casting should be made immediately.  Maintaining a high temp. for a considerable length of time may result in sulfur contamination, rough surface
  • 99.  Methods for rapid burnout procedure are ----- - Placing the mold in a furnace at 315ºC for 30min. & then rapid heating. Or - Directly place into a furnace at the final burnout temp. held for 30min. & cast.
  • 100. Burnout Procedure For Phosphate bonded Investments PBI require:- 1) Higher burnout temp. for total elimination of wax patterns. 2) Completion of chemical & physical changes. 3) Prevention of premature solidification of higher melting alloys. Usual burnout temp. range from 750⁰C-900⁰C. .
  • 101.  Total expansion of 2% or more is required for porcelain bonding alloys, since gold & base metal alloys require higher melting & solidification temp.  These investments- harder & stronger than GBI.
  • 102.  Heating rate is usually slow to 315ºC & is quite rapid thereafter, reaching completion after a hold at upper temp. for 30min. Disadvantage:-  - Quite brittle & are subject to the same unequal expansion of adjacent sections as phase changes occur during heating.
  • 103. TIME ALLOWABLE FOR CASTING---  The investment contracts thermally as it cools.  When high heat technique is used, the investment loses heat after the heated ring is removed from the furnace & the mould contracts.  Because of the liner & low thermal conductivity of the investment, a short period can elapse before the temp. of the mould is appreciably affected.
  • 104. Under average condition approx. 1min. can pass without a noticeable loss in dimensions. In low- heat casting technique, temp. gradient between the investment mould & the room is not as great as that employed with high- heat technique.
  • 105. Casting  Casting of an alloy into the mold space uses 2 basic requirements. A) Heat source – to melt the alloy B) Casting force – to force molten alloy into mould casting force > surface tension of alloy + resistance offered by gas in the mold
  • 106.  A) Heat Source: Different types of materials and method are used as heat source to melt alloy. Two basic modes are by using 1)Torch flame-- Gas air Gas oxygen Air acetylene Oxygen acetylene. Hydrogen oxygen generator 2) Electricity -- Electrical resistance melting Electrical melting Electrical induction melting
  • 107.  Crucibles : The Melting of alloy requires a crucible to act as a platform on which the heat can be applied to the metal. There are three types of casting crucibles available--- Clay Carbon Quartz
  • 108.  Clay crucibles are used with high noble and noble metal alloys used for crown and bridge alloy.
  • 109.  Quartz crucibles are recommended for high-fusing alloys of any type of base metal alloys and palladium alloys
  • 110.  Carbon crucibles – for high noble crown and bridge and also for higher fusing gold-based metal ceramic alloys.
  • 111.  Carbon crucibles should not be used in melting of high palladium palladium silver alloys (to be melted above 1504⁰c) and also with nickel-chromium/cobalt chromium base metal alloys  The crucibles used with noble metal alloys should not be used for melting base metal alloy
  • 112.  Copper –containing gold alloys and non- copper gold alloys for use with porcelain should not be melted in the same crucible  Crucible should be discarded if it contains large amount of oxides and contaminants from previous metals
  • 113. CLASSIFICATION OF DENTAL CASTING ALLOYS  1. ALLOY TYPES BY FUNCTIONS: In 1927, the Bureau of Standard established gold casting alloys, type I to type IV according to dental function with hardness increasing from type I to type IV.
  • 114.  Type I (Soft):  It is used for fabrication of small inlays, class III and class V restorations which are not subjected to great stress . These alloys are easily burnishable
  • 115.  Type -II (Medium):  These are used for fabrication of inlays subjected to moderate stress,  thick 3/4 crowns, abutments, pontics, full crowns and soft saddles.  Type I and II are usually referred to as inlay gold
  • 116. Type -III (Hard):  It is used for fabrication of inlays subjected to high stress,  thin 3/4 crowns, thin cast backing abutments, pontics, full crowns, denture bases and short span FPDs .  Type III alloys can be age hardened.
  • 117.  Type-IV (Extra hard):  It is used for fabrication of inlays subjected to high stress, denture bases, bars and clasps, partial denture frameworks and long span FPDs.  These alloys can be age hardened by heat treatment
  • 118.  Type III and Type IV gold alloys are generally called "Crown and Bridge Alloys", although type IV alloy is used for high stress applications such as RPD framework
  • 119.  Later, in 1960, metal ceramic alloys were introduced and removable partial denture alloys were added in this classification.  Metal ceramic alloys (hard and extra hard)--- It is suitable for veneering with dental porcelain, copings, thin walled crowns, short span FPDs and long span FPDs. These alloy vary greatly in composition and may be gold, palladium, nickel or cobalt based.
  • 120.  Removable partial denture alloys -- It is used for removable partial denture frameworks. Now a days, light weight, strong and less expensive nickel or cobalt based have replaced type IV alloys
  • 121.  2. ALLOY TYPES BY DESCRIPTION: By description, these alloys are classified into--- A)CROWN AND BRIDGE ALLOYS This category of alloys include both noble and base metal alloys that have been or potentially could be used in the fabrication of full metal or partial veneers. 1. Noble metal alloys: i) Gold based alloy - type III and type IV gold alloys , low gold alloys ii) Non-gold based alloy-Silver -palladium alloy
  • 122.  2. Base metal alloys: i) Nickel-based alloys ii)Cobalt based alloys  3. Other alloys: i) Copper-zinc with Indium and nickel ii)Silver-indium with palladium
  • 123. B) METAL CERAMIC ALLOY 1.Noble metal alloys for porcelain bonding:  i) Gold-platinum -palladium alloy  ii) Gold-palladium-silver alloy  iii) Gold-palladium alloy  iv) Palladium silver alloy  v) High palladium alloy
  • 124. 2. Base metal alloys for porcelain bonding:  i) Nickel -chromium alloy  ii) Cobalt-chromium alloy
  • 125. C) REMOVABLE PARTIAL DENTURE ALLOY Although type-IV noble metal alloy may be used, majority of removable partial framework are made from base metal alloys---  1. Cobalt-chromium alloy  2. Nickel-chromium alloy  3. Cobalt-chromium-nickel alloy  4. Silver-palladium alloy  5. Aluminum -bronze alloy
  • 126. 3.ALLOY TYPE BY NOBILITY  High noble, noble, and predominantly base metal.  Alloy Classification of the American Dental Association (1984) ALLOY TYPE TOTAL NOBLE METAL CONTENT High noble metal > 60 wt% of the noble metal elements Noble metal > 25 wt % of the noble metal elements Predominantly base metal < 25 wt % of the noble metal elements
  • 127.  Amount of metal needed: - Usually new gold alloys should be used for castings in case of gold alloys and other alloys if the remounts of castings are used.  They should be cleaned and at least 1/3rd of a new gold pellet by weight must be used for each melting..
  • 128. Sufficient mass of alloy must be present to sustain adequate casting pressure---  High-density noble metal alloys.  For premolar and anterior castings- 6 grams  For molor castings - 9 grams  For pontics - 12 grams
  • 129. MELTING OF ALLOY Different types of materials and method are used as heat source to melt alloy. Two basic modes are by using 1)Torch flame–  Gas air  Gas oxygen  Air acetylene  Oxygen acetylene.  Hydrogen oxygen generator
  • 130.  2) Electricity --  Electrical resistance melting  Electrical melting  Electrical induction melting
  • 131.
  • 132.  Expansion aids in enlarging the mold to compensate for the casting shrinkage-  For gold alloy-  3 type of expansion may be seen  1)normal setting expansion  2)hygroscopic setting expansion  3)thermal expansion
  • 133. Hygroscopic low-heat technique  used with gypsum bonded investment which are allowed to set under water.  They are used in casting gold alloys.  The temperature used in this technique is 482⁰c for 60-90 mins  0.55% of expansion
  • 134. High heat thermal expansion technique  . Gypsum bonded Investment : The investment is slowly heated to 650⁰c - 700⁰c in 60mins. Then maintained for 15-30 mins.  For phosphate bonded:  This technique is used when investment is allowed to set in open.
  • 135.  The temperature of 2nd stage in this technique depends on type of investment material used  After initial slow raise of temp to 315⁰c, the temperature is rapidly raised to 750- 900⁰c and maintained for 30 mins.  The technique cause 1.33-1.58 % of Thermal expansion
  • 136.  Normal setting expansion -0.5%  Hygroscopic setting expansion -minimal-1.2% - maximum-2.2% Thermal expansion -if Hygroscopic setting expansion is used then thermal expansion will be 0.5-0.6%
  • 137.  If normal setting expansion then thermal expansion should be 1-2%  For Phosphate bonded  1)wax pattern expansion;-the heat during setting allows a significant expansion of the wax pattern  Setting expansion-around 0.7 to 1%  Thermal expansion-around 1.33-1.58%
  • 138.  Casting shrinkage occurs in 3 stages  1)thermal contraction of the liquid metal  2)contraction of metal while changing from liquid to solid state  3)thermal contraction of solid metal as it cools to room temp.
  • 139.  Casting shrinkage—  Type 1- 1.56%  Type 2-1.37%  Type 3-1.42%  Type 4-(ni-cr based)-2.30%  Type4-(co-cr based)-2.30%
  • 140.  Melting temp of pure gold –1063⁰c  Melting temp of gold alloy-924-960⁰c  Melting temp of base metal alloy-1155- 1304⁰c
  • 141.  Fuel gas characteristics  flame temp heat content  Hydrogen: 2660⁰c 2362kcal/m3  Natural gas:2680⁰c 8898  Propane: 2850⁰c 21221  Acetylene: 3140⁰c 12884
  • 142. Melting of metal  Gas air torch: -Gas-air torch is used to melt conventional noble metal alloys (used for inlays, crown and bridge) whose melting points less than 1000⁰c
  • 143. Gas–oxygen torch:  Used to melt metal ceramic alloys of higher temperature up to 1200⁰c  The tip of torch is available as single orifice/multiorifice. the oxygen pressure is adjusted to 10-15 psi
  • 144.  The flame is directed onto metal with the nozzle of the torch about 1.5 cm away from the metal.  Complete fluid should be obtained within 30 second at which point the metal is poured into the mould.
  • 145. Oxy-acetylene torch : The actual production of flame can be done by adjusting the pressure and flow of individual gases . commonly advised pressure for acetylene nozzle is 3.5 N/cm2 and oxygen nozzle 7- 10 n/cm2
  • 146.  The best results are obtained when flame is used with a distance of 10cm between the face of blow torch nozzle and the base of crucible.  If distance is reduced to - 7.5 mm -slight porosity  - 5 mm -increased porosity due to occluded H2 gas
  • 147.  When the reducing zone is in contact, the surface of the gold alloy is bright and mirror like.  When the oxidizing portion of the flame is in contact with alloy there is a dull film of ―dross‖ developed over the surface
  • 148.  II Electrical source :-  A) Electrical resistance heated casting machine :-  It is used to melt ceramic alloys. Here the alloy is automatically melted in graphite crucible.  provides best means of temperature control. It is quite convenient as compared to blow torch.
  • 149.  B) Electrical arc melting:  is used to melt higher fusing alloys.
  • 150.  which is used to create a electrical arc at the end of two electrodes  The apparatus requires a high electrical input (30A)
  • 151.  A current is selected according to which alloy is being melted  One electrode is attached to the negative terminal and the other to the positive terminal. Both electrodes are placed about 5cm apart
  • 152.  A brilliant arc is produced around the end of electrodes.  The arc is directed on to the alloy , the end of electrodes being about 12mm away from the alloy.
  • 153. High fusing alloys show rounding off of corners and signs of collapsing, at which point they are thrust into the mould.
  • 154. C) Induction casting :  - It is used to melt base metal alloys of high melting temperature  . The centrifugal casting machine is controlled by electricity.
  • 155.  Principle :- Induction casting is based on electric currents in a metal core caused by induction from a magnetic field.
  • 156.  When high density alternating current (high frequency 1500 KHz) is passed through the copper coil then it will produce electric resistance  Because of electric resistance of coil energy is transferred to thermal energy.  Magnetic field is produced by current oscillating in that particular area.induces an oscillating current in crucible.
  • 157.  Because crucible has some resistance to the current,electric energy of current is continuously transferd to thermal energy
  • 158.  alloy with the capability to have its polarity changed, is placed inside the crucible
  • 159.  the rapid change of polarity produced causes the molecules of the alloy to oscillate and their molecular bonds to break down.  This high intensity of molecular activity produces heat. The effect is that the alloy becomes molten.
  • 160.  1) Water is circulated into the machine under pressure of 20 psi. This travels through the copper coil to keep it cool during the melting process.  The metal is melted by an induction field that develops within a crucible surrounded by water cooled metal tubing
  • 161.  In casting machines an electronic eye is present above the crucible.  The starter switch is activated until the metal becomes red in color.
  • 162.  In about 30 seconds the metal will begin to sag and a circular shadow appears to hour over the metal.  Eventually, the shadow will diminish in size towards the center of crucible and then disappear
  • 163. As the shadow disappears in the direction the induction coil is lowered and the casting machine is activated which usually rotate at a speed of 600 RPM. This causes the flow of molten alloy into the mold.
  • 164.  the electricity supply to the machine switched off and the water supply turned off.  If carbon crucible is used (for gold alloys) the crucible itself becomes hot and transfers heat to the alloy.
  • 165. CASTING MACHINES  Device for forcing the molten alloy into the mould under pressure after wax has been eliminated
  • 166. CASTING MACHINES  Type I Alloy melted in crucible , followed by application of air pressure (10-15 psi) to force the material into the mould  Type II Common Alloy is melted in separate crucible and the metal is cast into the mould by centrifugal force
  • 167.  Type III  Alloy melted electrically by resistance or induction furnace & cast into the mould by centrifugal force ( INDUCTION CASTING)
  • 168.  Type IV  Alloy melted electrically by resistance or induction furnace, metal cast into mould by air pressure or vaccum
  • 169. CASTING FORCE positive force has to be applied..for molten metal 1) Vacuum force 2) Pneumatic (steam/Gas) Pressure 3) Centrifugal force
  • 170.  The casting of alloy is affected by 2 main factors :-  1) Amount of force  2) Time duration within which force is applied  The amount of force can be increased by increasing the speed of rotation / amount of pressure applied. The time need to fill mold with pneumatic force is greater than centrifugal force.
  • 171. Casting by vacuum :- Vacuum is applied to the external surface of the investment mass, drawing out the investment and mold gases, allowing the melt to ingress.  It cannot work alone in filling the mold. So, machines are used in combination centifugal and gas pressure.
  • 172.  B) Gas pressure :-  The metal is melted in the investment crucible. Then gas pressure is applied on the molten metal.  different gases used are carbon dioxide, carbon monoxide / nitrogen.  They apply a pressure of 10-15 Psi
  • 173. by centrifugal force :-  This is the most feasible and commonly used mode, for casting  . This machine utilize the centrifugal force which is defined as a radical force radiating outward from the center of rotation of a body.
  • 174.  There are various types of machines which use this principle and may be categorized as :-  i) a) Spring operated  b) electrically operated  ii) a) Horizontally rotating  b) Vertically rotating   ADVANTAGE: Both small and large casting on the same machine
  • 179. Spring operated centrifugal mechine  It consists two arms one contains the casting assembly.  1) Cradle to seat the casting ring.  2) Bracket to place the crucible against the ring.  3) Head plate to prevent displacement of casting ring.
  • 180.
  • 181.  The other arm consists of appropriate counter weight for proper rotation. Loading pin prevents the rotation of arm. Both arms pivot on this central spindle Base consists of spring which rotates central
  • 182.
  • 183.  As the metal fills the mould a hydrostatic pressure gradient develops along the length of casting  Ordinarily the pressure gradient at the moment before solidification begins reaches about 0.21 – 0.28 Mpa (30.40 Psi) at the tip of casting.
  • 184.  Because of this pressure gradient, there is also a gradient in the heat transfer rate such that the greatest rate of heat transfer to the mold is at the high pressure end of the gradient (i.e. tip of the casting). Because this end also is frequently the sharp edge of the margin of a crown,
  • 185. Recovery of a casting quenched in water as soon as the button exhibits a dull red glow.
  • 186.  Advantages of quenching:-  1) The noble metal alloy is left in an annealed condition for burnishing, polishing & similar procedures.  2) When water contact with hot investment, a violent reaction ensues. The investment becomes soft & granular & the casting is more easily cleaned
  • 187.  A, Trimming is done from the button end of the ring. B, Investment is being pushed out of the casting ring
  • 188.  C, The mold is broken open.  D, Investment is removed from the casting. Care must be taken to avoid damaging the margin
  • 189. sandblasting  The casting is held in a sandblasting machine to clean the remaining investment from its surface.
  • 190. pickling  Surface of casting appears dark with oxides & tarnish. Such surface film can be removed by a process known as pickling  Best method for Pickling is to place the casting in a test tube or dish & pour the acid over it.
  • 191.  May be necessary to heat the acid, but boiling is avoided, because of considerable amount of acid fumes involved.  Pickling solution should be renewed frequently, since it is likely to become contaminated
  • 192.  Precious alloys(Gold-Platinum- Palladium) can be soaked with hydroflouric acid  Nickel Chromium should never be placed in acid because of high reactivity
  • 193. TRIMMING  The casting is trimmed , shaped and smooth with a suitable burs or stones.  The sprue is sectioned off with a cutting disc.
  • 194. POLISHING  Minimum polishing is required if all the procedures from the wax pattern to casting are followed meticulously.  White stone ,rubber wheels, rubber disks, and fine grit are included in the finishing and polishing agents
  • 195. CASTING DEFECTS Error in the procedure often results in defective casting  Dimensional inaccuracies &Distortion Due to distortion of wax Due to hygroscopic and setting expansion
  • 196. Surface roughness and irregularites  Surface roughness – Cause :silica particle in investment Inaccurate powder liquid ratio ,too rapid heating  Surface irregularities –nodules or fins Cause :air bubble attached to pattern ,water film on pattern ,careless removal of pattern  Prevention: correct powder liquid ratio,use of mechanical mixer , use of wetting agent
  • 197.  High W/P ratio .  Prolonged heating of the mold cavity .  Overheating of the gold alloy .  Too high or too low casting pressure .  Composition of the investment .  Foreign body inclusion
  • 198.  POROSITY  May be internal or external .  External porosity causes discolouration .  Internal porosity weakens the restoration .
  • 199. Classification of porosity .  I .Those caused by solidification shrinkage :  a) Localised shrinkage porosity .  b) Suck back porosity .  c) Microporosity .  They are usually irregular in shape
  • 200.  .  II ) Those caused by gas :  a) Pin hole porosity .  b) Gas inclusions .  c) Subsurface porosity .  Usually they are spherical in shape
  • 201.  III ) Those caused by air trapped in the mold :  Back pressure porosity .  Localised shrinkage porosity  Large irregular voids found near sprue casting junction.
  • 202.  Suck back porosity  It is an external void seen in the inside of a crown opposite the sprue .  Hot spot is created which freezes last .  It is avoided by :  Reducing the temp difference between the mold & molten alloy
  • 203.  Microporosity :  Fine irregular voids within the casting .  Occurs when casting freezes rapidly .  Also when mold or casting temp is too low .
  • 204.  Pin hole porosity :  Upon solidification the dissolved gases are expelled from the metal causing tiny voids .  Pt & Pd absorb Hydrogen .  Cu & Ag absorb oxygen
  • 205.  Gas inclusion porosities  Larger than pin hole porosities .  May be due to dissolved gases or due to gases Carried in or trapped by molten metal .  A poorly adjusted blow torech can also occlude gases
  • 206.  Back pressure porosity  This is caused by inadequate venting of the mold .  This can be prevented by :  - using adequate casting force .  -use investment of adequate porosity .  -place the pattern not more than 6-8 mm away from tne end of the casting
  • 207.  Incomplete casting  This is due to :  - insufficient alloy .  -Alloy not able to enter thin parts of the mold .  -When the mold is not heated to the casting temp .
  • 208.  -Premature solidification of the alloy .  -sprues blocked with foreign bodies .  -Back pressure of gases .  -low casting pressure .  -Alloy not sufficiently molten
  • 209.  Small casting :  occurs when proper expansion is not obtained & due to the shrinkage of the impression
  • 210.  Contamination of the casting  1) Due to overheating there is oxidation of metal .  2) Use of oxidising zone of the flame .  3) Failure to use a flux .  4) Due to formation sulfur compounds .
  • 211.  Black casting  It is due to :  1) Overheating of the investment .  2) Incomplete elimination of the wax
  • 213. REVIEW OF LITERATURE  Thomas E.M (1952) conducted studies on hygroscopic and setting expansion of investment and find out that a confined compensating expansion of at least 1.5 % is necessary to compensate for the casting shrinkage of the available inlay gold alloys. Hygroscopic expansion when taking place at 1000º F will compensate for the casting shrinkage and shape of the wax pattern has no influence on the amount of expansion required
  • 214.  Delgado et al (1953) studied hygroscopic expansion of investment and  Stated that:  The use of mechanical spatulation or hand spatulation does not affect the amount of hygroscopic setting expansion, when a water bath at mouth temperature is used.  Mechanical spatulation gives higher expansion values for thick mixes than hand spatulation when a water bath at room temperature is used.
  • 215.  David (1963): investigated the influence of factors on setting expansion and stated that:  Expansion of investment away from the wax pattern is relatively small than the expansion of the investment surrounded by the wax pattern.  Greased and dry asbestos liners tend to decrease effective setting expansion whereas loose and double asbestos tend to increase it.  Use of soft wax results in greater effective setting expansion and Over spatulation and thick mix increase setting expansion.
  • 216.  Robert Neiman and Atul Sarma in 1980 studied the setting and thermal reaction of phosphate investment. They concluded that  The sequence of reaction based on experimental findings were interpreted in terms of chemical and structural presentation.  The simple chemical reaction has been shown to be MgO + NH4 + H2PO4 = NH4MgPO4.6H2O. However the setting reaction is in reality a complex system of multi molecular structure as described.
  • 217.  Alton M. lacy, Hisao Fukui et al in 1983 studied factors affecting investment setting expansion they studied the related effect of mixing rate, ring liner position and storage. Their studies reveled that  -The rate and magnitude of of setting expansion varied directly to the rate of mixing. Although after 24 hrs the rapid mix investment showed reversal of expansion. This was seen with Gypsum bonded investment. No such shrinkage was observed with phosphate bonded investment
  • 218.  Lacy et al (1985) stated that machine mixing under vaccum is more effective than hand mixing in reducing the number of bubbles from investment. They also stated that increasing the mixing time had a little effect on reducing the air bubbles but decrease liquid powder ratio favors reduction of incidence of air bubbles. Debubblizer is effective in reducing air bubble adhering to the surface
  • 219.  Papadopoulos T and Margrette in 1990 studied the heat rate in thermal expansion of phosphate bonded investment. In their study three heating rates were used one too high (15c/min), too low (4c/min), and one in middle (9c/min) from the results it was concluded that rates that were too fast must be avoided in heating procedure. Optimum thermal expansion was found when the heating rate was around 9c per minute
  • 220.  J.E Hutton and G.Marshel in 1995 studied expansion of phosphate bonded investment. The investment were mixed with either distilled water or special liquid and allowed a setting time of 1 or 24 hrs, their study revealed that  1)1 hr is optimum time for achieving complete expansion of investment material after mixing  2) Mixing the material with special liquid increases the setting expansion
  • 221. REFERENCES  ASGAR. K - Further Investigation into the nature of hygroscopic expansion of dental Casting Investment. J. Prosthet. Dent 1958: 8;678.  DAVID B.M., BRUCEADY - Influence of factors on setting expansion J.Prosthet.Dent 1963; 13:365.  DELGADO V.P. PYTOM F.A. - The hygroscopic Setting Expansion of dental casting Investment. J. Prosthet. Dent 1953; 3-423.  LACY. M. A and MORA. A. incidence of bubbles on sample cast in phosphate bonded investment. J. Prosthet. Dent 1985; 44, 367-369.
  • 222.  THOMAS E.M. - Resume of the expansion required to compensation for casting gold shrinkage. J. Prosthet. Dent 1952; 550-56.  Stephen F. Rosenstiel. Contemporary fixed prosthodontics III Ed. 1995.  Kenneth J. Anusavice. Phillips Science of Dental materials. 11 th Ed. 2003.