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Manufacture of Cloud
Emulsions for Soft Drinks
The Advantages
Introduction
The Process
The Problem
The Solution
HIGH SHEAR MIXERS/EMULSIFIERS
FOOD
Solutions for Your TOUGHEST
MIXING Applications in
APPLICATION REPORT
Preparing a pre-emulsion with conventional agitators can lead to a number of problems:
• Powders must be added at a controlled rate to reduce agglomeration of particles.
• Conventional systems do not produce sufficient shear to break agglomerates down.
• Agitation of the solution and dispersion of powders becomes more difficult as the
viscosity increases.
• Long processing times are required to complete dispersion and achieve a satisfactory
consistency.
• A uniform pre-emulsion is required by the high pressure homogenizer. This is not
possible using conventional agitators.
• Obtaining full yield of stabilizers is difficult using traditional methods.
• Partially hydrated material can build up on the shaft of the mixer and on the vessel wall.
• The net result of conventional mixing is the product having to be passed several times
through the high pressure homogenizer to obtain the desired globule size.
The Problem
Typically cloud emulsions are oil-in-water emulsions. A typical manufacturing process
would be as follows:
• The gum (stabilizer), and any other additives would be dispersed into water to form
the continuous phase of the emulsion
• The citrus oil or other clouding agent is premixed with the weighting agent, added to
the vessel and mixed to form a pre-emulsion
• The pre-emulsion is then passed through a high pressure homogenizer to obtain the
required globule size
Clouding agents are used in soft drink manufacture to give a more natural appearance
to products with a low juice content; they can also mask sedimentation and “ringing” -
where coloring/flavoring oils rise to the surface of the container during storage.
Clouding agents are normally supplied as emulsions similar to flavor emulsions.
A typical formulation would contain the following:
• Clouding Agent:The clouding effect is obtained from fractions of oils with as neutral a
flavor as possible. Citrus oils are the most widely used; vegetable oil is used, but less
common due to poor resistance to oxidation.
• Stabilizer:The emulsion is stabilized with gum, typically gum arabic
• Weighting or Densifying Agents:Added to prevent “ringing.” Originally Brominated
Vegetable Oil (BVO) was common, but its use is now restricted.Typically resin gums
such as damar gum are used.
FOOD
The Process
Manufacture of Cloud Emulsions for Soft Drinks
FOOD
A Silverson High Shear Mixer can overcome these problems. The high shear action of
the rotor/stator workhead hydrates and disperses the powdered ingredients and
produces a finely dispersed pre-emulsion as follows:
The Solution
• After processing with a Silverson mixer, a single pass through a high pressure homogenizer
is normally sufficient to achieve the required globule size in the end product.
• The high pressure homogenizer can be eliminated in some cases.
• Typically a globule size of down to 1µm is achievable.
• Ability to start up or stop process quickly for processing of ingredients on demand.
• Agglomerate-free mix.
• Consistent product quality and repeatability.
• Stable pre-emulsion.
• Maximized yield of raw materials as thickening agents are fully hydrated and other
ingredients fully dispersed.
• Dramatic reduction in mixing times.
• Improved vessel hygiene.
The Advantages
The oil phase ingredients are added to the vessel and
an emulsion is rapidly formed. In a short mixing
cycle all the material passes through the workhead,
progressively reducing particle/globule size to
produce a stable, fine pre-emulsion.
Centrifugal force drives the materials to the
periphery of the workhead where they are sheared
in the gap between the rotor and stator. The
product is forced out of the stator and projected
radially back into the body of the mix as fresh
ingredients are drawn into the workhead.
The vessel is charged with liquid and the mixer is
started. The powdered ingredients are then added.
The high speed rotation of the rotor blades creates a
powerful suction which draws the liquid and
powdered ingredients into the workhead.
Silverson Machines,Inc. 355 Chestnut Street, East Longmeadow, MA 01028
Ph: (413) 525-4825 • Fax:(413) 525-5804 • www.silverson.com
Information contained in this report is believed to be correct and
is included as a guide only. No warranty is expressed or implied
as to fitness for use or freedom from patents. Silverson Machines
reserve the right to change product specification without notice.
Issue No. 44FA2
Silverson
In-Line
Mixer
Agitator for
in-tank
uniformity
Pipeline return below fluid
level to prevent aeration
High Shear Batch Mixers
• Suitable for batch sizes up to 400 Gallons
• Many units can be used on mobile floor stands
• Small units available for R&D and pilot production
High Shear In-Line mixers
• Ideal for larger batches
• Aeration-free
• Easily retro fitted to an existing plant
• Self pumping
• Can be used to discharge vessel
• Ultra Hygienic models available
Agitator
for in-tank
uniformity
Pipeline return configured
to minimize air entrainment
Powder
Feed
Hopper
In-Line
Mixer
Venturi
Assembly
Centrifugal
Pump
Flashblend
• Pilot through large production machines are available
• Capable of incorporating large volumes of powder
• Minimized cleaning requirements
• Minimum operator input required
• Easily automated
• Minimized dusting
There are several products in the Silverson range suitable for this application, the
selection of which is dictated by individual process requirements including
batch size.

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Food Industry Case Study: Manufacturing Cloud Emulsions in Soft Drinks

  • 1. Manufacture of Cloud Emulsions for Soft Drinks The Advantages Introduction The Process The Problem The Solution HIGH SHEAR MIXERS/EMULSIFIERS FOOD Solutions for Your TOUGHEST MIXING Applications in APPLICATION REPORT
  • 2. Preparing a pre-emulsion with conventional agitators can lead to a number of problems: • Powders must be added at a controlled rate to reduce agglomeration of particles. • Conventional systems do not produce sufficient shear to break agglomerates down. • Agitation of the solution and dispersion of powders becomes more difficult as the viscosity increases. • Long processing times are required to complete dispersion and achieve a satisfactory consistency. • A uniform pre-emulsion is required by the high pressure homogenizer. This is not possible using conventional agitators. • Obtaining full yield of stabilizers is difficult using traditional methods. • Partially hydrated material can build up on the shaft of the mixer and on the vessel wall. • The net result of conventional mixing is the product having to be passed several times through the high pressure homogenizer to obtain the desired globule size. The Problem Typically cloud emulsions are oil-in-water emulsions. A typical manufacturing process would be as follows: • The gum (stabilizer), and any other additives would be dispersed into water to form the continuous phase of the emulsion • The citrus oil or other clouding agent is premixed with the weighting agent, added to the vessel and mixed to form a pre-emulsion • The pre-emulsion is then passed through a high pressure homogenizer to obtain the required globule size Clouding agents are used in soft drink manufacture to give a more natural appearance to products with a low juice content; they can also mask sedimentation and “ringing” - where coloring/flavoring oils rise to the surface of the container during storage. Clouding agents are normally supplied as emulsions similar to flavor emulsions. A typical formulation would contain the following: • Clouding Agent:The clouding effect is obtained from fractions of oils with as neutral a flavor as possible. Citrus oils are the most widely used; vegetable oil is used, but less common due to poor resistance to oxidation. • Stabilizer:The emulsion is stabilized with gum, typically gum arabic • Weighting or Densifying Agents:Added to prevent “ringing.” Originally Brominated Vegetable Oil (BVO) was common, but its use is now restricted.Typically resin gums such as damar gum are used. FOOD The Process Manufacture of Cloud Emulsions for Soft Drinks
  • 3. FOOD A Silverson High Shear Mixer can overcome these problems. The high shear action of the rotor/stator workhead hydrates and disperses the powdered ingredients and produces a finely dispersed pre-emulsion as follows: The Solution • After processing with a Silverson mixer, a single pass through a high pressure homogenizer is normally sufficient to achieve the required globule size in the end product. • The high pressure homogenizer can be eliminated in some cases. • Typically a globule size of down to 1µm is achievable. • Ability to start up or stop process quickly for processing of ingredients on demand. • Agglomerate-free mix. • Consistent product quality and repeatability. • Stable pre-emulsion. • Maximized yield of raw materials as thickening agents are fully hydrated and other ingredients fully dispersed. • Dramatic reduction in mixing times. • Improved vessel hygiene. The Advantages The oil phase ingredients are added to the vessel and an emulsion is rapidly formed. In a short mixing cycle all the material passes through the workhead, progressively reducing particle/globule size to produce a stable, fine pre-emulsion. Centrifugal force drives the materials to the periphery of the workhead where they are sheared in the gap between the rotor and stator. The product is forced out of the stator and projected radially back into the body of the mix as fresh ingredients are drawn into the workhead. The vessel is charged with liquid and the mixer is started. The powdered ingredients are then added. The high speed rotation of the rotor blades creates a powerful suction which draws the liquid and powdered ingredients into the workhead.
  • 4. Silverson Machines,Inc. 355 Chestnut Street, East Longmeadow, MA 01028 Ph: (413) 525-4825 • Fax:(413) 525-5804 • www.silverson.com Information contained in this report is believed to be correct and is included as a guide only. No warranty is expressed or implied as to fitness for use or freedom from patents. Silverson Machines reserve the right to change product specification without notice. Issue No. 44FA2 Silverson In-Line Mixer Agitator for in-tank uniformity Pipeline return below fluid level to prevent aeration High Shear Batch Mixers • Suitable for batch sizes up to 400 Gallons • Many units can be used on mobile floor stands • Small units available for R&D and pilot production High Shear In-Line mixers • Ideal for larger batches • Aeration-free • Easily retro fitted to an existing plant • Self pumping • Can be used to discharge vessel • Ultra Hygienic models available Agitator for in-tank uniformity Pipeline return configured to minimize air entrainment Powder Feed Hopper In-Line Mixer Venturi Assembly Centrifugal Pump Flashblend • Pilot through large production machines are available • Capable of incorporating large volumes of powder • Minimized cleaning requirements • Minimum operator input required • Easily automated • Minimized dusting There are several products in the Silverson range suitable for this application, the selection of which is dictated by individual process requirements including batch size.